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85results about How to "Small and uniform" patented technology

Atomizing electronic cigarette

An electronic cigarette has a power device (1), a sensor (2), an atomizing core component and a liquid storage component (3). The atomizing core component includes an electric heater (5) and a liquid permeating component (6). The electric heater (5) has a through hole (51), the liquid storage component (3) has a channel (31), and the sensor (2) is connected with the through hole (51) and the channel (31) to form an airflow loop by the auxiliary air inlet. The liquid permeating component (6) is directly sleeved on the electric heater (5), so that the cigarette can adequately heat gasified smoke with uniform small drops. The electric heater (5) and the liquid storage component (3) are connected with the through hole (51) and the channel (31), so that the vapor generated by the atomizing process can be cooled.
Owner:FONTEM HLDG 1

Blast furnace slag granulation and waste heat utilization process technology and equipment

The invention provides a process technology for granulating blast-furnace slag and utilizing waste heat. The process technology is characterized by comprising the following steps of: performing primary cooling and triple granulation on high-temperature molten slag from a blast furnace in a slag primary cooling device to form fine granules with diameter of less than 3mm and temperature of about 800-1,000 DEG C; discharging the fine granules through a high-temperature slag discharge valve; entering a slag basket and conveying to the upper part of a slag secondary cooling device; falling to the lower part of the slag secondary cooling device along a plurality of layers of baffle heat exchange components which are arranged in the slag secondary cooling device; and cooling to about 200 DEG C and discharging through a low-temperature slag discharging valve, wherein waste heat of normal pressure steam of 200 DEG C can be recovered by the slag primary cooling device; and waste heat of hot circulating air of over 600 DEG C can be recovered by the slag secondary cooling device. The invention provides equipment for granulating blast-furnace slag and utilizing waste heat. The equipment mainlycomprises the slag primary cooling device, the slag secondary cooling device, a waste heat boiler and the like. The process technology and the equipment have the advantages of good granulation effectof the molten slag, small and uniform size of slag granules, almost zero new water consumption and low environmental pollution.
Owner:北京中冶设备研究设计总院有限公司

Synthesis method for near-infrared fluorescent probe copper nano-cluster and application of synthesis method

The invention discloses a synthesis method for a near-infrared fluorescent probe copper nano-cluster and a detection method for glycoprotein. The near-infrared fluorescent probe copper nano-cluster is synthesized through a one-pot method, aminophenylboronic acid is used for functionally transforming the synthesized copper nano-cluster, and the functionalized copper nano-cluster is obtained. Due to the specific action of boric acid groups on aminophenylboronic acid and cis diol in glycoprotein, the fluorescence intensity of the copper nano-cluster is quenched. A fluorescent probe can detect glycoprotein at high specificity and sensitivity. Glycoprotein widely exists in mucus, plasma, cytoplasm and cell membranes, is tightly related to living organisms, is an important physiological active material, and is tightly related to certain genetic diseases, and therefore important practical significance is provided for detecting glycoprotein.
Owner:TIANJIN NORMAL UNIVERSITY

Rubber tire tread and milling process thereof

The invention discloses a rubber tire tread and a milling process thereof. The rubber tire tread comprises the following components in parts by weight: 70-110 parts of natural rubber, 0-15 parts of styrene-butadiene rubber, 5-20 parts of tread rubber powder, 1.5-2.5 parts of stearic acid, 1-2 parts of sulfur powder, 2-18 parts of white carbon black, 12-15 parts of carbon block, 2-30 parts of aromatic oil, 1-8 parts of zinc oxide, 4-7 parts of an anti-aging agent, 1-4 parts of pine tar, 1-4 parts of an accelerating agent, 0.2-1 part of an anti-reversion agent and 2-5 parts of a binding agent. A three-section milling process is adopted, and the milling process can improve the abrasive resistance, tear resistance and chunking and chipping resistance of the tire tread.
Owner:SHANDONG YONGTAI CHEM GROUP

