The invention discloses a preparation method of hexaaniline cyclotriphosphazene and non-
halogen flame retardant
epoxy resin composition. The preparation method of hexaaniline cyclotriphosphazene comprises the following steps: adding
solvent, hexachlorocyclotriphosphazene,
aniline and acid-binding agent into a reaction device, stirring and introducing
nitrogen for protection, heating the mixture to 50-120 DEG C, adding catalyst into the reaction device, reacting for 5-16h and cooling to
room temperature, filtering, carrying out reduced pressure
distillation on the filtrate, carrying out
evaporation to remove
solvent to obtain brown thick product, placing the product in a
drying oven,
drying for 8h in vacuum at 40-70 DEG C, crushing to obtain
powder product, namely the hexaaniline cyclotriphosphazene. The non-
halogen flame retardant
epoxy resin composition applied to large-scale and very-large-scale integrated circuits encapsulation is prepared by mixing the prepared hexaaniline cyclotriphosphazene with o-
cresol formaldehyde epoxy resin, microsilica, curing catalyst,
silane coupling agent,
lubricant, flexibilizer and
stearic acid, milling, crashing and demagnetizing.