A light-absorbing and heat-storing far-infrared fiber, its preparation method and application
A far-infrared fiber and far-infrared technology, applied in the field of textile fabrics, can solve the problems that the thermal insulation performance cannot meet the general requirements, the fiber fabric with a single thermal insulation effect, and the thermal insulation effect is not obvious, etc., and achieve good light absorption and heat storage performance, good warmth and comfort , the effect of good far-infrared heat storage performance
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[0030] In the present invention, the preparation method of the compound microparticles may include the following steps:
[0031] The light-absorbing and heat-storing particles, the far-infrared particles, the silane coupling agent and the solvent are mixed under the condition of stirring, and then filtered, dried and ground in sequence to obtain compound particles.
[0032] In the embodiment of the present invention, light-absorbing heat-storage particles and far-infrared particles are mixed uniformly according to a certain ratio, and then the mixed particles and silane coupling agent are added into a container, and then solvent is added, and stirred at a certain temperature for a period of time. In the embodiment of the present invention, the light-absorbing and heat-storage particles, the far-infrared particles and the solvent can also be mixed first, usually after stirring for 10 minutes to 15 minutes, and then the obtained composite particle suspension is stirred and mixed ...
Embodiment 1
[0061] Add nano-titanium carbide and nano-titanium dioxide into water, and stir evenly for 10 minutes to obtain a composite particle suspension; then add 3-aminopropyltriethoxysilane to the composite particle suspension, and stir evenly at 70°C for 80 minutes Wherein, the mass ratio of nano-titanium carbide and nano-titanium dioxide is 7:3, the ratio of the mass sum of particles in the suspension to the mass of 3-aminopropyltriethoxysilane is 80:1, and the particle diameter of nano-titanium carbide is 5nm ~20nm, the particle size of nano-titanium dioxide is 5nm~15nm.
[0062] Then, the composite microparticle sample modified by 3-aminopropyltriethoxysilane is obtained by filtration, and then dried and fully ground in sequence to obtain the composite microparticle with a particle diameter of 5nm-25nm.
[0063] Finally, the composite particles are added to PET melt spinning liquid at 225°C-235°C, and then through the melt spinning process, the light-absorbing and heat-storing fa...
Embodiment 2
[0065] Add nano-antimony oxide and nano-titanium nitride into water, and stir evenly for 10 minutes to obtain a composite particle suspension; then add 3-aminopropyltriethoxysilane to the composite particle suspension, and evenly mix at 65°C Stir for 80 minutes; wherein, the mass ratio of nano antimony oxide to nano titanium nitride is 6:4, the mass ratio of the sum of particles in the suspension to the mass of 3-aminopropyltriethoxysilane is 75:1, and the nano antimony oxide The particle size of nano-titanium oxide is 5nm-20nm, and the particle size of nano-titanium oxide is 5nm-15nm.
[0066] Then, the composite microparticle sample modified by 3-aminopropyltriethoxysilane is obtained by filtration, and then dried and fully ground in sequence to obtain the composite microparticle with a particle diameter of 5nm-25nm.
[0067] Finally, the compound particles are added to the PP melt spinning solution at 250°C-270°C, and the light-absorbing and heat-storing far-infrared polyprop...
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