Chromium-doped red fluorescent powder and preparation method thereof

The invention discloses chromium-doped red fluorescent powder and a preparation method thereof. The fluorescent powder comprises a zinc gallate substrate and an optical active component Cr<3+>, and the chemical formula of the fluorescent powder is ZnGa2O4:xCr<3+>, wherein the x is greater than 0.01 and smaller than 0.6, the excitation peak of the fluorescent powder is 590 nm, and the emission peak of the fluorescent powder is 710 nm. The fluorescent powder is prepared through the following steps: (1) accurately weighing oxides of Zn, Ga and Cr or corresponding salts according to the chemical formula; (2) mixing the raw materials after weighing, and sintering for 1-5 hours at the temperature of 900-1200 DEG C; (3) grinding products obtained after sintering, and enabling the ground products to pass through a mesh sieve, so as to obtain the red fluorescent powder. According to the invention, relatively cheap metallic elements are used for replacing expensive rare-earth elements to prepare the relatively cheap inorganic fluorescent powder; the fluorescent powder can shine in a dark red area that the light wavelength of the common rare earth doped fluorescent powder cannot reach.
Owner:HUIZHOU UNIV

Ternary copolymerized composite material of functional graphene in-situ polymerized polyester and preparation method and special device thereof

The invention discloses a ternary copolymerized composite material of functional graphene in-situ polymerized polyester and a preparation method and a special device thereof and belongs to the technical field of preparation of composite materials. The composite material is prepared from dihydric alcohol, binary acid and functional graphene through esterification and polycondensation reactions, wherein the molar ratio of dihydric alcohol and binary acid is (1.2-2): 1, the functional graphene accounts for 0.01-2% by mass of the ternary copolymerized composite material and the number-average molecular weight of the ternary copolymerized composite material is 10000-150000. By introducing active functional groups to the surface of graphene, graphene is grafted to a polyester chain segment, so that stable covalent bonds are formed between the graphene and the polyester. The polyester molecular chain is enhanced as the graphene material has good physical and mechanical properties, so that thecomposite material shows good mechanical properties and comprehensive performance.
Owner:CHANGZHOU HIGHBERY NEW NANO MATERIALS TECH CO LTD +1

Porous cubic bimetallic phosphide catalyst as well as preparation method and application thereof

The invention relates to a porous cubic bimetallic phosphide catalyst as well as a preparation method and application thereof. The preparation method comprises the following steps: firstly preparing abimetallic Prussian blue precursor, and performing heating calcination on the bimetallic Prussian blue precursor and phosphorus in a tube furnace to dope the phosphorus into the bimetallic Prussian blue analogue. The synthetic method provided by the invention has the advantages of simple operation, low costs and easy mass production in an industrial scale; the catalyst synthesized by the method has a smaller and uniform size, so that the catalyst has a larger specific surface area and rich active sites, and the electro-catalytic property of the catalyst is enhanced; and in addition, the catalyst synthesized by the method has good stability, can be recycled and applied to the fields of energy and environmental protection, and has potential value.
Owner:ANHUI UNIVERSITY

Method for preparing monocrystalline silicon suede

The invention discloses a method for preparing monocrystalline silicon suede, which comprises the following steps of: 1) preparing 0.05 to 0.5 percent rough polishing solution from 45 percent aqueous alkali and deionized water in a thermostat with the temperature of between 75 and 85DEG C; 2) preparing 0.5 to 5 percent analytical pure alkali and 87 to 98.4 percent of deionized water into 45 percent aqueous alkali, and mixing the 45 percent aqueous alkali, 1 to 7 percent analytical pure isopropanol, 0.1 to 1 percent analytical pure sodium silicate and the rest deionized water into alkaline corrosion solution in the thermostat with the temperature of between 75 and 85DEG C; and 3) pre-cleaning a monocrystalline silicon piece for 1 to 6 minutes in the rough polishing solution, taking the monocrystalline silicon piece out, soaking in warm water, reacting for 10 to 30 minutes in the alkaline corrosion solution, taking the monocrystalline silicon piece out, washing with deionized water, anddrying. The prepared monocrystalline silicon suede has small-size and uniform pyramids, the light absorbing capacity of batteries is improved, the suede preparing reaction time is shortened, and the production cost is reduced.
Owner:河北兆能新能源科技有限公司

