Preparation method of low-loss ferrite bismuth-barium titanate-based piezoelectric ceramic
A technology of bismuth ferrite and barium titanate, applied in the field of preparation of lead-free piezoelectric ceramics, can solve the problems of high dielectric loss, difficult polarization and the like, and achieve the effect of reducing volatilization
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Embodiment 1
[0019] General composition formula: 0.75(Bi 0.99 La 0.01 )FeO 3 -0.25Ba(Ti 0.98 sn 0.02 )O 3 -0.5%BiMnO 3 + 0.6%LiBiO 3 +0.6%Ba(Cu 1 / 3 Nb 2 / 3 )O 3 +0.5%Ba(W 1 / 2 Cu 1 / 2 )O 3 , the preparation method comprises the following steps:
[0020] (1) To analyze pure Fe 2 o 3 、 Bi 2 o 3 、BaCO 3 、TiO 2 , La 2 o 3 , SnO 2 , MnCO 3、 CuO, WO 3 , Nb 2 o 5 , Li2 CO 3 as raw material, according to 0.75(Bi 0.99 La 0.01 )FeO 3 -0.25Ba(Ti 0.98 sn 0.02 )O 3 -
[0021] 0.5%BiMnO 3 +0.8%LiBiO 3 +0.6%Ba(Cu 1 / 3 Nb 2 / 3 )O 3 +0.5%Ba(W 1 / 2 Cu 1 / 2 )O 3 , for batching, ball milling with absolute ethanol as the medium for 24 hours, drying at 100°C / 12 hours, sieving, putting into a high-alumina crucible with a cover, and then putting it into a closed oxygen-through tube furnace at 250°C / h The heating rate is increased to 800°C, the high pressure oxygen is added to 20MPa, and the temperature is kept for 4 hours to synthesize, and the temperature is lowered to below 200...
Embodiment 2
[0031] Composition: 0.75(Bi 0.99 La 0.01 )FeO 3 -0.25Ba(Ti 0.99 sn 0.01 )O 3 -0.5%BiMnO 3 +0.6%LiBiO 3 +
[0032] 0.6%Ba(Cu 1 / 3 Nb 2 / 3 )O 3 +0.8%Ba(W 1 / 2 Cu 1 / 2 )O 3
[0033] The preparation method is the same as in Example 1.
[0034] The performance measurements are as follows:
[0035] d 33 (pC / N) Q m k p ε r tanδ(%) 157 41 0.30 764 0.961
Embodiment 3
[0037] Composition: 0.75(Bi 0.99 La 0.01 )FeO 3 -0.25Ba(Ti 0.99 sn 0.01 )O 3 -0.5%BiMnO 3 + 0.8%LiBiO 3 +
[0038] 0.6%Ba(Cu 1 / 3 Nb 2 / 3 )O 3 +1.0%Ba(W 1 / 2 Cu 1 / 2 )O 3 The preparation method is the same as in Example 1, except that the sintering temperature is 850°C / 4h
[0039] The performance measurements are as follows:
[0040] d 33 (pC / N) Q m k p ε r tanδ(%) 138 37 0.296 730 0.984
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