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A kind of sheep oil degumming method

A degumming method and sheep oil technology, applied in the field of sheep oil degumming, can solve the problems of poor separation of oil and soap, increase of oil color, and decline of sheep oil quality, so as to shorten the enzymatic hydrolysis reaction time, avoid a large amount of waste water, and process safe effect

Active Publication Date: 2019-11-08
WUHAN POLYTECHNIC UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] However, due to the high content of colloid in sheep oil, there are a series of adverse effects in the refining and processing of sheep oil. For example, when alkali refining deacidification, oil soap can not be separated well, resulting in refining The consumption increases, and the soap content in sheep oil increases at the same time; when deodorizing, the gum is easy to carbonize, which increases the color of the oil; when decolorizing, it adheres to the surface of the decolorizing agent, reducing the decolorization efficiency, etc., resulting in a decline in the quality of the final product sheep oil

Method used

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  • A kind of sheep oil degumming method

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Effect test

Embodiment 1

[0031] Add a citric acid solution with a concentration of 45% to the sheep oil raw material, the addition of the citric acid solution is 0.10% of the quality of the sheep oil raw material, and carry out acidification treatment under the assistance of ultrasound, and control the temperature at 80 ° C during the acidification treatment. The ultrasonic intensity is 1.40W / cm 2 , the ultrasonic time is 25 minutes, and after the acidification treatment is completed, the acidified sheep oil is obtained; wherein, the composition content of the sheep oil raw material includes: a moisture content of 0.31%, an insoluble impurity content of 0.09%, and a phospholipid content of 879.26 mg / kg; Add a certain amount of distilled water to the acidified sheep oil, the addition of the distilled water is 3.4% of the acidified sheep oil quality, adjust the pH of the acidified sheep oil to 5.0, and add phospholipase A1 to carry out ultrasonic-assisted enzymolysis, the phospholipid The amount of enzyme...

Embodiment 2

[0033] Add a citric acid solution with a concentration of 45% to the sheep oil raw material, the addition of the citric acid solution is 0.12% of the quality of the sheep oil raw material, and carry out acidification treatment under the assistance of ultrasound, and control the temperature at 75 ° C during the acidification treatment. Ultrasonic intensity is 1.50W / cm 2 , the ultrasonic time is 20 minutes, and after the acidification treatment is completed, the acidified sheep oil is obtained; wherein, the composition content of the sheep oil raw material includes: a moisture content of 0.20%, an insoluble impurity content of 0.25%, and a phospholipid content of 1001.42 mg / kg; Add a certain amount of distilled water to the acidified sheep oil, the addition of the distilled water is 3.6% of the acidified sheep oil quality, adjust the pH of the acidified sheep oil to 4.9, and add phospholipase A1 to carry out ultrasonic-assisted enzymolysis, the phospholipid The amount of enzyme ...

Embodiment 3

[0035] Add a citric acid solution with a concentration of 45% to the sheep oil raw material, the addition of the citric acid solution is 0.14% of the quality of the sheep oil raw material, and carry out acidification treatment under the assistance of ultrasound, and control the temperature at 85 ° C during the acidification treatment. The ultrasonic intensity is 1.60W / cm 2 , the ultrasonic time is 15 minutes, and after the acidification treatment is completed, the acidified sheep oil is obtained; wherein, the composition content of the sheep oil raw material includes: a moisture content of 0.08%, an insoluble impurity content of 0.17%, and a phospholipid content of 1123.58 mg / kg; Add a certain amount of distilled water to the acidified sheep oil, the addition of the distilled water is 3.2% of the quality of the acidified sheep oil, adjust the pH of the acidified sheep oil to 5.1, and add phospholipase A1 for ultrasonic-assisted enzymolysis, the phospholipid The amount of enzym...

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Abstract

The invention discloses a sheep oil degumming method, which comprises the following steps: adding citric acid solution to the sheep oil raw material, and carrying out acidification treatment under the assistance of ultrasound to obtain acidified sheep oil; adding a certain amount of distilled water to the acidified sheep oil, Adjust the pH and temperature of acidified sheep oil, and add phospholipase A1 for ultrasonic-assisted enzymolysis to obtain sheep oil for one enzymatic hydrolysis; adjust the pH and temperature for one enzymatic hydrolysis of suet, and add phospholipase B for ultrasonic-assisted enzymolysis to obtain Secondary enzymatic hydrolysis of sheep oil; adjust the pH and temperature of the second enzymatic hydrolysis sheep oil, and add phospholipase C for ultrasonic-assisted enzymolysis to obtain third enzymatic hydrolysis sheep oil; perform enzyme inactivation treatment on the third enzymatic hydrolysis sheep oil, centrifuge The oil sample in the upper layer was used to obtain enzyme-inactivated sheep oil; the enzyme-inactivated sheep oil was vacuum-dried to obtain degummed sheep oil. The sheep oil degumming method provided by the invention has safe process and convenient operation.

Description

technical field [0001] The invention relates to the technical field of sheep oil, in particular to a method for degumming sheep oil. Background technique [0002] Since the 1990s, my country's meat production has leapt to the first place in the world. In 2009, my country's meat output was 75 million tons, accounting for about 40% of the world's total output, of which mutton production accounted for 6% of the domestic total meat output, accounting for 37% of the world's total. At present, the development direction of the global sheep industry has shifted from pure wool to meat. my country is a big sheep-raising country. The number of sheep and goats and the total production of mutton rank first in the world. Because of its high protein content, low cholesterol content, rich nutrition, high edible value and warm nature, mutton has a warm after eating. With the effects of warming the body, nourishing the body and warming the spleen and stomach, the market share in the inland a...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C11B3/00C11B3/04
CPCC11B3/001C11B3/003C11B3/04
Inventor 何东平胡传荣刘零怡周力
Owner WUHAN POLYTECHNIC UNIVERSITY
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