High-performance silicon-based thermal-conducting gel and preparation method thereof
A high-performance, silicone gel technology, applied in the field of thermal interface silicone thermal conductive materials, can solve the problems of reduced production efficiency and use efficiency of thermally conductive silicon gaskets, reduced thermal conductivity, and precipitation of silicone oil, to avoid high contact resistance, easy to use. The effect of low filling and volatilization weight loss
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[0043] A preparation method of silicon-based thermally conductive gel is: comprising the following steps:
[0044] (i) Thermally conductive powder drying
[0045] Bake the thermally conductive powder at 150°C for 20-40 hours to remove moisture;
[0046] (ii) The particle size of the thermally conductive powder is extremely matched
[0047] The particle size of the heat-conducting powder is perfectly matched, and the heat-conducting powder with three particle sizes of large, medium and small is selected according to the weight ratio of 5:3:1 for pre-mixing;
[0048] (iii) mix
[0049] Mix the thermally conductive powder obtained in step (ii) with silicone gel, hydrogen-containing silicone oil and hydroxyl silicone oil in a double planetary mixer for 20 to 30 minutes;
[0050] (iv) Vulcanization
[0051] The mixture obtained in step (iii) was baked at 120°C for 24 hours to fully cross-link, and then cooled to obtain a high-performance silicon-based thermally conductive gel. ...
Embodiment 1~3
[0053] (1) Raw material preparation
[0054] a. Silicone gel (two-component A and B, mixed in a ratio of 1:1.)
[0055] b. Methyl hydrogen silicone oil
[0056] c. Hydroxy silicone oil
[0057] d. Thermal powder
[0058] Among them: d1 aluminum powder (average particle size 3μm)
[0059] d2 alumina powder (average particle size 55μm)
[0060] d3 boron nitride powder (average particle size 25μm)
[0061] After the above-mentioned heat-conducting powder is dried, it is matched according to the ratio shown in Table 1.
[0062] (2) Put the above-mentioned components in proportion (see Table 1 for specific components and their proportions) into a double planetary mixer for mixing to obtain a silicon-based thermally conductive gel.
[0063] The composition of Examples 1-3 silicon-based thermally conductive gel is shown in Table 1 below:
[0064] Table 1
[0065]
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