Method for preparing 3-methyl-4-nitrobenzoic acid by oxidizing with nitric acid
A technology of oxidation of nitrobenzoic acid and nitric acid, which is applied in the field of synthesis of fine chemical products, can solve the problems of expensive catalysts and oxidants, high production costs, and difficult processing, and achieves improved production operation safety, low manufacturing costs, The effect of improving cleanliness
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[0018] This embodiment is a method for preparing 3-methyl-4-nitrobenzoic acid by oxidation of nitric acid. The preparation of 3-methyl-4-nitrobenzoic acid uses dilute nitric acid as an oxidant and 2,4-dimethylnitrobenzene as a raw material, and is prepared in a common reaction kettle.
[0019] The specific operation steps of this embodiment are as follows:
[0020] Step 1, feeding. Put 2,4-dimethylnitrobenzene and dilute nitric acid with a concentration of 30-65% into the reactor through the elevated tank, and the molar ratio of 2,4-dimethylnitrobenzene to dilute nitric acid is 1:5.5 ~8.0.
[0021] The specific parameters of step 1 in each embodiment of table 1
[0022] Example
Dilute nitric acid concentration%
The ratio of 2,4-dimethylnitrobenzene to dilute nitric acid
1
30
1:5.5
2
30
1:6
3
30
1:6
4
30
1:6
5
30
1:8
6
45
1:8
7
45
1:8
8
45
...
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