Three-hole rock core kettle and ultra-low-permeability reservoir fluid damage evaluation test apparatus and method

An experimental method and technology of experimental device, applied in measurement device, permeability/surface area analysis, suspension and porous material analysis, etc., can solve the problem of not considering osmotic pressure, high displacement pressure difference, long flow rate stabilization time, etc.

Active Publication Date: 2016-04-27
CHINA UNIV OF PETROLEUM (BEIJING)
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

It is clearly stated in the SY/T5358-2010 standard that this standard applies to air permeability greater than 1×10 -3 um 2 The experimental method for sensitivity evaluation of rock samples in clastic rock reservoirs, while the gas permeability of ultra-low permeability reservoirs is generally lower than 1×10 -3 um 2 , using the above evaluation method will have the following problems: On the one hand, it needs a high displacement pressure difference and a long flow rate stabilization time, which requires high equipment, and the permeability is 0.1×10 -3 um 2 Take a rock sample as an example. Under the conditions of 2.54 cm in diameter, 5 cm in length, 1 ml/min flow rate, and water as the displacement medium, the displacement pressure difference exceeds 16 MPa, and the flow rate basically stabilizes for more than 5 hours.
On the other ha

Method used

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  • Three-hole rock core kettle and ultra-low-permeability reservoir fluid damage evaluation test apparatus and method
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  • Three-hole rock core kettle and ultra-low-permeability reservoir fluid damage evaluation test apparatus and method

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Embodiment 1

[0070] like figure 1 As shown, the present invention provides a three-hole core kettle 100 for holding a core sample therein for experiments. The three-hole core kettle 100 includes an upper cover 10 , a lower cover 20 , and a core sample 30 . The upper cover body 10 is a cylinder made of stainless steel, the diameter of the upper cover body 10 is 3.86 inches, and the thickness is 1.25 inches. like figure 2 , image 3 , Figure 4 and Figure 5 As shown, the lower end surface of the upper cover body 10 is provided with a circular first groove 101, the first groove 101 is located in the middle position of the upper cover body 10, and the upper cover body 10 is provided with a first concave groove through its upper end surface. The first through hole 102 and the second through hole 103 of the groove 101 . The first through hole 102 and the second through hole 103 can be formed by drilling the upper cover body 10 , and the diameter of the first through hole 102 and the secon...

Embodiment 2

[0077] The present invention also provides an ultra-low permeability reservoir fluid damage evaluation experimental device 1000 using the three-hole core kettle 100, such as Figure 11 As shown, the experimental device 1000 includes a three-hole core tank 100 , an intermediate container 200 for the upstream simulated formation fluid, an intermediate container 300 for the downstream simulated formation fluid, and an intermediate container 400 for the liquid to be tested.

[0078]The first end of the upstream simulated formation fluid intermediate container 200 and the first end of the downstream simulated formation fluid intermediate container 300 are respectively connected to the plunger pump 500 through pipelines, and the first end of the upstream simulated formation fluid intermediate container 200 is connected to the plunger pump 500 The pipeline between them is provided with a control valve a1; the pipeline between the first end of the downstream simulated formation fluid i...

Embodiment 3

[0086] A certain area in my country is rich in shale gas resources, and the shale reservoir matrix is ​​dense, which is a typical ultra-low permeability reservoir. The development of shale gas resources requires large-scale hydraulic fracturing operations to transform the reservoir. In order to form complex The volume fracture network is proposed to use slick water fracturing fluid system. In order to test the damage degree of the fracturing fluid to the shale reservoir in the area, the present invention also provides an experimental method using the above-mentioned experimental device 1000, the experimental method comprising:

[0087] S1, prepare a core sample 30 with a diameter of 2.5 inches and a thickness of 0.25 inches, and prepare a simulated formation fluid with the same activity as the original interstitial fluid.

[0088] S2, put the prepared core sample 30 into the three-hole core kettle 100, and connect all components through pipelines. Connect the pipelines between...

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Abstract

The present invention is a three-hole rock core kettle and an ultra-low-permeability reservoir fluid damage evaluation test apparatus and method, the three-hole rock core kettle takes upper and lower cover bodies for clamping a rock core sample, and the upper and lower cover bodies are respectively provided with through holes communicating rock core sample surface. The ultra-low-permeability reservoir fluid damage evaluation test apparatus includes the three-hole rock core kettle, an upstream simulated formation fluid intermediate vessel, a downstream simulated formation fluid intermediate vessel, a to-be-tested fluid intermediate vessel, a plunger pump, a vacuum pump and a nitrogen bottle; the various components are connected by pipes, and corresponding control valves, gas pressure regulation valves and back-pressure valves are arranged. The ultra-low-permeability reservoir fluid damage evaluation test method is as follows: simulated reservoir fluids with same activity are contacted with upper and lower surfaces of the rack core sample, meanwhile the simulated reservoir fluid continuously flows on the upper surface of the simulated reservoir fluid, osmotic pressure transmission is eliminated, and by monitoring of the change with time of downstream fluid pressure, penetration rates of the sample before and after contamination can be obtained, and further damage degree can be evaluated. The three-hole rock core kettle is simple in structure, the test apparatus and method are easy to use, the test pressure is reduced, and experimental data is reliable.

Description

technical field [0001] The invention relates to an oil and natural gas reservoir damage evaluation technology, in particular to a three-hole core kettle and an ultra-low permeability reservoir liquid damage evaluation experimental device and method. Background technique [0002] At present, low-permeability and ultra-low-permeability reserves account for about two-thirds of the proven oil and gas reserves. Low-permeability and ultra-low-permeability reserves will be the focus and difficulty of exploration and development for my country's oil production replacement. In the process of exploration, development and production, low-permeability and ultra-low-permeability reservoirs are more vulnerable to damage than medium and high-permeability reservoirs during production operations, and the damage caused by the reservoir is more harmful. To eliminate the damage Also more difficult. Therefore, to improve the exploration and development effect of ultra-low permeability reservoir...

Claims

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Application Information

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IPC IPC(8): G01N33/00G01N15/08
CPCG01N15/08G01N33/00
Inventor 薛艳鹏周福建姚二冬曲鸿雁杨凯左洁秦小仑王博
Owner CHINA UNIV OF PETROLEUM (BEIJING)
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