A kind of curing agent for phosphate binder self-setting sand and its preparation and use method
A curing agent and binder technology, used in manufacturing tools, casting equipment, metal processing equipment, etc., can solve problems such as poor hygroscopic resistance, achieve good collapsibility, and improve the effect of pollution
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Embodiment 1
[0022] The weight ratio of each component in the curing agent of this embodiment is: component I aniline is 20% of the weight of the binder, and component II is 10% of the weight of the binder. Wherein the weight percentage of each component in component II is: 43% of urea, 40% of water, 5% of ammonium chloride, 4% of silane, and 8% of tetraethylenepentamine.
[0023] The preparation method of component II:
[0024] Step 1: first add 40Kg of water to the reactor, and raise the temperature to 70°C;
[0025] Step 2: Start the agitator to start stirring, add 43Kg of urea into the reaction kettle, at this time the temperature will drop, after all dissolve, heat up to 75°C again;
[0026] Step 3: Slowly add 5Kg of ammonium chloride to the reaction kettle, and keep warm at 70°C until completely dissolved;
[0027] Step 4: Cool down to room temperature, add 8Kg of tetraethylenepentamine and 4Kg of silane, stir for 20 minutes after the dissolution is complete, and discharge.
[002...
Embodiment 2
[0030] The weight ratio of each component in the curing agent in this embodiment is: component I aniline is 20% of the weight of the binder, and component II is 20% of the weight of the binder. Wherein the weight percentage of each component in component II is: 30% of urea, 34% of water, 15% of ammonium chloride, 6% of silane, and 15% of tetraethylenepentamine.
[0031] The preparation method of component II:
[0032] Step 1: First add 34Kg of water to the reactor, and raise the temperature to 70°C;
[0033] Step 2: Start the agitator to start stirring, add 30Kg of urea into the reaction kettle, at this time the temperature will drop, after all dissolve, heat up to 75°C again;
[0034] Step 3: Slowly add 15Kg of ammonium chloride to the reaction kettle, and keep warm at 70°C until completely dissolved;
[0035] Step 4: Cool down to room temperature, add 15Kg of tetraethylenepentamine and 6Kg of silane, stir for 30 minutes after the dissolution is complete, and discharge.
...
Embodiment 3
[0038] The weight ratio of each component in the curing agent of this embodiment is: component I aniline is 10% of the weight of the binder, and component II is 10% of the weight of the binder. Wherein the weight percentage of each component in component II is: urea 25%, water 40%, ammonium chloride 20%, silane 1%, tetraethylenepentamine 14%.
[0039] The preparation method of component II:
[0040] Step 1: first add 40Kg of water to the reactor, and raise the temperature to 50°C;
[0041] Step 2: Start the agitator to start stirring, add 25Kg of urea into the reaction kettle, the temperature will drop at this time, after all dissolve, heat up to 70°C again;
[0042] Step 3: Slowly add 20Kg of ammonium chloride into the reaction kettle, keep warm at 60°C until completely dissolved;
[0043] Step 4: Cool down to room temperature, add 14Kg of tetraethylenepentamine and 1Kg of silane, stir for 15 minutes after the solution is transparent, and discharge.
[0044] The core-makin...
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