Biodegradable linerless adhesive tapes and labels
A biodegradable, linerless technology used in the field of linerless labels and tapes, biodegradable, adhesive labels and tapes, which can solve the problem of not providing labels or tapes
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[0084] Preparation of amide diol ethylene-N,N-dihydroxycaproamide (C2C)
[0085] The C2C monomer is under nitrogen protection, in a stainless steel reactor equipped with a stirrer and a cooling water jacket, 1.2 kg of ethylenediamine (EDA) is reacted with 4.56 kg of s-caprolactone. preparation. An exothermic condensation reaction occurred between ε-caprolactone and EDA, causing the temperature to gradually rise to 80 °C, a white precipitate formed and the reactor components solidified, at which point the stirring was stopped. Then, the contents of the reactor were cooled to 20°C and then left to stand for 15 hours. The reactor contents were then heated to 140°C, at which temperature the solidified reactor contents were in a molten state. The liquid product is then discharged from the reactor to a collection pan. The molar concentration of C2C in the product was shown to exceed 80% by NMR studies. The melting point of the C2C product was determined to be 140°C.
[0086] C2...
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