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207results about How to "Reduce silicon content" patented technology

Method for preparing super-fine aluminum hydroxide and alumina from fly ash

ActiveCN102153117AHigh purityEliminate high temperature calcination activation stepsProductsReagentsAluminium chlorideAluminate
The invention discloses a method for preparing super-fine aluminum hydroxide and super-fine alumina by using fly ash of a circulating fluidized bed as a raw material. The method comprises the following steps of: 1, after grinding the fly ash, carrying out wet magnetic separation on the ground fly ash to remove iron and then performing a reaction of the obtained product and hydrochloric acid to obtain immersion liquid of hydrochloric acid; 2, adsorbing the immersion liquid of hydrochloric acid by filling a macroreticular cation resin column and after a resin is adsorbed and saturated, the resin is eluted by eluent to obtain the eluent containing aluminium chloride and ferric chloride; 3, carrying out alkali dissolution iron removal on the eluent to obtain sodium meta-aluminate solution; 4, adding a dispersant into the sodium meta-aluminate solution and uniformly mixing the mixture to obtain dispersion liquid; and 5, carrying out carbon dioxide decomposition on the dispersion liquid to obtain the super-fine aluminum hydroxide. Gamma-alumina and alpha-alumina can be respectively obtained by calcining the super-fine aluminum hydroxide at different temperatures. Compared with other methods, the method has the advantages of wide raw material sources, simple production process and high product purity.
Owner:CHINA SHENHUA ENERGY CO LTD

Method for preparing low-silicon vanadium pentoxide from solution containing vanadium, chromium and silicon

The invention discloses a method for preparing high-purity low-silicon vanadium pentoxide (V2O5) from a mixed solution containing vanadium, chromium and silicon. The method mainly comprises the following steps: firstly removing the silicon from the solution containing the vanadium, the chromium and the silicon by utilizing amphoteric metal salt and / or alkali metal salt, then also removing other introduced impurities by regulating the pH value of the solution and performing solid and liquid separation; afterwards, selectively extracting most of the vanadium into an organic phase according to a certain phase ratio by use of a primary amine extraction system, then also reversely extracting the vanadium in the organic phase rich in the vanadium by use of an alkaline solution containing ammonium salt, precipitating ammonium metavanadate, filtering or centrifuging the reversely-extracted water phase to obtain a high-purity ammonium metavanadate solid, washing, drying and calcining under a certain temperature to obtain a brick-red substance V2O5, wherein the purity of the V2O5 is above 99.9%, the content of silicon is smaller than 0.007% and no interlayer is formed during the extraction-reverse extraction process. The method disclosed by the invention is used for preparing the high-purity low-silicon V2O5 through processes of intensified silicon removal, extraction, reverse extraction and vanadium precipitation.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI

Method for preparing cryolite by alkaline leachate of cathode carbon block of aluminum electrolytic cell

The invention relates to a method for preparing cryolite by alkaline leachate of a cathode carbon block of an aluminum electrolytic cell, and belongs to a leachate preparation method. The method comprises the steps of grinding the cathode carbon block of the aluminum electrolytic cell to a certain particle size, mixing the ground cathode carbon block with alkaline liquid, carrying out size mixing, carrying out stirring leaching at a heating temperature of 20-90 DEG C, filtering to obtain first filtrate and a first filter residue, adding sodium fluoride and a small amount of Na3AlF6 solids into the first filtrate, controlling the introducing velocity of CO2-rich gas to generate precipitates while heating and stirring, after the reaction is finished, filtering to obtain second filtrate and a second filter residue, and drying the second filter residue at 100-150 DEG C, so as to obtain a cryolite product. According to the method, acidy leaching is replaced with alkaline leaching, so that the equipment requirements in the production process are reduced, processing processes such as flotation are omitted, an absorption process of hydrogen fluoride is omitted, and the processing process is simplified; a high-temperature processing process is saved, so that the energy consumption is reduced; and by adding crystal seeds, high-quality cryolite with the uniform particle size is generated when airflow rate is controlled. The method has the beneficial effects that the process is simple, a closed loop is utilized, the resource utilization rate is high, and the secondary pollution is avoided.
Owner:CENT SOUTH UNIV

Method for producing cryolites by using aluminum electrolytic cell cathode carbon block alkaline leaching solution