Large-Size Glass Substrate For Photomask and Making Method, Computer-Readable Recording Medium, and Mother Glass Exposure Method

A large-size glass substrate, from which a photomask substrate is formed, is prepared by processing a large-size glass substrate stock by (1) a flattening removal quantity based on height data of the substrate stock in the vertical attitude plus a deformation-corrective removal quantity. The deformation-corrective removal quantity is calculated from (2) a deflection of the substrate stock by its own weight in the horizontal attitude, (3) a deformation of the photomask substrate caused by chucking in an exposure apparatus, and (4) an accuracy distortion of a platen for supporting a mother glass.
Owner:SHIN ETSU CHEM IND CO LTD

Dust collecting device for digestion water bath of quick lime

The invention relates to a dust collecting device for digestion water bath of quick lime. The dust collecting device comprises a de-dusting pool, a dust collector shell, a de-dusting pipeline, an overflow water seal pool, a buffering water pool, a water level adjusting hole and a water level adjusting device, wherein the dust collector shell is located above the de-dusting pool; one end of the de-dusting pipeline is externally connected with a de-dusting interface of a lime digester while the other end passes through the dust collector shell and extends into the de-dusting pool under the dust collector shell; an underwater pipeline nozzle is arranged at one end of the de-dusting pipeline extending into the de-dusting pool; a net structure or a porous structure is arranged at the tail end of the underwater pipeline nozzle; the overflow water seal pool is located on one side of the de-dusting pool; the buffering water pool is located on the other side of the de-dusting pool; the water level adjusting hole is located between the de-dusting pool and the overflow water seal pool and is formed at the lower end on one side of the dust collector shell; a clamping and releasing slot is formed on the outer side of the shell aside the water level adjusting hole; the water level adjusting device comprises a water level adjusting plate, a screw rod and an adjusting valve; the water level adjusting plate is placed in the clamping and releasing slot; the vertical width of the water level adjusting plate is slightly more than the vertical width of the water level adjusting hole.
Owner:ZHONGYE-CHANGTIAN INT ENG CO LTD

A preparing method of rutile vanadium dioxide nanometer particles and the particles

A preparing method of rutile vanadium dioxide nanometer particles is disclosed. The method includes 1) preheating purified water or deionized water until the water is boiling, adding a vanadium compound, stirring to obtain a vanadium compound suspension A, cooling to room temperature, adding ammonia water, sealing a container, and stirring for 0.5-3 h until a transparent solution B is prepared, 2) adding a hydrazine compound into the transparent solution B, stirring to obtain black suspension C, transferring the suspension C to a hydrothermal reactor, heating and reacting to obtain a black brown suspension D, 3) transferring the black brown suspension D into a transparent container, adding ethanol, allowing the mixture to stand so that the mixture is layered naturally after the solution is stationary, removing the supernatant liquid, adding ethanol again, stirring, allowing the mixture to stand, naturally layering, and removing the supernatant liquid again to obtain wet powder E, and 4) drying and oxidizing the wet powder E in a drying oven, firing in an atmosphere furnace containing a protective atmosphere, and treating to obtain the rutile vanadium dioxide nanometer particles. Raw materials of the method are cheap. The method greatly reduces emission of 'three wastes' or secondary environment pollution.
Owner:刘闽苏

Method for preparing strontium barium niobate ceramics with high pyroelectric effects

