A kind of activated carbon activation method of hydrogen combustion steam activation furnace

A technology of water vapor activation and activation method, applied in the field of activated carbon physical activation, can solve the problems of uneven activation effect, high feeding requirements and high technical requirements, and achieve the effect of improving activation effect, uniform activation reaction and saving energy.

Inactive Publication Date: 2017-09-05
TAIYUAN UNIV OF TECH
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  • Abstract
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Problems solved by technology

Vertical activation furnaces are mainly Sleep furnaces, and their main disadvantages are: complex structure, high requirements for feed materials, and high technical requirements
During the actual operation of the activation furnace, the actual consumption of water fed into the activation furnace in the two processes of gasification and activation is unknown, and the actual consumption of water vapor in the activation process can only be calculated according to a specific calculation formula Conversion, there are inaccurate factors
Secondly, the phenomenon of uneven activation effect is easy to appear during the activation process.

Method used

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  • A kind of activated carbon activation method of hydrogen combustion steam activation furnace
  • A kind of activated carbon activation method of hydrogen combustion steam activation furnace
  • A kind of activated carbon activation method of hydrogen combustion steam activation furnace

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Embodiment Construction

[0030] The specific implementation manners of the present invention will be further described below.

[0031] Implement a kind of gac activation method of hydrogen combustion steam activation furnace, the activation method of described gac is to carry out according to the following steps:

[0032] Firstly, the activated carbon carbonized material is pretreated;

[0033] Then the pretreated activated carbon is weighed, and 300g of activated carbon samples with a particle size of 8 × 10mm are weighed and replaced with

[0034] Then put the activated carbon into the activation reaction section 9 of the hydrogen combustion steam activation furnace and wait for the activation process.

[0035] Then set the reaction temperature, reaction time, ventilation time, heating rate and gas flow rate in the controller.

[0036] as attached figure 1 to attach Figure 7shown. The entire activation process begins. First, the activated carbon carbonized material is heated and activated in t...

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Abstract

The invention discloses an active carbon activation method of a hydrogen burning water vapor activation furnace. The method comprises the following steps: adding the pretreated carbonization raw material into an activation reaction section of the activation furnace; in a nitrogen atmosphere with a normal pressure, heating to form primary active carbon; proportionally introducing hydrogen and oxygen into the bottom layer of the activation furnace at the same time and mixing; enabling the mixture to rise to a gas mixing firing section of the activation furnace through a first-level gas distribution plate, and mixing with the introduced nitrogen for reacting to generate water vapor; enabling the water vapor serving as an activator to rise into a gas buffering distribution section through a second-level gas distribution plate for buffering and then rise for an activation reaction with the primary active carbon through a material support gas distribution plate; and in the nitrogen atmosphere, cooling to obtain active carbon. In the method, a new activator introducing way is provided, and the generation amount of water vapor is accurately controlled through the introduced oxygen while the heat energy released by the burning of hydrogen and oxygen is utilized; and therefore, the energy is saved, and the activation efficiency is improved.

Description

technical field [0001] The invention relates to a method for physical activation of activated carbon and activation equipment for activated carbon, in particular to a method for activating activated carbon by burning steam with hydrogen and an activation furnace for burning steam with hydrogen. Background technique [0002] Activated carbon is an excellent adsorbent. Because of its extremely developed inner pore structure and large specific surface area, it is widely used in various aspects such as chemical wastewater treatment and environmental protection. There are two production methods of activated carbon, chemical activation and physical activation. [0003] There are usually two kinds of activation furnaces in the existing physical activation methods, one is a vertical activation furnace, and the other is a horizontal rotary activation furnace. The vertical activation furnace is mainly the Sleep furnace, and its main disadvantages are: complex structure, high requirem...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C01B32/39C01B32/336
CPCY02P20/10
Inventor 李源李国强付亚利张国杰张静刘俊张永发
Owner TAIYUAN UNIV OF TECH
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