A kind of spandex composite fiber and preparation method thereof
A composite fiber and spandex fiber technology, which is applied in fiber processing, fiber type, textiles and papermaking, etc., can solve the problems of vulnerable parts, high strength, easy winding, etc., and achieve the effect of simple process, low cost and good hand feeling
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Embodiment 1
[0025] A kind of preparation method of spandex composite fiber, described preparation method comprises the following steps:
[0026] a) Surface treatment is carried out on the main raw material, the spandex fiber is washed twice with acetone, dried, and then the cleaned spandex fiber is placed in a vacuum dryer under a nitrogen atmosphere, and then dichloromethane and diphenylene are injected at 50°C The mixed steam of methyl methane diisocyanate, the reaction time is 10 hours, the mixed quality of dichloromethane and isocyanate is 50 times that of spandex fiber, and the mass ratio of dichloromethane to isocyanate is 1:3; After the reaction is completed, wash with toluene for 2 times Rinse with ethanol solution, vacuum dry for later use; then put into N-methylpyrrolidone solution containing carbon nanotubes, the mass fraction of carbon nanotubes in the N-methylpyrrolidone solution is 5%, ultrasonic vibration 18 hours, take out and vacuum dry, obtain the spandex fiber after the...
Embodiment 2
[0029] A kind of preparation method of spandex composite fiber, described preparation method comprises the following steps:
[0030] a) Surface treatment of the main raw material, cleaning the spandex fiber with acetone 3 times, drying, and then placing the cleaned spandex fiber in a vacuum dryer under a nitrogen protection atmosphere, and then passing dichloromethane and 2 at 55°C, The mixed steam of 4-toluene diisocyanate, reaction time 11 hours, the mixing quality of dichloromethane and 2,4-toluene diisocyanate is 85 times of spandex fiber, the mass ratio of dichloromethane and 2,4-toluene diisocyanate is 1:4; After the reaction is completed, wash with toluene for 3 times, rinse with ethanol solution, and vacuum dry for later use; then put it into the N-methylpyrrolidone solution containing carbon nanotubes, and the N-methylpyrrolidone solution The mass fraction of carbon nanotubes in the medium is 6%, ultrasonic vibration is performed for 20 hours, and vacuum drying is tak...
Embodiment 3
[0033] A kind of preparation method of spandex composite fiber, described preparation method comprises the following steps:
[0034] a) Surface treatment of the main raw material, cleaning the spandex fiber with acetone 4 times, drying, and then placing the cleaned spandex fiber in a vacuum dryer under a nitrogen protection atmosphere, and then passing dichloromethane and 2 at 65°C, The mixed vapor of 4-toluene diisocyanate, reaction time 12 hours, the mixing quality of dichloromethane and 2,4-toluene diisocyanate is 120 times of spandex fiber, and the mass ratio of dichloromethane and 2,4-toluene diisocyanate is 1:6; After the reaction is completed, wash with toluene for 4 times, rinse with ethanol solution, and vacuum dry for later use; then put it into the N-methylpyrrolidone solution containing carbon nanotubes, and the N-methylpyrrolidone solution The mass fraction of carbon nanotubes in the medium is 7%, ultrasonic vibration is performed for 24 hours, and vacuum drying i...
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