A kind of growth method of nano-titanium oxide on glass fiber surface
A technology of nano-titanium oxide and glass fiber, which is applied in the field of fiber modification and fiber synthesis, can solve the problems of large fixed investment, difficulty in large-scale production, and high production cost, and achieve the effects of good repeatability, low cost, and convenient operation
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Examples
Embodiment 1
[0027] A method for growing nano-titanium oxide on the surface of glass fibers, comprising the steps of:
[0028] (1) Weigh 5 g of washed chopped glass fiber, add it to 150 mL of Tris-HCl buffer solution with pH 8.2, weigh 0.2 g of dopamine solid, and shake at 180 rpm at room temperature under the condition of oxygen. After shaking for 8 hours, the glass fibers with surface dopamine polymerization were obtained.
[0029] (2) Measure 5 mL of concentrated hydrochloric acid and 15 mL of water, mix and stir for 5 minutes, then add 0.3 mL of tetrabutyl titanate dropwise, and continue stirring until the solution is clear, as the titanium source solution.
[0030] (3) Add 0.05 g of glass fiber obtained in step (1) and 20 mL of titanium source solution in step (2) into a 30 mL reactor, seal the reactor, and o C was reacted for 5 hours to obtain glass fibers with nano-titanium oxide grown on the surface.
Embodiment 2
[0032] A method for growing nano-titanium oxide on the surface of glass fibers, comprising the steps of:
[0033] (1) Weigh 5 g of washed chopped glass fiber, add it to 150 mL of Tris-HCl buffer solution with pH 8.2, weigh 0.2 g of dopamine solid, and shake at 180 rpm at room temperature under the condition of oxygen. Shake for 8 hours to obtain glass fibers with surface dopamine polymerization.
[0034] (2) Measure 5 mL of concentrated hydrochloric acid and 15 mL of water, mix and stir for 5 minutes, then add 0.5 mL of tetrabutyl titanate dropwise, and continue stirring until the solution is clear, as the titanium source solution.
[0035] (3) Add 0.05 g of glass fiber obtained in step (1) and 20 mL of titanium source solution in step (2) into a 30 mL reactor, seal the reactor, and o C was reacted for 5 hours to obtain glass fibers with nano-titanium oxide grown on the surface.
Embodiment 3
[0037] A method for growing nano-titanium oxide on the surface of glass fibers, comprising the steps of:
[0038] (1) Weigh 8 g of washed chopped glass fiber, add it to 200 mL of Tris-HCl buffer solution with pH 8.5, weigh 0.3 g of dopamine solid, shake in air at room temperature at a shaking speed of 200 rpm for 12 Hours, the glass fibers with surface dopamine polymerization were obtained.
[0039] (2) Measure 5 mL of concentrated hydrochloric acid and 15 mL of water, mix and stir for 5 minutes, then add 0.3 mL of tetrabutyl titanate dropwise, and continue stirring until the solution is clear, as the titanium source solution.
[0040] (3) Add 0.05 g of glass fiber obtained in step (1) and 20 mL of titanium source solution in step (2) into a 30 mL reactor, seal the reactor, and o C was reacted for 5 hours to obtain glass fibers with nano-titanium oxide grown on the surface.
PUM
Login to view more Abstract
Description
Claims
Application Information
Login to view more - R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap