Diagenetic evolution simulation experiment method for mud shale
A simulation experiment, mud shale technology, applied in the field of simulation experiment, can solve the problem of incompetent material composition, observation and research of diagenesis phenomenon, fine grain size of mud shale, etc.
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[0005] 1) Sample selection: for samples of different kerogen types. Select fresh shale samples with high organic matter abundance and low evolution degree.
[0006] 2) Sample preparation: cut the sample into a fixed shape (cube and sheet), the cube size is 1cmx1cmx1cm, and the sheet size is 1cmx1cmx0.5mm. The thin slice surface should be perpendicular or oblique to the bedding surface, and polished with 500 mesh, 600 mesh, 800 mesh, 1000 mesh, 1200 mesh, 1500 mesh sandpaper in sequence, and finally fully polished with 2000 mesh sandpaper.
[0007] 3) Experimental device: thermal simulation experiment system for high temperature and high pressure oil and gas formation. The system consists of an autoclave, a high temperature heating furnace, a vacuum and pressurization system, a thyristor heating control system, a temperature and pressure sensing system and a gas collection system.
[0008] 4) Sample filling: put the prepared sample into an autoclave, and add distilled water, ...
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