The invention discloses a method for preparing strontium barium niobate ceramics with high pyroelectric effects.The method includes mixing raw materials BaCO<3>, SrCO<3> and Nb<2>O<5> according to a chemical formula of Sr<x>Ba<1-x>Nb<2>O<6> to obtain Sr<x>Ba<1-x>Nb<2>O<6> powder; sintering the Sr<x>Ba<1-x>Nb<2>O<6> powder by the aid of a spark plasma sintering system in a vacuum environment at the temperature of 1000-1050 DEG C to prepare ceramic sintered bodies and thermally treating the ceramic sintered bodies in the air at the temperature of 965-980 DEG C for 3 hours to obtain the strontium barium niobate ceramics with the high pyroelectric effects.The x can be equal to 0.4 or 0.5 or 0.6.The method has the advantages that the strontium barium niobate ceramics with the high pyroelectric effects have small crystal grain sizes and are high in density, the dielectric breakdown field strength is improved, accordingly, the strontium barium niobate ceramics hopefully can be used for solid-state refrigerating systems, and various currently confronted climatic environmental problems due to the fact that ozone layers are destructed by Freon which is used as a refrigerants can be solved.
Owner:ZHEJIANG UNIV

Preparation method for rutile phase vanadium dioxide superfine nano powder

The invention discloses a preparation method for rutile phase vanadium dioxide superfine nano powder, which comprises the following steps: S1, enabling ammonium hydroxide to quickly react with an acidic tetravalent vanadium solution to obtain turbid liquid B; S2, performing sealing, heat preservation and stirring treatment on the turbid liquid B to obtain a colloidal suspension C, wherein the temperature for heat preservation is not higher than the boiling point of a solvent in the tetravalent vanadium solution; S3, performing solid-liquid separation and cleaning on the colloidal suspension Cto obtain hydrated vanadium hydroxide colloid D; S4, drying the hydrated vanadium hydroxide colloid D and sintering in the protection atmosphere to obtain the rutile phase vanadium dioxide superfine nano powder. The rutile phase vanadium dioxide particles prepared by the process method disclosed by the invention have the advantages of high purity, smaller and even size and good dispersion and canserve as an excellent raw material for high-quality vanadium dioxide intelligent temperature-control coated windows.
Owner:INST FOR PROCESS MODELING & OPTIMIZATION JITRI

Carbon quantum dots prepared from pyrolysis molecular sieves and application of carbon quantum dots in detection of hydrogen peroxide

The invention provides carbon quantum dots prepared from pyrolysis molecular sieves and application of the carbon quantum dots in detection of hydrogen peroxide, and belongs to the technical field ofcarbon-based nanomaterials. With the aid of the spatial confinement effect of the molecular sieves, the carbon quantum dot materials with ultraviolet light excitation, small size, size uniformity (about 2.5 nm), good stability and photoluminescence properties are obtained through hydrothermal synthesis and aftertreatment, and the carbon quantum dot materials can be applied as a fluorescent probe to detect hydrogen peroxide. The main preparation process includes the following steps that an aluminum source, a magnesium source, phosphoric acid and an organic templating agent are used as raw materials, molecular sieve crystal products are prepared through hydrothermal synthesis, and water-soluble carbon dot products are obtained through pyrolysis, chromatography and the like. The prepared carbon dots show excitation-independent blue fluorescence (the emission peak is about 420 nm) and can achieve high sensitivity response to hydrogen peroxide. The quenching constants and detection limits of the carbon dots are 7.3 x 10(3)M(-1) and 3.16 microM respectively.
Owner:JILIN UNIV

Superparamagnetic nano-particle and preparation method and application thereof

The invention provides a superparamagnetic nano-particle, a preparation method of the superparamagnetic nano-particle and application of the superparamagnetic nano-particle. A ferrous compound and a ferric compound are reacted with an aqueous alkali, a water-soluble citrate compound serves as a modifier, and the ferroferric oxide superparamagnetic nano-particle with the surface wrapped by the water-soluble citrate compound is obtained by a co-precipitation method. A nucleating stage and a growing stage of ferroferric oxide particles are effectively separated, and the superparamagnetic nano-particle which is small and uniform in particle size and good in dispersibility is obtained; the water-soluble citrate compound is used for modifying the surfaces of the ferroferric oxide nano particles, so that the stability and the biocompatibility of the superparamagnetic nano-particle in a human body are improved. A stable dispersion system is formed by dispersing the superparamagnetic nano-particle in an aqueous solution, a superparamagnetic contrast agent is obtained, and the contrast agent can perform magnetic resonance imaging in a pathological tissue of myocardial infarction.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI

