Emulsifier composition and preparation method thereof
A technology of composition and emulsifier, which is applied in the field of drilling fluid, can solve the problems of unsatisfactory emulsification rate and electrical stability, and achieve the effects of increasing emulsification efficiency, simple preparation method, and easy maintenance of uniformity
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Embodiment 1
[0023] An emulsifier composition comprising the following raw materials: 100kg of white oil, 60kg of tall oil, 10kg of fumaric acid, 6kg of diethylenetriamine, 8kg of tetraethylenepentamine, and 90kg of oxidatively polymerized fatty acid ester.
[0024] When preparing the above-mentioned emulsifier composition, (1) stir tall oil, diethylenetriamine and tetraethylenepentamine for 0.8h, stir evenly and then heat up to 110°C, and react for 2.5h; (2) to step (1) Add fumaric acid to the system, maintain the temperature for 1.5h; (3) add white oil and oxidatively polymerized fatty acid ester to the system in step (2), stir evenly, and cool down to room temperature to obtain the product.
[0025] Add the emulsifier composition obtained above at 3% of the weight of the oil-based drilling fluid, and the obtained product is used to test its performance.
Embodiment 2
[0027] An emulsifier composition comprising the following raw materials: 100kg of white oil, 65kg of tall oil, 12kg of fumaric acid, 8kg of diethylenetriamine, 10kg of tetraethylenepentamine, and 85kg of oxidatively polymerized fatty acid ester.
[0028] When preparing the above-mentioned drilling fluid, (1) stir tall oil, diethylenetriamine and tetraethylenepentamine for 1 hour, stir evenly, then raise the temperature to 115°C, and react for 3 hours; (2) add rich Maic acid, maintain the temperature for 2 hours; (3) Add white oil and oxidized polymerized fatty acid ester to the system in step (2), stir evenly and cool down to room temperature.
[0029] The emulsifier composition obtained above was added thereto at 4% by weight of the oil-based drilling fluid, and the obtained product was used to test its performance.
Embodiment 3
[0031] An emulsifier composition comprising the following raw materials: 100kg of white oil, 65kg of tall oil, 15kg of fumaric acid, 12kg of diethylenetriamine, 15kg of tetraethylenepentamine, and 82kg of oxidatively polymerized fatty acid ester.
[0032] When preparing the above drilling fluid, (1) Stir tall oil, diethylenetriamine and tetraethylenepentamine for 1.5h, stir well and then raise the temperature to 120°C, and react for 3h; (2) Add to the system in step (1) Fumaric acid, maintain the temperature for 2.5 hours; (3) add white oil and oxidized polymerized fatty acid ester to the system in step (2), stir evenly and cool down to room temperature.
[0033] Add the emulsifier composition obtained above at 3% of the weight of the oil-based drilling fluid, and the obtained product is used to test its performance.
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