The invention relates to a method for preparing cryolites by using an aluminum electrolytic cell cathode carbon block alkaline leaching solution, and belongs to preparation methods of the cryolites. The method comprises the following steps: grinding aluminum electrolytic cell cathode carbon blocks finely to a certain particle size, performing slurry mixing with alkali liquor, and performing agitation leaching at a heating temperature of 20-90 DEG C; then performing filtration to obtain a first filtrate and a first filter residue; adding sodium fluoride and a small amount of Na3AlF6 solids into the first filtrate; then controlling the speed of introducing NH3-rich gas or adding NH4F to generate a deposit under the action of heating agitation; and after reaction, performing filtration to obtain a second filtrate and a second filter residue, and drying the second filter residue at 100-150 DEG C to obtain a cryolite product. According to the method provided by the invention, by replacing acid leaching with alkali leaching, the requirement of a production process on equipment is reduced, treatment processes including floatation are reduced, an absorption process of hydrogen fluoride is reduced, and the treatment process is simplified; a high-temperature treatment process is not used, so that the energy consumption is reduced; and by adding a crystal seed, high-quality cryolites with uniform particle sizes are generated under the condition that the airflow rate is controlled. The method provided by the invention is simple in process, achieves closed cycle, is high in resource utilization rate and avoids secondary pollution.
Owner:CENT SOUTH UNIV

Iron-increasing and silicon-reducing reselection technique for mixed-type lean iron ore tailings

ActiveCN102909124AAchieve recyclingAchieve quality improvement and silicon reductionSolid separationMechanical material recoveryIron increasedRisk stroke
The invention discloses an iron-increasing and silicon-reducing reselection technique for mixed-type lean iron ore tailings, comprising the following steps of: strong magnetic roughing: putting mixed-type lean iron ore tailings through a strong magnetic separator with the magnetic field intensity of [U1] Oersteds to obtain roughed concentrate and roughed tailings; strong magnetic cleaning: selecting the roughed concentrate in the strong magnetic separator with the magnetic field intensity of 10000-20000 Oersteds to obtain magnetic concentrate and magnetic tailings; centrifugal selecting: putting the magnetic concentrate in a centrifugal concentrating machine with the rotating speed of 150-250r/min to obtain centrifugal concentrate and centrifugal tailings; and table selecting: selecting the centrifugal tailings through a table with the stroke of 8-10mm and the frequency of stroke of 250-300 times/min to obtain table concentrate and table tailings. According to the iron-increasing and silicon-reducing reselection technique, a great quantity of tailings is dropped through rough and concentrate double magnetic selection; the magnetic concentrate is selected by using the centrifugal machine so that irons are increased and silicon is reduced; and then the centrifugal tailings are selected by using the table so that the productivity is increased. The iron-increasing and silicon-reducing reselection technique has the effects of realizing iron increment and silicon reduction of the mixed-type lean iron ore tailings, incrasing the productivity of the iron ore to a great extent at the same time and providing an effective approach to iron increment and silicon reduction of the reselected concentrate for the mixed-type lean iron ore tailings.
Owner:YUXI DAHONGSHAN MINING

Carbides-free bainite wear resistant steel plate and production process thereof

The invention relates to a steel and a production technique thereof, in particular to a non-carbide bainite wear-resistant steel plate and a production technique thereof; the component weight percentages are: 0.15 to 0.25 percent of C, 1.50 to 2.00 percent of Mn, 0 to 0.015 percent of P, 0 to 0.006 percent of S, 1.30 to 2.00 percent of Si, 0.20 to 0.60 percent of Al, 0.60 to 1.00 percent of Cr, 0.25 to 0.50 percent of Mo, 0.010 to 0.035 percent of Nb and the rest is Fe. The production technique is carried out according to the following working procedures: (1) feeding a continuous casting plate to a heating furnace for heating; (2) feeding the continuous casting plate after being heated into a hot rolling production line to carry out the rolling of controlled rolling and controlled cooling; (3) carrying out middle-low temperature drawing temper on a rolling steel plate after the rolling is finished. The non-carbide bainite wear-resistant steel plate can be produced by the working procedures without carrying out online or offline hardening and tempering thermal processing which not only can simplify the working procedures of production, but also can improve the performance and the quality of a product as well as obtain the bainite wear-resistant steel with high intensity and high toughness.
Owner:NANJING IRON & STEEL CO LTD

