Preparation method of high-purity chalcogenide infrared glass
A technology of infrared glass and uniformity, applied in the field of infrared glass materials, can solve the problems of long-term mixing and the generation of component stripes, and achieve the effects of reducing energy consumption, eliminating component stripes, and shortening mixing time.
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[0021] Implementation example: chalcogenide glass composition is As 38 S 62
[0022] Using high-purity sulfur with a purity of 5N and high-purity arsenic with a purity of 6N as raw materials, according to the above-mentioned chemical composition ratio, weigh the materials in a glove box filled with argon, and fill them with pre-cleaned and pre-calcined hydroxyl content lower than In the 10ppm quartz distillation tubes A and B, pass high-purity argon gas into the distillation tubes and connect with the quartz spiral tube with a hydroxyl content lower than 10ppm, and heat the distillation tubes A and B to 425°C and 600°C respectively, so that the gaseous The S and As simple substances are fully mixed at the molecular scale in a spiral tube heated to 650°C, and then the mixed gaseous As-S infrared glass frit is passed into a cleaned and pre-fired quartz ampoule with a hydroxyl content lower than 10ppm Condensation; vacuumize the quartz ampoule containing the mixture, when the v...
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