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A method of pressurized production of ammonia caramel color

An ammonia caramel and process technology, applied in chemical instruments and methods, azo dyes, organic dyes, etc., can solve the problems of raising production costs, frequent ammonia additions, and complicated production operations, and reduce the overall cost of products. , Improve product market competitiveness and reduce energy consumption

Active Publication Date: 2016-09-21
QIANHE CONDIMENT & FOOD CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The result of this method is: 1. As the temperature rises during the reaction process, part of the ammonia escapes with the steam. The higher the temperature, the greater the amount of escape, and the escape gas contains higher ammonia nitrogen and COD. ,polluted environment
2. A large amount of ammonia is used, which increases production costs
3. Large amount of steam and high energy consumption
[0005] Recently, a small number of manufacturers use the pressurized method to produce ammonia products, but the frequency of ammonia addition is frequent, the production operation is more complicated, and some heat will inevitably be lost each time, and the production is not convenient, and the energy consumption is also higher.

Method used

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  • A method of pressurized production of ammonia caramel color
  • A method of pressurized production of ammonia caramel color
  • A method of pressurized production of ammonia caramel color

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] Production of 36Be, 30000EBC ammonia caramel color.

[0031] Estimate: Estimate the dry basis of the ingredients needed for the raw material based on the caramel product Baume. Considering that some water will be produced during the caramel polycondensation reaction, it is estimated that 75% of the dry basis of the raw material ingredients is more appropriate.

[0032] Dosing: Measure 6000kg of starch syrup with a DE value of 97% and a dry basis of 70% into the reaction tank, start stirring, heat up and concentrate. The temperature of the sugar solution rose from 31°C to 115°C, and the dry basis content of the sugar solution was 75% by sampling. Turn off the steam and cool for 48 minutes, and the temperature of the liquid sugar drops to 72°C.

[0033] Ammonia addition: Close the reaction tank, stir, and add ammonia directly into the sugar solution. The amount of ammonia added is 3% of the mass of raw materials, that is, 180kg of liquid ammonia needs to be added, the a...

Embodiment 2

[0042] Production of 33Be, 40000EBC ammonia caramel color.

[0043] Estimate: Estimate the dry basis of the ingredients needed for the raw material based on the caramel product Baume. Considering that some water will be produced during the caramel polycondensation reaction, it is estimated that 74% of the dry basis of the raw material ingredients is more appropriate.

[0044]Dosing: Measure 6000kg of starch syrup with a DE value of 98% and a dry basis of 68% into the reaction tank, start stirring, heat up and concentrate. The temperature of the sugar solution rose from 29°C to 113°C, and the dry basis of the sugar solution was 74% by sampling. Turn off the steam and cool for 45 minutes, and the temperature of the liquid sugar drops to 70°C.

[0045] Ammonia addition: Close the reaction tank, stir, and add ammonia directly into the sugar solution. The amount of ammonia added is 5% of the mass of the raw material, that is, 420kg of liquid ammonia is required, the ammonia addit...

Embodiment 3

[0055] In order to verify whether the pressurized method saves ammonia consumption more than the normal pressure method, the production of 36Be and 30000EBC ammonia caramel color is still taken as an example, but the ammonia addition and reaction are all carried out under normal pressure.

[0056] Dosing: Measure 6000kg of starch syrup with a DE value of 97% and a dry basis of 70% into the reaction tank. Because it is designed for normal pressure reaction, it does not need to be concentrated, and it is more convenient to add ammonia.

[0057] Ammonia addition: Start stirring, add ammonia directly into the sugar solution, the amount of ammonia added is 3% of the raw material mass, that is, 180kg of liquid ammonia needs to be added, the ammonia addition speed is 3.0kg / min, and the ammonia addition time is 60 minutes. The temperature in the reaction tank rises slowly from 39°C to 50°C. After the ammonia addition is completed, disconnect the ammonia addition connection and close th...

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Abstract

The invention relates to the field of foods, in particular to a process for producing ammonia caramel pigment by adopting a pressurization method. The process comprises the following steps: 1), raw material proportioning: adding metered starch sugar into a reaction tank and preparing 60-90% of required dry basis in the reaction tank; 2), ammonia adding: cooling the proportioned starch sugar to appropriate temperature, sealing, starting to stir in a sealing condition, starting to add ammonia, controlling the ammonia adding speed in the ammonia adding process, so as to control the pressure in the tank; 3), reacting: in a sealing condition, with the proceeding of ammonia adding, the temperature of the feed liquid rises gradually, performing Maillard reaction of the feed liquid, and performing termination reaction when the color index meets the requirement; 4), cooling: when the color index meets the requirement, quickly cooling the material to be under 80 DEG C; 5), filtering: filtering the cooled material by a filter to remove the impurities; 6), blending and conducting other steps. According to the invention, ammonia adding is only carried out at a time in the sealing condition, so that the dissolution heat of ammonia can be more effectively utilized, and the operation is simple, convenient and easy to conduct.

Description

technical field [0001] The invention relates to a production method of caramel color in food production, in particular to a process for producing ammonia-based caramel color by pressurization. Background technique [0002] Caramel color, commonly known as caramel color, is a natural food coloring obtained from sugar substances through caramelization or Maillard reaction. Caramel color is a natural coloring agent that is allowed to be used in most foods in my country. It is usually made of food-grade sugars such as glucose, fructose, sucrose, invert sugar, malt syrup, molasses, starch hydrolyzed sugar, etc., under high temperature ( Atmospheric pressure or pressurized) to make it coking, and further processed in the system. In the food industry, caramel color has a wide range of applications and a large amount. According to the statistics of the China Colorant Professional Committee, the current production and sales of caramel color account for more than 90% of the entire ed...

Claims

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Application Information

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IPC IPC(8): C09B61/00
CPCC09B61/00
Inventor 伍学明徐义刘明宣胡述勇郑小明张九龙杨九辜良燕
Owner QIANHE CONDIMENT & FOOD CO LTD
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