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33results about How to "Stay decentralized" patented technology

Method for preparing modified polyvinyl alcohol copolymer cross-linked ceramic green body reinforcing agent

The invention relates to a modified polyvinyl alcohol copolymer cross-linked ceramic green body reinforcing agent. Vinyl acetate and acrylic acid are subjected to a free-radical polymerization reaction in the presence of an initiator and a chain transfer agent, part of ester bonds of the copolymer are hydrolyzed when an alkali is added for treatment, and then, the acrylic acid and vinyl acetate modified polyvinyl alcohol copolymer ceramic green body reinforcing agent is prepared. The copolymer cross-linked ceramic green body reinforcing agent disclosed by the invention has relatively good dispersity, and the viscosity of slurry cannot be improved by adding the reinforcing agent into a ceramic slurry system; and during the forming of green body slurry, the slurry is completely hydrolyzed into an acrylic acid and vinyl alcohol copolymer under alkaline conditions, and hydroxyl groups of the copolymer are subjected to hydrogen bonding with particles in a green body, so that internal particles of the green body are of a reticular structure, the green strength, dried strength and glazed strength of the green body are greatly improved. The strength of the ceramic green body is greatly improved while the original adhesiveness, dispersity and viscosity reducing property of polyvinyl alcohol are kept, so that the reinforcing agent has a broad application prospect.
Owner:四会市奥耳新材料有限公司

Novel medicinal composition containing amorphous vortioxetine hydrobromide and preparation method of novel medicinal composition

The invention relates to a medicinal composition containing vortioxetine hydrobromide. The medicinal composition contains a solid dispersion (formed by vortioxetine hydrobromide and an organic carrier), at least one adsorbent, and at least one medicinal adjuvant, wherein vortioxetine hydrobromide is amorphous, in the X-ray powder diffraction spectrum of the composition, after the background peak of the organic carrier, the adsorbent and the medicinal adjuvant is deducted, the characteristic peak of crystal of vortioxetine hydrobromide does no exist. The invention further relates to a preparation method of the medicinal composition of the amorphous vortioxetine hydrobromide. The medicinal composition of vortioxetine hydrobromide provided by the invention is good in stability and dispersibility, the dissolution rate of vortioxetine hydrobromide is increased, the bioavailability of the medicinal preparation and the absorption of the body for the medicine can be improved, and under the condition of acceleration test, good physical stability and chemical stability can be kept. The preparation method provided by the invention is easy to operate, low in cost, good in reproducibility, easyto realize, and suitable for industrial production.
Owner:SHANGHAI FANGNAN PHARMA

Formula and preparation method of low-carbon lubricating oil

The invention provides a formula and a preparation method of low-carbon lubricating oil. The formula is characterized by comprising the following components in parts by weight: 5 to 30 parts of synthetic base oil, 35 to 55 parts of III-type hydrogenated base oil, 15 to 22 parts of II-type hydrogenated base oil, 8 to 15 parts of V-type synthetic phenolic ester base oil, 5 to 15 parts of hydrogenated base oil 150BS and the balance of additives. The preparation method comprises the following steps of adding the base oil in parts by weight into blending equipment, raising temperature to 60 DEG C, and uniformly blending the base oil at constant temperature; sequentially adding various additives, raising the temperature to 70 to 75 DEG C (not more than 75 DEG C), stirring the base oil and the additives within 40 minutes at constant temperature to completely mix the base oil and the additives, and performing circulating filtration and cooling in four stages to obtain the low-carbon lubricating oil. The formula and the preparation method thereof have the beneficial effects that the limit of soot content is reduced; the low-carbon lubricating oil is energy-saving, low-phosphorus, environment-friendly, high in abrasion resistance and resistant to high temperature and high load; the high-temperature detergency is greatly improved; the carbon emission of the lubricating oil is effectively reduced.
Owner:TIANJIN LINXAN PETROCHEM

Automatic nutrient solution preparation device and method

The invention belongs to the technical field of medical instruments, and particularly relates to an automatic nutrient solution preparation device and method.The automatic nutrient solution preparation device comprises a device body with an opening in the upper end, a solution preparation cavity formed in the device body and a solution outlet pipe valve located at the lower end of the solution preparation cavity; the annular cover is located at the opening position of the device body, the equipment cover is movably installed in the center of the annular cover, the spiral stirrer is located in the liquid preparation cavity, an umbrella cover is arranged above blades of the spiral stirrer, and a liquid feeding mechanism, a fixed feeding assembly, a fluid pump and a driving device of the spiral stirrer are arranged at the upper end of the equipment cover. The discharging end of the liquid feeding mechanism and the discharging end of the fixed feeding assembly are each provided with a feeding pipe valve. According to the invention, automatic preparation of the nutrient solution is realized, rapid stirring is realized, large-particle solid components are stirred and dissolved rapidly after being ground, the fluid pump is used for feeding, the spiral stirrer and the umbrella cover cooperate with each other, the material mixing speed is high, and the preparation time of the nutrient solution is short.
Owner:THE FIRST AFFILIATED HOSPITAL OF ANHUI MEDICAL UNIV

Method for synthesizing mesoporous titanium dioxide by adding template agent through ultrasonic coupling and microwave