Polypropylene-based thermoplastic shielding material for cable, and preparation method thereof

The invention provides a polypropylene-based thermoplastic shielding material for a cable and a preparation method of the shielding material. The shielding material comprises the following componentsin parts by weight: 100 parts of ethylene-propylene block copolymer polypropylene, 3-20 parts of conductive carbon black, 0.5-1.5 parts of high-conductivity graphene, 0.5-1.5 parts of a coupling agentand 1.4-4.5 parts of an auxiliary agent, wherein the auxiliary agent comprises an antioxidant, a lubricant and an anti-bonding agent; and the mass fraction of ethylene fragments in the ethylene-propylene block copolymer polypropylene is 5%-30%. According to the shielding material in the invention, the problem that mechanical properties are reduced due to the fact that high-content conductive carbon black needs to be added for improving the conductivity of a conventional polypropylene-based thermoplastic shielding material for the cable is solved, and the polypropylene-based thermoplastic shielding material for the cable in the invention has excellent conductivity and mechanical properties, and still has excellent conductivity and mechanical properties under a high-temperature condition through cooperation among the ethylene-propylene block copolymer polypropylene, the conductive carbon black and the high-conductivity graphene.
Owner:ELECTRIC POWER RESEARCH INSTITUTE, CHINA SOUTHERN POWER GRID CO LTD +1

Recycling of large-size photomask substrate

A used large-size photomask substrate having a patterned light-shielding film is recycled by (i) removing the light-shielding film from the used substrate to provide a photomask-forming glass substrate stock, (ii) resurfacing the glass substrate stock by sand blasting, (iii) repolishing the resurfaced glass substrate stock to yield a regenerated glass substrate stock, (iv) applying a light-shielding film onto the regenerated glass substrate stock to yield a regenerated photomask-forming blank, and (v) processing the light-shielding film of the blank into a pattern corresponding to the desired exposure of a mother glass, yielding a regenerated photomask substrate.
Owner:SHIN ETSU CHEM IND CO LTD

Preparation method of GSH@AgNCs/MgAl-ELDH modified electrode

The invention discloses a preparation method of a GSH@AgNCs / MgAl-ELDH modified electrode. The method comprises the following specific steps: S1, preparing glutathione-coated silver nano-cluster GSH@AgNCs: preparing a GSH@AgNCs sample by taking glutathione as a stabilizer and sodium borohydride as a reducing agent and adopting a chemical reduction method; s2, preparing a magnesium-aluminum hydrotalcite material: preparing magnesium-aluminum hydrotalcite MgAl-LDH and a magnesium-aluminum hydrotalcite nanosheet MgAl-ELDH by adopting a coprecipitation and formamide stripping method; s3, preparingGSH@AgNCs / MgAl-LDH, and GSH@AgNCs / MgAl-ELDH; and S4, preparing the GSH@AgNCs / MgAl-ELDH modified electrode. The invention discloses a preparation method of a GSH@AgNCs / MgAl-ELDH modified material, a modified electrode is prepared, the electrochemical activity of the electrode is improved, and simultaneous determination of pesticides carbaryl and isoprocarb by the GSH@AgNCs / MgAl-ELDH modified electrode is realized.
Owner:QINGDAO UNIV OF SCI & TECH

Fuel cell operation technology for improving regeneration rate and electricity generating efficiency of complex iron in desulfuration process

