Influenza vaccine immunization preparation for nasal administration and preparation method thereof
A technology for influenza vaccines and immune preparations, which is applied in the field of human influenza vaccine preparations and its preparation, and can solve the problems that the nasal immunization preparations of influenza vaccines have not yet seen clinical application.
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Embodiment 1
[0041] prescription:
[0042]
[0043] The immune enhancer is dodecyl / tetradecyl-glucoside, the pH regulator is phosphate buffer saline (0.01mM, pH=7.2); the osmotic pressure regulator is sodium chloride.
[0044] Preparation:
[0045] Adding the alkyl glycoside to the phosphate buffer solution to dissolve to obtain an alkyl glycoside solution;
[0046] The inactivated influenza vaccine is mixed with the alkyl glycoside solution, and other components are added to obtain the nasally administered influenza vaccine immune preparation. Store at 2-8°C.
Embodiment 2
[0048] prescription:
[0049]
[0050] Described immunopotentiator is chitosan (500,000 molecular weight, deacetylation degree 90%);
[0051] Described pH adjusting agent is glacial acetic acid-sodium acetate buffer solution (pH4.5)
[0052] Preparation:
[0053] Chitosan and glacial acetic acid-sodium acetate buffer solution (pH4.5) are mixed and dissolved, and then inactivated influenza vaccine is added to obtain the influenza vaccine immune preparation for nasal administration;
[0054] Then add 50 g of mannitol, and freeze-dry at -40° C. to obtain an immune freeze-dried preparation of influenza vaccine for nasal administration.
Embodiment 3
[0056] prescription:
[0057] Calculated as HA, inactivated influenza vaccine 75mg for each subtype
[0058] Low Acyl Gellan Gum 5g
[0059] water 1000mL
[0060] The immune enhancer is low acyl gellan gum;
[0061] Preparation:
[0062] The low acyl gellan gum is added to water, stirred and dissolved at 80-100° C., allowed to cool, and then mixed with the inactivated influenza vaccine to obtain the nasally administered influenza vaccine immune preparation.
PUM
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