Load-type nano zero-valence iron particle and preparation method therefor
A nano-zero-valent iron, load-type technology, applied in the fields of nanotechnology, nanotechnology, nanotechnology for materials and surface science, can solve the problem of uneven particle size distribution of nano-zero-valent iron particles, low reactivity, and ease of use. Problems such as agglomeration occur, and the effect of small particle size distribution range, uniform distribution and low price is achieved.
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[0037] Example 1
[0038] A supported nano-zero-valent iron particle uses modified sepiolite as a carrier, and nano-zero-valent iron particles are loaded on the surface and inside of the modified sepiolite carrier. The preparation process specifically includes the following steps:
[0039] (1) Preparation of modified sepiolite
[0040] Add a 15% hydrochloric acid aqueous solution with a concentration of 15% by mass to the natural sepiolite powder, then mix and stir it thoroughly at 25-30℃ for 48h, then wash with deoxygenated deionized water until the effluent is neutral, and then control the temperature to 115- Dry at 125°C, then control the temperature to 310-330°C for roasting, then grind, pass through a 160-200 mesh sieve, and the resulting powder is modified sepiolite;
[0041] The amount of hydrochloric acid aqueous solution with a mass percentage concentration of 15% is calculated by mass ratio, that is, natural sepiolite powder: a hydrochloric acid aqueous solution with a ma...
Example
[0052] Comparative Example 1
[0053] A nano zero-valent iron particle is prepared by a method including the following steps:
[0054] The preparation process is the same as the steps (2), (3), (4) in Example 1 except that modified sepiolite is not added, and finally nano zero-valent iron particles are obtained.
Example Embodiment
[0058] Example 2
[0059] A supported nano-zero-valent iron particle, using modified sepiolite as a carrier, and nano-zero-valent iron particles are loaded on the surface and inside of the modified sepiolite carrier. The preparation process is except for the step (3) NaBH with a concentration of 0.4mol / L 4 KBH with a concentration of 0.4mol / L for aqueous solution 4 Instead of aqueous solution, the others are the same as in Example 1.
[0060] Using transmission electron microscope equipment (JEM 2011, Jeol, Japan) to measure the supported nano-zero-valent iron particles obtained above, it can be concluded that the nano-zero-valent iron particles supported on the surface of the modified sepiolite support The diameter is 5-20 nm, and the diameter of the nano zero-valent iron particles loaded inside the modified sepiolite is about 0.01-1 nm.
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