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Method for analyzing pore distribution of sediment by virtue of saturation change of gas hydrate

A gas hydrate and pore distribution technology, applied in the analysis of suspensions and porous materials, permeability/surface area analysis, measurement devices, etc. Effect

Active Publication Date: 2015-03-04
DALIAN UNIV OF TECH
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Problems solved by technology

However, since natural gas hydrate deposits are mostly dispersed, the traditional method of testing usually destroys the natural sediment structure, affecting the accuracy of the test

Method used

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  • Method for analyzing pore distribution of sediment by virtue of saturation change of gas hydrate
  • Method for analyzing pore distribution of sediment by virtue of saturation change of gas hydrate
  • Method for analyzing pore distribution of sediment by virtue of saturation change of gas hydrate

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Embodiment

[0017] Put the pressurized and saturated sediment in the vacuum pressure saturation device in the core tube, put the core tube in the MRI and connect the gas source, constant temperature bath, and the pipeline of the data acquisition and monitoring system, open the valve, and use the gas The injection pump injects methane gas into the core tube to 3.3 MPa and then closes the valve. Let stand for three to four hours to fully dissolve the methane in the water. After the pressure is stable, turn on the constant temperature bath to lower the temperature in the core tube to 274.15K. The pressure sensor and thermocouple will collect the pressure and temperature data in the core holder in real time, and the change of pressure and temperature can be observed through the data collection and monitoring system, and the magnetic resonance imaging will also record the signal intensity change of the water in the sediment pores in real time and the distribution of sediment pores. When the ...

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Abstract

The invention belongs to the field of geological exploration and resource development of gas hydrates and relates to a method for analyzing the pore distribution of sediment by virtue of the saturation change of a gas hydrate. According to the method, the gas hydrate is generated in the sediment by virtue of pressurization temperature reduction. In the decomposition process of the generated gas hydrate, the temperature remains unchanged. In a mode of gradually reducing the pressure, the hydrate is promoted to be gradually decomposed. The signal strength of water in the sediment in each decomposition stage and the pore distribution situation of the decomposed hydrate are measured by virtue of nuclear magnetic resonance imaging equipment. The size and total quantity of pores occupied by the gas hydrate decomposed in each stage are determined by virtue of the temperature and pressure of each decomposition stage, so that the pore distribution characteristics of the sediment are calculated and described by virtue of an image shot by nuclear magnetic resonance imaging. The method has the advantage that under the condition that the natural core structure is not destroyed, the internal porosity distribution characteristics of the sediment can be clearly identified by virtue of the generation decomposition process of the hydrate. The method is easy to operate.

Description

technical field [0001] The invention belongs to the fields of gas hydrate geological exploration and resource development, and in particular relates to a method for analyzing sediment pore distribution by using gas hydrate saturation changes. Background technique [0002] With the depletion of traditional fossil fuel resources, the discovery of natural gas hydrate is undoubtedly a huge breakthrough in the energy field. In nature, natural gas hydrates are mainly distributed in deep sea sediments or permafrost on land, which brings great difficulties to the exploitation and utilization. Accurate characterization of sediment particle size distribution, sedimentary structure, and pore structure and other microscopic physical properties can obtain reliable geological data and provide important data support for the exploration and development of gas hydrates. [0003] At present, the commonly used methods for analyzing sediments include mercury intrusion curve, X-ray diffraction,...

Claims

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Application Information

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IPC IPC(8): G01N15/08
Inventor 宋永臣杨明军经文刘卫国赵越超蒋兰兰
Owner DALIAN UNIV OF TECH
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