Preparation method of low-furfuryl-alcohol-content high-strength furan resin
A furan resin, high-strength technology, applied in the field of preparation of high-strength furan resin, can solve the problems of sand mold collapse, resin high-temperature performance surplus, regeneration difficulties, etc., to achieve the effect of improving high-temperature collapse and reducing casting costs
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Embodiment 1
[0029] Ⅰ. Stir 500 kg of furfuryl alcohol and 2 kg of silane KH602 in a stirred tank and react at 30°C for 6 hours to form a small molecule initial polymer of furfuryl alcohol, which is released for use;
[0030] Ⅱ. Add 165 kg of urea and 185 kg of formaldehyde in a 1-ton resin reactor, and react to completion under alkaline conditions for about 2 hours;
[0031] Ⅲ. After completion of the reaction, add 150 kilograms of furfuryl alcohol small molecular initial polymers in step I, and react to complete under acidic conditions for about 2 hours;
[0032] Ⅳ. After completion of the reaction, add the furfuryl alcohol small molecular initial polymer in 150 kilograms of steps I, turn off the steam, and stir for 1h;
[0033] Ⅴ. cooling water is cooled to 60 DEG C, add 200 kilograms of furfuryl alcohol small molecular primary polymers in step I, stir evenly;
[0034] VI. Add 75 kg of water and 75 kg of methanol.
[0035] The product is tested according to the national standard "JBT7...
Embodiment 2
[0037] Ⅰ. Stir 570 kg of furfuryl alcohol and 2.5 kg of silane KH550 in a stirred tank and react at 40°C for 4 hours to form a small molecule initial polymer of furfuryl alcohol, which is released for use;
[0038] Ⅱ. Add 170 kg of urea and 180 kg of formaldehyde to a 1-ton resin reactor, and react completely under alkaline conditions for about 2 hours;
[0039] Ⅲ. After completion of the reaction, add 190 kilograms of furfuryl alcohol small molecular initial polymers in step I, and react to complete under acidic conditions for about 2 hours;
[0040] Ⅳ. after completion of the reaction, add the furfuryl alcohol small molecular initial polymer in 190 kilograms of steps I, turn off the steam, and stir for 1.5h;
[0041] Ⅴ. cooling water is cooled to 65 DEG C, add the furfuryl alcohol small molecular initial polymer in 190 kilograms of steps I, stir;
[0042] VI. Add 50 kg of water and 30 kg of methanol.
[0043] The product is tested according to the national standard "JBT752...
Embodiment 3
[0045] Ⅰ. Stir 600 kg of furfuryl alcohol and 3 kg of silane KH602 in a stirred tank and react at 50°C for 2 hours to form a small molecule initial polymer of furfuryl alcohol, which is released for later use;
[0046] Ⅱ. Add 148 kg of urea and 152 kg of formaldehyde to a 1-ton resin reactor, and react to completion under alkaline conditions for about 2 hours;
[0047] Ⅲ. After completion of the reaction, add 200 kg of furfuryl alcohol small molecular initial polymer in step I, and react to complete under acidic conditions for about 2 hours;
[0048] Ⅳ. After completion of the reaction, add 200 kilograms of furfuryl alcohol small molecular initial polymers in the step I, turn off the steam, and stir for 2h;
[0049] Ⅴ. cooling water is cooled to 70 DEG C, add 200 kilograms of furfuryl alcohol small molecular primary polymers in step I, stir evenly;
[0050] VI. Add 50 kg of water and 50 kg of methanol.
[0051] The product is tested according to the national standard "JBT752...
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Abstract
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