Mint-extract, menthol and cool-feeling-substance combined modification additive and application thereof
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Embodiment 1
[0037] The peppermint extract menthol cooling substance composite modification additive of this embodiment is a peppermint extract-menthol-jade composite modifier, and its preparation method includes the following steps:
[0038] Step 1: Preparation of Menthol Microcapsule Slurry
[0039] Add the emulsifier sodium dodecyl sulfate (SDS) into distilled water, stir well at room temperature until completely dissolved to form an emulsifier solution, and the mass ratio of emulsifier to distilled water is 1:3;
[0040]Weigh acrylonitrile monomer and menthol into the above emulsifier solution, emulsify and disperse at high speed for 15 minutes to obtain a mixed emulsified solution of menthol and acrylonitrile; wherein the weight ratio of menthol to acrylonitrile monomer is 1.0:3.5 , the consumption of emulsifier SDS is 2.0% of the total weight of menthol and acrylonitrile monomer;
[0041] Heat and stir the mixed emulsified solution in a water bath at 55°C, and at the same time add d...
Embodiment 2
[0053] The composite modified additive of peppermint extract menthol cooling sensation substance in this embodiment is a composite modifier of peppermint extract-menthol-silicate, and its preparation method comprises the following steps:
[0054] Step 1: Preparation of Menthol Microcapsule Slurry
[0055] Add the emulsifier sodium dodecyl sulfate (SDS) into distilled water, stir well at room temperature until it is completely dissolved to form an emulsifier solution, and the mass ratio of emulsifier to distilled water is 1:3;
[0056] Weigh acrylonitrile monomer and menthol into the above emulsifier solution, emulsify and disperse at high speed for 19 minutes to obtain a mixed emulsified solution of menthol and acrylonitrile; wherein the weight ratio of menthol to acrylonitrile monomer is 1.0:3.1 , the consumption of emulsifier SDS is 2.9% of the total weight of menthol and acrylonitrile monomer;
[0057] Heat and stir the mixed emulsified solution in a water bath at 61°C, an...
Embodiment 3
[0069] The composite modified additive of peppermint extract menthol cooling sensation substance in this embodiment is a composite modifier of peppermint extract-menthol-silicate, and its preparation method comprises the following steps:
[0070] Step 1: Preparation of Menthol Microcapsule Slurry
[0071] Add the emulsifier sodium dodecyl sulfate (SDS) into distilled water, stir well at room temperature until it is completely dissolved to form an emulsifier solution, and the mass ratio of emulsifier to distilled water is 1:3;
[0072] Weigh acrylonitrile monomer and menthol into the above emulsifier solution, emulsify and disperse at high speed for 22 minutes to obtain a mixed emulsified solution of menthol and acrylonitrile; wherein the weight ratio of menthol to acrylonitrile monomer is 1.0:2.7 , the consumption of emulsifier SDS is 3.6% of the total weight of menthol and acrylonitrile monomer;
[0073] Heat and stir the mixed emulsified solution in a water bath at 66°C, an...
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