Technological method for reducing block masses containing carbon, iron, zinc, etc. into molten iron, zinc, etc. in blast furnace molten iron trough

Te invention discloses a production technological method for reducing oxide block masses (pellets) containing carbon, iron and/or zinc, etc. into molten iron and/or zinc, etc. in a blast furnace molten iron trough (containing a swing flow spout in front of a furnace) and belongs to the field of steel metallurgy. The production technological method is characterized in that the oxide block masses containing the carbon, iron and/or zinc, etc. are added into the blast furnace molten iron trough before blast-furnace tapping and/or during tapping, so that the iron and/or zinc, etc. in the block masses are obtained in a reduction mode through the carbon. The production technological method has the advantages that one kind or several kinds of industrial powder material of cheap blast furnace gas dust (or gas mud), gravitational dust collection dust, sintering machine dust collection dust, converter dust collection dust (or mud), steelmaking steel slag powder, oxidized iron scales, reduced iron powder, etc. and reductants of carbon-containing coal powder, coke powder, etc. are mixed and made into the block masses, the block masses are added into the blast furnace molten iron trough, and the zinc is recovered through increased iron and/or dezincification; the industrial powder material difficult to treat is treated well, so that good economic and social benefits are achieved. Meanwhile, the effect of molten iron desilicication is further achieved.
Owner:廖辉明

High-silicon nitrogen-contained austenitic stainless steel and preparing method thereof

InactiveCN106756628AExcellent resistance to high temperature concentrated sulfuric acid corrosionImprove corrosion resistanceRare-earth elementChemical composition
The invention provides high-silicon nitrogen-contained austenitic stainless steel. The high-silicon nitrogen-contained austenitic stainless steel is characterized by comprising chemical compositions including, by mass percent, 15%-20% of Cr, 15%-20% of Ni, 2%-5% of Mn, 4.5%-6.0% of Si, 1%-3% of Mo, 0.5%-1.5% of Cu, 0.1%-0.3% of N, not larger than 1.0% of Al, 0.05%-0.5% of RE, not larger than 0.03% of C, not larger than 0.010% of S, not larger than 0.02% of P and the balance Fe. The invention further provides a preparing method of the above high-silicon nitrogen-contained austenitic stainless steel. The high-silicon nitrogen-contained austenitic stainless steel is mainly used for in the field of chemical engineering, in particular to the sulfuric acid industry; the high-silicon nitrogen-contained austenitic stainless steel can be further used in the fields of food catering instruments, ornaments, environmental protection and the like; and according to the high-silicon nitrogen-contained austenitic stainless steel, by optimizing the silicon content and adding the nitrogen, the copper, the aluminum and the rare earth elements, the corrosion resistance of the stainless steel is improved, and the stainless steel has the excellent cold and heat machining performance and corrosion resistance.
Owner:JIANGSU XIHU SPECIAL STEEL

SiCf/SiC composite material flame tube and automatic preparation method thereof

The invention discloses an automatic preparation method of a SiCf/SiC composite material flame tube. The preparation method comprises the following steps: preparing an interface layer from SiC fibersby adopting chemical vapor deposition, so as to obtain SiC fibers with a continuous interface layer; performing unidirectional tape laying and filament winding on the SiC fibers with the continuous interface layer according to the fiber volume and fiber orientation obtained by simulation calculation, so as to obtain net size forming preform; performing densifying treatment on the obtained preformby adopting a reactive melt infiltration process and the chemical vapor deposition process; preparing an environmental barrier coating on the surface of the obtained preform; finally, continuously preparing a thermal barrier coating on the surface, thereby fully intelligently obtaining the high-density SiCf/SiC composite material flame tube. The SiCf/SiC composite material flame tube prepared withthe method disclosed by the invention has the characteristics of high temperature resistance and long service life and also has the advantages such as low thermal expansion coefficient, high thermalconductivity, high thermal shock resistance and excellent mechanical property. Meanwhile, the preparation method is high in degree of automation, short in production cycle, low in cost and controllable in quality.
Owner:CENT SOUTH UNIV
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