The invention discloses an Al-Zn-In sacrificial
anode coating metallographic
analysis method, and relates to the technical field of metallographic detection of aluminum sacrificial anodes.The method comprises the four core steps of mechanical coarse
grinding, mechanical fine
grinding, electrolytic
polishing and
anode coating, firstly, an Al-Zn-In sacrificial
anode is prepared, then, a sample is
cut from the Al-Zn-In sacrificial anode, and then the Al-Zn-In sacrificial anode is obtained; the method comprises the following steps: carrying out mechanical coarse
grinding and mechanical fine grinding on a sample, carrying out electrolytic
polishing by adopting an
electrolyte mixed by
perchloric acid and absolute ethyl
alcohol, connecting the sample subjected to electrolytic
polishing with a direct-current power supply anode, connecting a stainless steel sheet with a
cathode, putting into a
film coating solution for
film coating, cleaning to obtain a film-coated sample, and finally carrying out metallographic analysis on the film-coated sample. According to the method, the problems of blurred
grain boundary,
grain boundary covering, residual scratches, unclear second phase and the like in traditional metallographic analysis are solved, the
grain boundary is completely displayed, the grain contour is clear and distinguishable, the contrast is high, false image interference is avoided, and the
structure analysis requirement is met.