Method for detecting mixing uniformity of soil heavy metal pollution samples

A technology for mixing uniformity and detection method, applied in the measurement of color/spectral characteristics, etc., can solve the problems of uniformity not meeting experimental requirements, low precision, errors, etc., to achieve rich raw materials, improve accuracy, and achieve accurate detection Effect

Inactive Publication Date: 2015-11-18
ZHEJIANG UNIV
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  • Abstract
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  • Application Information

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Problems solved by technology

At present, in the research on the detection of heavy metal content in soil, the samples are often directly tested by various means and conditions after being stirred by agitator or mixer during processing. The processing is simple, the accuracy is not high, and the uniformity is often not up to the experiment. Requirements, large or small errors will be brought to follow-up experiments, so it is difficult to meet the sample needs of today's high-tech means
[0004] The methyl violet tracer technology is mostly used in the field of feed mixing, and there are few domestic methods that use the methyl violet tracer technology to detect the uniformity of soil heavy metal contaminated samples.

Method used

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  • Method for detecting mixing uniformity of soil heavy metal pollution samples
  • Method for detecting mixing uniformity of soil heavy metal pollution samples
  • Method for detecting mixing uniformity of soil heavy metal pollution samples

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Experimental program
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Embodiment 1

[0029] 1. Using methyl violet as a tracer to test its own stability and interference with sample components

[0030] (1) Full-wavelength scanning of methyl violet

[0031] Dissolve 0.1 g (accurate to 0.001 g) of methyl violet solid in 1 L of absolute ethanol to prepare a 100 mg / L solution; absorb 200 μL of the solution, and use a microplate reader to perform full-wavelength scanning at 400-700 nm. Determine the best absorption wavelength of methyl violet is 579nm.

[0032] (2) Full-wavelength scanning of sample components

[0033] Take 10g of the soil and the heavy metal ion raw material as the total amount, and weigh the heavy metal ion according to the formula weight ratio: soil=1:1000 (respectively accurate to 0.001g), dissolve with absolute ethanol and set the volume to 100mL, 9000r / min Centrifuge for 5 minutes, filter the supernatant, draw 200 μL of the sample solution, and use a microplate reader to scan at a full wavelength of 400-700 nm.

[0034] (3) Detection of th...

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Abstract

The invention provides a method for detecting mixing uniformity of soil heavy metal pollution samples. The method comprises steps as follows: (1), methyl violet powder is mixed with a plurality of to-be-detected soil heavy metal pollution samples; (2), the mixed powder at different sites is selected and sampled at random; (3), the mixed powder at different sites is dissolved with ethyl alcohol respectively and prepared to form solutions; (4), light absorption values of the solutions at the level of 579 nm are measured respectively; (5), CV (coefficients of variation) of distribution of methyl violet in the mixed powder at different sites are calculated. According to the detection method, the mixing uniformity of the soil heavy metal pollution samples is reflected by comparing differences of distribution of methyl violet in the mixed powder samples at different sites, mixing uniformity of heavy metal ions in soil is accurately detected, the detection accuracy of the content of heavy metals in soil is improved later, and further treatment of pollution of heavy metals in soil is facilitated.

Description

technical field [0001] The invention relates to the research field of soil heavy metal pollution detection and comprehensive prevention and control, in particular to a detection method for mixing uniformity of soil heavy metal pollution samples. Background technique [0002] Heavy metals from pesticides, wastewater, sludge, and atmospheric deposition mainly include elements with significant biological toxicity such as mercury (Hg), cadmium (Cd), lead (Pb), chromium (Cr) and metalloid arsenic (As), as well as some Toxic zinc (Zn), copper (Cu), nickel (Ni) and other elements are gradually polluting the soil that is closely related to our lives. Excessive heavy metals can cause plant physiological dysfunction, nutritional imbalance, and affect plant roots and leaves. development; heavy metal pollutants have little mobility in the soil, are not easy to leach with water, and are not degraded by microorganisms. After entering the human body through the food chain, they will damage...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/31
Inventor 刘飞周莉萍何勇彭继宇冯雷方慧
Owner ZHEJIANG UNIV
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