Liquid-phase hydration method separation ash treatment process

A technology of treatment process and hydration method, which is applied in the direction of alkali metal carbonate to change the content of crystallization water, etc., can solve the problems of endangering the normal operation of the separation and drying system, deteriorating the hydration operating conditions, loss of raw materials, etc., achieving low cost of process transformation, preventing Environmental pollution and waste of soda ash, the effect of improving yield

Inactive Publication Date: 2015-04-22
青岛海湾集团有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Adding separated ash to light soda ash for hydration reaction will not only seriously deteriorate the hydration operation conditions, inhibit the hydration reaction, make the hydration reaction unable to continue, but also endanger the normal operation of the subsequent separation and drying system, sometimes causing pipeline blockage, full line parking
Workers have to clean up scars, clear passages and equipment maintenance, which can take a few days or more than ten days, which requires a lot of manpower and material resources, resulting in huge loss of raw materials

Method used

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  • Liquid-phase hydration method separation ash treatment process

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Effect test

Embodiment 1

[0031] Embodiment 1, the liquid phase hydration separation ash treatment process, including the following steps:

[0032] (1) Liquid-phase hydration reaction of light ash and mother liquor is used to prepare wet sodium carbonate monohydrate;

[0033] (2) The wet material of sodium carbonate monohydrate is dried in a heavy ash fluidized bed to obtain heavy ash, and the tail gas produced by the heavy ash fluidized bed is passed into a cyclone separator to obtain separated ash and dust-containing air, wherein the separated ash The content of sodium carbonate is;

[0034] (3) The separated ash is dried in the separated ash fluidized bed to obtain heavy ash, and the tail gas generated by the separated ash fluidized bed is passed into the cyclone separator for cyclone separation again.

[0035] The separated ash is dried in a separated ash fluidized bed to obtain heavy ash with a higher content of sodium carbonate. Adding it to the heavy ash product improves the quality of the heavy ash and...

Embodiment 2

[0036] Example 2, such as figure 1 As shown, the liquid-phase hydration separation ash treatment process includes the following steps:

[0037] (1) The light ash is calcined in a light ash calciner to obtain high-temperature light soda ash and steam. The high-temperature light soda ash and mother liquor are hydrated to obtain a monohydrate containing a large amount of water, and the monohydrate containing a large amount of water is obtained Carry out solid-liquid separation through a hydrocyclone and a centrifuge to obtain a wet alkali monohydrate and mother liquor;

[0038] (2) The crushed wet sodium carbonate monohydrate is dried in a heavy ash fluidized bed to obtain heavy ash, and the tail gas generated from the heavy ash fluidized bed is passed into a cyclone separator to separate separated ash and dust-containing air;

[0039] (3) Pass the separated ash in the drying chamber of the separated ash fluidized bed with 140-160℃ hot air and the steam in the heating tube to remove mo...

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Abstract

The invention provides a liquid-phase hydration method separation ash treatment process comprising the following steps: (1) a sodium carbonate monohydrate wet material is prepared with a liquid-phase hydration method; (2) the sodium carbonate monohydrate wet material is added into a heavy ash fluidized bed, and drying is carried out, such that heavy ash is obtained; tail gas produced in the heavy ash fluidized bed is separated in a cyclone separator, such that separation ash and dust-containing air are obtained; (3) the separation ash is added into a separation ash fluidized bed, and drying is carried out, such that heavy ash and separation ash tail gas are obtained; and the separation ash tail gas is subjected to cyclone separation again in the cyclone separator. The process provided by the invention has the following advantages: separation ash is subjected to the drying treatment on the basis of an original liquid-phase hydration method heavy ash preparation process, such that separation ash alkali content is improved, and heavy ash product quality is improved; a situation of low separation ash total alkali content and the restriction on variety alkali production of prior arts are solved.

Description

Technical field [0001] The invention belongs to the field of preparing heavy ash by liquid-phase hydration, and particularly relates to a separation ash processing device by liquid-phase hydration. Background technique [0002] Sodium carbonate, common name soda, soda ash, washing soda, chemical formula Na 2 CO3, usually a white powder, is a strong electrolyte, easily soluble in water, and has the properties of salt. Soda ash is an important industrial raw material, widely used in glass, chemical, light work, metallurgy and other industries. Both heavy ash and light soda ash refer to soda ash. The difference between them is the sodium carbonate content and the salt content. In the current national soda ash standard in my country, the salt content of high-quality sodium carbonate ≤0.7% means heavy soda ash. [0003] Heavy soda ash, also called heavy ash, is granular, with a bulk density ≥0.9g / cm 3 , It has a wide range of uses, and its alkaline is generally used. Heavy soda ash ca...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C01D7/35
Inventor 代善乐石信平宋昌杰徐志国伊盛鑫刘伟伟
Owner 青岛海湾集团有限公司
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