InactiveCN104766981ASimple processControl conversionCell electrodesPlatinumElectricity
The invention discloses a fuel cell operation technology for improving the regeneration rate and electricity generating efficiency of complex iron in the desulfuration process. An air electrode using a single-chamber proton exchange membrane fuel cell as a reactor and using a platinum carbon catalyst serves as a cathode, a carbon material serves as an anode, a desulfurized complex iron solution is added, and a NaOH solution is used for regulating a pH value to be 9-12 under the nitrogen condition so as to seal the cell. The cathode and anode of the cell are connected through a lead, a resistor is connected to the middle and used for measuring voltages at two ends of the resistor, and when the voltages are reduced to be zero, a circuit is disconnected, and an in-situ loaded Fe (III) compound catalyst is obtained from the cathode of the cell. The solution in the cell is replaced by a new desulfurized complex iron solution, the circuit is connected, and the Fe (III) compound catalyst loaded on the cathode enables the coulombic efficiency of the cell and the regeneration rate of Fe (III) in the solution to be remarkably improved.
Owner:HEFEI UNIV OF TECH

Method for one-step synthesis of metal oxide loaded transition metal carbide

The invention provides a method for one-step synthesis of a metal oxide loaded transition metal carbide. The method comprises following steps: preparing a saturated strong alkali solution; then addinga raw material MAX phase and a metal precursor; carrying out one-step preparation of the metal oxide loaded transition metal carbide by utilizing the reactivity of the saturated strong alkali solution to the MAX phase and pyrolysis of the metal precursor at high temperature, and on the basis, selectively adding hydrazine hydrate to regulate and control the valence state of the formed transition metal oxide metal; and uniformly stirring an obtained system, heating to 280-350 DEG C, keeping the temperature for 6-10 hours, cooling, centrifugally collecting a black solid; washing, and drying to obtain a finished product. The method is easy to operate, reaction parameters are easy to control, the metal content is controllable, the method can be used for large-scale industrial production, and the obtained metal oxide / MXenes composite material has good hydrophilicity and a large specific surface area, can be subjected to magnetic separation and has outstanding technical advantages.
Owner:NANCHANG UNIV

Nano-hollow sphere structured amorphous zinc oxide and method for producing the same

The invention discloses amorphous zinc oxide with a nanometer hollow sphere structure and a preparation method thereof, which is characterized in that the preparation method comprises the following steps: slowly heating the temperature to 240 to 280 DEG C under the protection of inert atmosphere after zinc stearate of 126.466 milligram is uniformly mixed with hexadecylamine of 2.0 plus or minus 0.5 gram, 1, 2- hexadecane diol of 143.6 plus or minus 30 milligram and trioctylphousphine oxide of 2.0 plus or minus 0.5 gram according to the blending ratio; and obtaining the amorphous zinc oxide with the nanometer hollow sphere structure which has the diameter of 10 to 23 nm when heat preservation is conducted under the action of an active oxygen source, wherein the thickness of the spherical shell of a hollow sphere is 1 to 5 nm and the diameter of a hollow cavity in the hollow sphere is 8 to 13 mm. The amorphous zinc oxide with the nanometer hollow sphere structure prepared by adopting the method has the advantages of small and uniform dimension, large specific area and good dispersivity, and has wide application prospect in the field of drug release, catalytic reaction and micro-reactors and the like.
Owner:UNIV OF SCI & TECH OF CHINA

Preparation method of lithium ion battery negative electrode material

The invention discloses a preparation method of a lithium ion battery negative electrode material. The preparation method comprises the following steps of growing a nanometer silicon sphere on a surface of graphene; forming a graphene / nanometer silicon composite material; performing sugar coating on the graphene / nanometer silicon composite material; and carbonizing the graphene / nanometer silicon composite material subjected to sugar coating to form a carbon / graphene / nanometer silicon composite material. The preparation method is simple and high in production yield, the nanometer silicon sphereis small and uniform in size, the volume expansion of silicon caused by lithium intercalation and de-intercalation during the charge-discharging process can be effectively reduced by combining the nanometer silicon sphere and the graphene, the internal stress of an electrode is reduced, and the silicon sphere is prevented from being excessively expanded and damaged.
Owner:XIFENG 2D FUJIAN MATERIAL TECH CO LTD