The invention relates to a method for synthesizing mesoporous titanium dioxide by adding a template agent through ultrasonic coupling microwaves. The method is characterized in that the template agentis added, so that the mesoporous size is reduced and the product dispersity is improved under the ultrasonic action. And the dispersity of titanium dioxide is maintained through microwave heating. The prepared particles are small in size and good in dispersity and have an ordered and controllable mesoporous structure, and the photocatalytic performance of the particles is improved. The method comprises the following steps: preparing a 0.045-0.18 g / L NaOH solution, preparing a mixed solution of a certain amount of tetrabutyl titanate, 0.1 g of a template agent and a certain amount of absoluteethyl alcohol, dripping the mixed solution into the NaOH solution under the conditions that the reaction temperature is 20 DEG C-80 DEG C, the ultrasonic power density is 0.077 W / mL-0. 385W / mL, the ultrasonic operation mode is intermittent operation, the operation period is 5-20 seconds of ultrasonic operation and 25-10 seconds of no ultrasonic operation, and the time for the ultrasonic operationis 7-30 minutes; and after dropping, transferring the obtained precursor into a microwave reactor, conducting reacting under the conditions that the microwave power density is 1 W / mL- 2.5 W / mL and themicrowave temperature and time are certain, and obtaining the mesoporous titanium dioxide after the reaction.
Owner:TIANJIN UNIV OF SCI & TECH

Tecarfarin or pharmaceutically acceptable salt or pharmaceutic adjuvant solid dispersion body and preparation method thereof

The invention provides amorphous form Tecarfarin and a pharmaceutically acceptable salt thereof. The amorphous form Tecarfarin is characterized in that in the X-ray powder diffraction spectrum, no characteristic peak of the Tecarfarin or the pharmaceutically acceptable salt of the Tecarfarin exists. According to an amorphous form preparation method of the amorphous form Tecarfarin or the pharmaceutically acceptable salt of the Tecarfarin, and a pharmaceutic adjuvant solid dispersion body and a manufacturing method, the Tecarfarin or the pharmaceutically acceptable salt and the pharmaceutic adjuvant are included, which have the weight ratio of 1:0.1 to 1:100, wherein the Tecarfarin or the pharmaceutically acceptable salt is in the amorphous form; after the background peak of the pharmaceutic adjuvant is deducted from the X-ray powder diffraction spectrum of the solid dispersion body, no Tecarfarin or salt crystal feature peak exists. The Tecarfarin or the pharmaceutically acceptable salt and pharmaceutic adjuvant solid dispersion body has good stability and dispersibility; the Tecarfarin or salt dissolution rate is increased; under the acceleration test conditions, good physical stability and chemical stability can be maintained. The preparation method of the amorphous form solid dispersion body has the advantages that the operation is simple; the cost is low; the reproducibility is good; the realization is easy; the method is suitable for industrial production.
Owner:CHANGZHOU FANGNAN MEDICINE TECH CO LTD

Low-carbon lubricating oil formula and preparation method thereof

The invention provides a formula and a preparation method of low-carbon lubricating oil. The formula is characterized by comprising the following components in parts by weight: 5 to 30 parts of synthetic base oil, 35 to 55 parts of III-type hydrogenated base oil, 15 to 22 parts of II-type hydrogenated base oil, 8 to 15 parts of V-type synthetic phenolic ester base oil, 5 to 15 parts of hydrogenated base oil 150BS and the balance of additives. The preparation method comprises the following steps of adding the base oil in parts by weight into blending equipment, raising temperature to 60 DEG C, and uniformly blending the base oil at constant temperature; sequentially adding various additives, raising the temperature to 70 to 75 DEG C (not more than 75 DEG C), stirring the base oil and the additives within 40 minutes at constant temperature to completely mix the base oil and the additives, and performing circulating filtration and cooling in four stages to obtain the low-carbon lubricating oil. The formula and the preparation method thereof have the beneficial effects that the limit of soot content is reduced; the low-carbon lubricating oil is energy-saving, low-phosphorus, environment-friendly, high in abrasion resistance and resistant to high temperature and high load; the high-temperature detergency is greatly improved; the carbon emission of the lubricating oil is effectively reduced.
Owner:TIANJIN LINXAN PETROCHEM

A preparation method of a modified polyvinyl alcohol copolymer cross-linked ceramic green body reinforcing agent

The invention relates to a modified polyvinyl alcohol copolymer cross-linked ceramic green body reinforcing agent. Vinyl acetate and acrylic acid are subjected to a free-radical polymerization reaction in the presence of an initiator and a chain transfer agent, part of ester bonds of the copolymer are hydrolyzed when an alkali is added for treatment, and then, the acrylic acid and vinyl acetate modified polyvinyl alcohol copolymer ceramic green body reinforcing agent is prepared. The copolymer cross-linked ceramic green body reinforcing agent disclosed by the invention has relatively good dispersity, and the viscosity of slurry cannot be improved by adding the reinforcing agent into a ceramic slurry system; and during the forming of green body slurry, the slurry is completely hydrolyzed into an acrylic acid and vinyl alcohol copolymer under alkaline conditions, and hydroxyl groups of the copolymer are subjected to hydrogen bonding with particles in a green body, so that internal particles of the green body are of a reticular structure, the green strength, dried strength and glazed strength of the green body are greatly improved. The strength of the ceramic green body is greatly improved while the original adhesiveness, dispersity and viscosity reducing property of polyvinyl alcohol are kept, so that the reinforcing agent has a broad application prospect.
Owner:四会市奥耳新材料有限公司
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