A branched viscoelastic powder oil displacement agent and its preparation method
A powdery, oil-displacing agent technology, applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problems of low recovery rate of oil-displacement, low volume of oil-displacing agent, etc., and achieve stable product performance and Excellent, small amount of initiator, easy to control the effect
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Embodiment 1
[0022] a. Dissolve 100g of acrylamide in 200g of water to prepare an aqueous solution of acrylamide;
[0023] b. First, put the acrylamide aqueous solution in step a into a three-neck container, put nitrogen in a water bath at 15°C for 15 minutes, and then put the persulfide aqueous solution prepared according to the ratio of potassium persulfate: water = 0.04g: 40g Add the pentaerythritol aqueous solution prepared according to the ratio of pentaerythritol: water = 0.004g: 40g into the three-neck container for reaction. After the temperature rise of the reaction solution exceeds 1°C, stop the nitrogen flow and start recording the temperature of the reaction system;
[0024] c. When the temperature of the reaction system does not rise any more, put the three-necked container into an 85°C water bath and keep it warm for 4 hours, then take out the gel, cut it into pieces, dry it, and pulverize it to obtain a viscoelastic powder oil displacing agent product. After screening, the p...
Embodiment 2
[0026] a. Dissolve 100g of acrylamide in 250g of water to prepare an aqueous solution of acrylamide;
[0027] b. First, put the acrylamide aqueous solution in step a into a three-neck container, put nitrogen in a water bath at 10°C for 30 minutes, and then add the persulfide aqueous solution prepared according to the ratio of potassium persulfate: water = 0.04g: 40g Add the pentaerythritol aqueous solution prepared according to the ratio of pentaerythritol: water = 0.004g: 40g into the three-neck container for reaction. After the temperature rise of the reaction solution exceeds 1°C, stop the nitrogen flow and start recording the temperature of the reaction system;
[0028] c. When the temperature of the reaction system no longer rises, put the three-necked container in a 70°C water bath and keep it warm for 6 hours, then take out the gel, cut it into pieces, dry it, and pulverize it to obtain a viscoelastic powder oil displacing agent product. After screening, the product of ...
Embodiment 3
[0030] a. Dissolve 100g of acrylamide in 220g of water to prepare an aqueous solution of acrylamide;
[0031] b. First, put the acrylamide aqueous solution in step a into a three-neck container, put nitrogen in a water bath at 12°C for 20 minutes, and then add the persulfide aqueous solution prepared according to the ratio of potassium persulfate: water = 0.025g: 60g Add the pentaerythritol aqueous solution prepared according to the ratio of pentaerythritol: water = 0.0030g: 50g into the three-necked container for reaction. After the temperature rise of the reaction solution exceeds 1°C, stop the nitrogen flow and start recording the temperature of the reaction system;
[0032] c. When the temperature of the reaction system no longer rises, put the three-neck container in a 78°C water bath and keep it warm for 5 hours, then take out the gel, cut it into pieces, dry it, and pulverize it to obtain a viscoelastic powder oil displacing agent product. After screening, the product o...
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