Preparation method of interface heat conduction material silicone rubber pad

An interface thermal conductive material and silicone rubber technology, which is applied in the field of thermally conductive polymer composite materials, can solve the problems of not meeting the requirements of thermal conductivity, failing to reflect graphene, and being unfavorable for industrial production, so as to improve the thermal conductivity and speed up the vulcanization rate. , the effect of enhancing physical strength

Active Publication Date: 2016-04-13
DEYANG CARBONENE TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

This patent uses a mixture of expanded graphite and other carbon materials as a filler to improve the thermal conductivity of the silicone rubber composite material. Although this method can increase the thermal conductivity of the silicone rubber composite material to 4W/m·K, it still cannot meet the high power requirements. Electronic equipment requires thermal conductivity of thermal gap filler materials, and its preparation process is very complicated, which is not conducive to industrial production
[0006] Another example is that th...

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  • Preparation method of interface heat conduction material silicone rubber pad

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Embodiment 1

[0032] A method for preparing a silicone rubber mat, which is a thermal interface material, includes the following steps:

[0033] (1) Add 10-300 parts by weight of inorganic thermally conductive powder, 1-10 parts by weight of catalyst, and 1-10 parts by weight of a mixture of dimethyl silicone oil and hydrogen-containing silicone oil into 100 parts by weight of silicone rubber, and knead After homogenization, the rubber compound is obtained;

[0034] (2) Take 10-90 parts by weight of a carbon material with a three-dimensional network structure, and evenly fill the mixed rubber obtained in step (1) into the carbon material to obtain a composite material; wherein the carbon material with a three-dimensional network structure is graphene Or carbon fiber, and when it is graphene, the thickness of graphene is 0.5-10mm;

[0035] (3) Put the composite material into an oven to vulcanize, the vulcanization temperature is 120-180℃, and the vulcanization time is 0.5-2h. After vulcanization, ...

Embodiment 2

[0043] A method for preparing a silicone rubber mat, which is a thermal interface material, includes the following steps:

[0044] (1) Prepare materials, prepare 100g of raw silicone rubber, 10g of metal aluminum powder, 1g of tert-butyl peroxybenzoate and 1g of a mixture composed of dimethyl silicone oil and hydrogen-containing silicone oil. After the preparation is completed, the silicone rubber and inorganic thermal conductivity The powder, the catalyst, and the mixture composed of dimethyl silicone oil and hydrogen-containing silicone oil are added to a kneader for kneading, and the mixed rubber is obtained after uniform kneading. Among them, simethicone with a viscosity of 500mPa·s is added to the catalyst, and the mass percentage of the catalyst and simethicone is 1:10; in the mixture of simethicone and hydrogen-containing silicone oil, hydrogen-containing silicone oil and The mass percentage of simethicone is 1:20, the hydrogen content in hydrogen-containing silicone oil i...

Embodiment 3

[0048] A method for preparing a silicone rubber mat, which is a thermal interface material, includes the following steps:

[0049] (1) Prepare materials, prepare 100g of raw silicone rubber, 300g of metal aluminum powder, 10g of tert-butyl peroxybenzoate and 10g of a mixture composed of dimethyl silicone oil and hydrogen-containing silicone oil. After the preparation is completed, the silicone rubber and inorganic thermal conductivity Powder, catalyst, and a mixture of simethicone and hydrogen-containing silicone oil are added to the kneader and kneaded. After uniform kneading, a rubber compound is obtained; among them, dimethyl silicone oil with a viscosity of 5000 mPa·s is added to the catalyst. The mass percentage of simethicone is 10:100; in the mixture of simethicone and hydrogen-containing silicone oil, the mass percentage of hydrogen-containing silicone oil and simethicone is 20:100, and the hydrogen content in hydrogen-containing silicone oil It is 0.5%, and the viscosity...

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Abstract

The invention discloses a preparation method of an interface heat conduction material silicone rubber pad. The method comprises steps as follows: (1) adding 10-300 parts of inorganic heat conduction powder by weight, 1-10 parts of a catalyst by weight and 1-10 parts of a mixture of dimethicone and hydrogen-containing silicone oil by weight to 100 parts of silicone rubber by weight, and evenly kneading the mixture to obtain a rubber compound; (2) taking 10-90 parts of a carbon material adopting a 3D network structure by weight, and filling the carbon material with the rubber compound obtained in step (1) to obtain a composite material; (3) vulcanizing the composite material to obtain a finished product, namely, the silicone rubber pad. With the adoption of the method, the carbon material with the ultrahigh heat-conducting property can be arranged directionally in the silicone rubber to form the regular directional heat conduction network structure, so that the product with the ultrahigh heat conductivity is obtained.

Description

Technical field [0001] The invention relates to the field of thermally conductive polymer composite materials, in particular to a method for preparing an interface thermally conductive material silicone rubber pad with ultra-high thermal conductivity. Background technique [0002] With the rapid development of microelectronics integration technology and high-density printed circuit board assembly technology, microelectronics devices are now gradually developing in the direction of miniaturization and convenience. Driven by high power, the working thermal environment of semiconductors moves rapidly to high temperatures, which requires that the heat generated by the semiconductors can be conducted at a high speed to ensure the normal operation of electronic equipment. With the development of electronic equipment in the direction of high power and miniaturization, the requirements for thermal conductivity of thermally conductive gap fillers are getting higher and higher. It can even...

Claims

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Application Information

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IPC IPC(8): C08L83/04C08L83/05C08L83/07C08K13/04C08K3/08C08K3/34C08K3/38C08K3/22C08K3/04C08K3/28C08K7/06B29C35/02
CPCB29C35/02C08L83/04C08L2205/025C08L2205/03C08K3/04C08K2003/0812C08K2003/085C08K3/34C08K2003/385C08K7/06C08K2003/282C08K2003/2227C08K13/04
Inventor 何洪泉姚林尹天平黄全国高华
Owner DEYANG CARBONENE TECH
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