Preparation method of natural product anti-fouling agent
A technology of natural products and antifouling agents, applied in paints containing biocide, antifouling/underwater coatings, coatings, etc., can solve the problems of inconspicuous antifouling effect, secondary pollution, strong toxicity, etc., and achieve Long duration of antifouling, good antifouling effect and low cost
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example 1
[0017] Firstly, according to the mass ratio of 3:2:2, weigh jujube kernels, cypress kernels, and Prunella vulgaris respectively and put them in an oven, dry them at 80°C for 2 hours, put them into a ball mill for grinding, pass through a 150-mesh standard sieve, and put the sieved Put the particles into a beaker, add a 3% sodium chloride solution to the beaker, the amount added is twice the mass of the particles, move the beaker to an induction cooker, set the power to 2000W, and heat for 40 minutes; after the above heating is completed, Increase the power to 2700W, continue heating for 2 hours, then add sodium chloride solution volume 15% ethyl acetate to the beaker, stir evenly with a stirring bar, then cool naturally to room temperature, use cotton as a filter membrane, and filter the mixture in the beaker Filter, collect the filtrate and put it in a centrifuge, centrifuge at 5000r / min, and collect the supernatant; according to the mass ratio of 1:1, weigh fresh red algae an...
example 2
[0020] Firstly, according to the mass ratio of 3:2:2, weigh jujube kernels, cypress kernels, and Prunella vulgaris respectively and put them in an oven, dry them at 80°C for 2.5 hours, put them into a ball mill for grinding, pass through a 150-mesh standard sieve, and put the sieved Put the particles into a beaker, add a 3% sodium chloride solution to the beaker, the amount added is 2.5 times the mass of the particles, move the beaker to the induction cooker, set the power to 2100W, and heat for 43min; after the above heating is completed , increase the power to 2800W, continue heating for 2.5h, then add sodium chloride solution volume 17% ethyl acetate to the beaker, stir evenly with a stirring bar, then cool naturally to room temperature, use cotton as a filter membrane, The mixture is filtered, the filtrate is collected and put into a centrifuge, centrifuged at 5500r / min, and the supernatant is collected; according to a mass ratio of 1:1, fresh red algae and freshly deseeded...
example 3
[0023]First, according to the mass ratio of 3:2:2, weigh the jujube kernels, cypress kernels and Prunella vulgaris respectively and put them in an oven, dry them at 80°C for 3 hours, put them into a ball mill for grinding, pass through a 150-mesh standard sieve, and put the sieved Put the particles into a beaker, add a 3% sodium chloride solution to the beaker, the amount added is 3 times the mass of the particles, move the beaker to an induction cooker, set the power to 2200W, and heat for 45 minutes; after the above heating is completed, Increase the power to 2900W, continue heating for 3 hours, then add sodium chloride solution volume 20% ethyl acetate to the beaker, stir evenly with a stirring bar, then cool naturally to room temperature, use cotton as a filter membrane, and filter the mixture in the beaker Filter, collect the filtrate and put it in a centrifuge, centrifuge at 6000r / min, collect the supernatant; according to the mass ratio of 1:1, weigh fresh red algae and ...
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