Light silicon dioxide aerogel with ultrahigh transparency and ultralow haze as well as preparation method and application of light silicon dioxide aerogel

The invention relates to light silicon dioxide aerogel with ultrahigh transparency and ultralow haze as well as a preparation method and application of the light silicon dioxide aerogel. The method comprises the steps of preparing a microreactor; preparing ultra-small silica sol in the microreactor by adjusting the flow velocity of a silicon source precursor, fluorocarbon oil and a catalyst phase and the pipeline reaction temperature; quickly stirring a mixture containing silica sol liquid drops and an oil dispersion phase, standing for layering, quickly freezing, and separating out a silica sol phase; and adding a gel accelerator into the silica sol to obtain wet gel, and carrying out aging, solvent replacement and supercritical drying to obtain the light silica aerogel with ultrahigh transparency and ultralow haze. The nano-particle size of the prepared material is adjustable in a range of 5-10 nm, the highest light transmittance can reach 94.2%, the lowest haze can reach 4.7%, and the light silicon dioxide aerogel shows ultrahigh transparent quality and is widely applied to the fields of transparent heat insulation building glass, solar heat collection systems, Cherenkov detectors, deep space high-speed particle capture and the like.
Owner:AEROSPACE INST OF ADVANCED MATERIALS & PROCESSING TECH

Preparation method of CoAl-LDH/PANI modified electrode

The invention discloses a preparation method of a CoAl-LDH / PANI modified electrode. The method comprises the following specific steps of S1, preparing hydrotalcite-like LDH: preparing a mixed salt microemulsion A and an alkali microemulsion B by taking hydrophobic ionic liquids BmimPF6 and TX-100 and a water microemulsion system as media, and preparing three CoAl-LDH samples by adopting a double-microemulsion coprecipitation method according to different water contents in the microemulsions, S2, preparation of polyaniline PANI: preparing the PANI by adopting a double-microemulsion method, S3,preparation of CoAl-LDH / PANI, and S4, preparation of the CoAl-LDH / PANI modified electrode. The invention discloses a preparation method of a CoAl-LDH / PANI modified electrode, preparation of the modified electrode is carried out, the electrochemical activity of the electrode is improved, and simultaneous determination of pesticides carbaryl and isoprocarb by the CoAl-LDH / PANI modified electrode isrealized.
Owner:青岛鸿硅高沃新材料科技有限公司

Preparation method of nickel-iron-copper-molybdenum alloy target material

ActiveCN113265627AGrain size growthSmall and uniform grain sizeVacuum evaporation coatingSputtering coatingIngotCopper
The invention discloses a preparation method of a nickel-iron-copper-molybdenum alloy target material. The preparation method of the nickel-iron-copper-molybdenum alloy target material comprises the following steps that (1) raw materials Mo and raw materials Ni are added into a smelting furnace, suspension smelting is carried out in a vacuum environment, and an alloy ingot A is obtained after cooling; (2) raw materials Fe and raw materials Cu are added into the smelting furnace containing the alloy ingot A in the step (1), smelting treatment continues to be conducted in the vacuum environment, and an alloy ingot B is obtained after cooling; (3) the alloy ingot B is refined for three times in the vacuum environment, and the melt of the alloy ingot B is cast after the third refining to obtain a cast ingot; and (4) the cast ingot obtained in the step (3) is rolled, and the nickel-iron-copper-molybdenum alloy target material is obtained. According to the preparation method, a nickel-molybdenum alloy is firstly smelted, then the raw materials Fe and Cu are added to be smelted again, and then three times of homogenizing refining are combined, so that the uniformity of components of the nickel-iron-copper-molybdenum alloy target material is guaranteed to a large extent, and the target material has the performance of high resistivity, high relative density and high magnetic permeability.
Owner:XIANDAO THIN FILM MATERIALS GUANGDONG CO LTD

Method for preparing gamma-Fe2O3 magnetic nano-particles

The invention discloses a method for preparing gamma-Fe2O3 magnetic nano-particles. The method comprises the steps that Fe3+ salt is directly dissolved in dimethylformamide (DMF), the amount of the Fe3+ salt does not exceed the amount of saturated solubility thereof in the DMF, the mixture is evenly stirred into a transparent solution, and then the solution is sintered for 1-4 hours at the temperature of 150-280 DEG C, so that gamma-Fe2O3 magnetic nano-particles are obtained. The method for preparing gamma-Fe2O3 magnetic nano-particles overcomes the defects of tedious process, complex post processing and the like in the prior art, the pH value does not need to be adjusted in the whole preparation process, washing and filter are not needed, no assistant agent or surface active agent is needed, and the method has the advantages of being high in production rate, high in yield and benefit, and capable of achieving large-batch industrial production.
Owner:LANZHOU UNIVERSITY

Method for synthesizing chain-globular nano platinum in self-assembly manner by using bacitracin as template

The invention discloses a method for synthesizing chain-globular nano platinum in a self-assembly manner by using bacitracin as a template. The method for synthesizing the chain-globular nano platinum in the self-assembly manner by using the bacitracin as the template mainly comprises the following steps of adding the bacitracin into a hydrochloric acid solution, so as to prepare an obtained first mixture into an acidic bacitracin solution of which the concentration is 0.4mM to 0.6mM, and processing the acidic bacitracin solution in a metal bath for 40min to 60min at 50 DEG C to 70 DEG C; adding a platinum tetrachloride solution of which the concentration is 4mM to 5mM into the bacitracin solution, putting an obtained second mixture into a double-layer gas bath oscillator, and incubating the obtained second mixture for 16h to 22h at a rotary speed of 100rpm to 120rpm and at a temperature of 22 DEG C to 24 DEG C; adding sodium borohydride of which the concentration is 4mM to 6mM into the obtained second mixture, and controlling a dripping speed, wherein a total addition amount is 60[mu]L to 90 [mu]L, a reaction temperature is 23 DEG C to 25 DEG C, and the reaction time is 10min to 20min, so as to prepare the chain-globular nano platinum of which the particle size is 15nm to 30nm. The method for synthesizing the chain-globular nano platinum in the self-assembly manner by using the bacitracin as the template is green and environmentally friendly, and is low in cost, simple in process and easy to operate; the prepared chain-globular nano platinum is good in dispersity, uniform in appearance and high in metal loading rate; the defects that platinum nano particles prepared under a conventional chemical process condition easily coagulate and pollute the environment are overcome.
Owner:YANSHAN UNIV

Impinging-stream-based continuous magnesium hydroxide production process

The invention discloses an impinging-stream-based continuous magnesium hydroxide production process, and relates to a magnesium hydroxide production process. The process comprises the steps that a magnesium salt and precipitant with certain concentration serve as raw materials, an impinging stream reactor is adopted, in the impinging stream reactor, the magnesium salt and the precipitant react at20-90 DEG C, magnesium hydroxide precipitates are generated, the obtained precipitates are aged at 50-120 DEG C for 1-10 hours, then filtering and drying are conducted, and a magnesium hydroxide product is finally obtained. Auxiliary equipment of the process comprises a raw material storage tank, a pump, a flowmeter, a filter, an ageing tank, a dryer and the like. Accordingly, the impinging streamreactor is adopted, the magnesium salt and the precipitant serve as the raw materials, and the magnesium hydroxide product which is high in dispersion, small in specific surface area, uniform in particle size and consistent in crystal form can be obtained. By means of the continuous magnesium hydroxide production process, the materials are mixed rapidly, the reaction is efficient, and residence time distribution is narrow. The process flow is short, the equipment is less, and the product quality is good and stable.
Owner:SHENYANG INSTITUTE OF CHEMICAL TECHNOLOGY
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