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Preparation method of efflorescence-resistant ceramic tile adhesive

A tile adhesive and anti-efflorescence technology, which is applied in the direction of adhesives, adhesive additives, inorganic adhesives, etc., can solve the problems of strong anti-efflorescence ability, affecting the overall appearance of the building, and high viscosity of anti-efflorescence tile adhesives. problem, and achieve the effects of low cost, strong anti-pantherine ability, and simple preparation steps

Inactive Publication Date: 2016-08-31
张静
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The technical problem to be solved by the present invention: Aiming at the problem that the alkali content in the cement-based tile adhesive with ordinary Portland cement as the main raw material is relatively high, and the phenomenon of efflorescence is very easy to occur, which affects the overall appearance of the building, a calcined cement is provided. The final coal gangue is crushed, stirred and mixed with hydrochloric acid, filtered, and the filtrate is rinsed, dried, and the dried material is mixed with allyl acetate and other substances to be heated, then naturally cooled to room temperature, and silicate is added Cement and hydroxypropyl methylcellulose solution are mixed and stirred to obtain the anti-pan-alkaline tile adhesive base material, and finally mixed with ethylene-vinyl acetate copolymer and other substances to prepare the anti-pan-alkali tile adhesive method, the anti-pan-alkaline tile adhesive prepared by the present invention has high viscosity and strong anti-pan-alkali ability

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0017] Firstly, coal gangue is put into a calciner, calcined at 500°C for 2 hours, and then cooled to room temperature with the furnace, the calcined material is taken out and put into a pulverizer for crushing, passed through a 100-mesh sieve, and the sieved particles and mass fraction Mix 10% hydrochloric acid solution at a solid-to-liquid ratio of 1:3, and stir for 40 minutes at 50°C at a speed of 120r / min; filter after the above stirring is completed, rinse the filtrate with water for 3 times, and wash the filtrate Put it in a drying oven at 90°C and dry it overnight to obtain the dried product, and then take 62 parts of the dried product, 15 parts of allyl acetate, 15 parts of polyethylene glycol and 8 parts of sulfated castor oil in a container , heated to 80°C; after maintaining the above temperature for 2 hours, then cooled naturally to room temperature, and added Portland cement with a dry mass of 110% of the above-mentioned Portland cement and the above-mentioned poly...

example 2

[0020] Firstly, coal gangue is put into a calciner, calcined at 450°C for 1 hour, and then cooled to room temperature with the furnace, the calcined material is taken out and put into a pulverizer for crushing, passed through a 100-mesh sieve, and the sieved particles and mass fraction Mix 10% hydrochloric acid solution at a solid-to-liquid ratio of 1:3, stir at 50°C for 35 minutes at a speed of 120r / min; filter after the above stirring is completed, rinse the filtrate twice with water, and wash the filtrate Put it in a drying oven at 90°C and dry it overnight to obtain the dried product, and then take 50 parts of the dried product, 20 parts of allyl acetate, 18 parts of polyethylene glycol and 12 parts of sulfated castor oil in a container , heated to 70°C; after maintaining the above temperature for 2 hours, then cooled naturally to room temperature, and added the Portland cement with 90% of the above-mentioned dry matter and 15% of the above-mentioned polyethylene glycol wit...

example 3

[0023] Firstly, coal gangue is put into a calciner, calcined at 450°C for 1 hour, and then cooled to room temperature with the furnace, the calcined material is taken out and put into a pulverizer for crushing, passed through a 100-mesh sieve, and the sieved particles and mass fraction Mix 10% hydrochloric acid solution at a solid-to-liquid ratio of 1:3, stir at 50°C for 35 minutes at a speed of 120r / min; filter after the above stirring is completed, rinse the filtrate twice with water, and wash the filtrate Put it in a drying oven at 90°C and dry it overnight to obtain the dried product, then take 60 parts of the dried product, 15 parts of allyl acetate, 17 parts of polyethylene glycol and 8 parts of sulfated castor oil in a container , heated to 75°C; after maintaining the above temperature for 2 hours, then cooled naturally to room temperature, and added Portland cement with 100% of the above-mentioned dry matter and 15% of the above-mentioned polyethylene glycol with a mass...

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Abstract

The invention relates to a preparation method of efflorescence-resistant ceramic tile adhesive and belongs to the technical field of adhesive preparation. The preparation method includes: crushing calcined gangue, stirring and mixing with hydrochloric acid, filtering, washing filtered substances, drying, mixing the dried substances with allylic acetate and the like and heating, naturally cooling to room temperature, adding Portland cement and a hydroxypropyl methyl cellulose solution, and mixing and stirring to obtain efflorescence-resistant ceramic tile adhesive base material, mixing the efflorescence-resistant ceramic tile adhesive base material with ethylene-vinyl acetate copolymer and the like to obtain the efflorescence-resistant ceramic tile adhesive. The efflorescence-resistant ceramic tile adhesive prepared by method is high in efflorescence resistance, and the efflorescence area is only 1.25-2.25%; the adhesive is high in viscosity coefficient, and the measured tensile adhesive strength of the adhesive after 16 days is 0.98-1.25MPa.

Description

technical field [0001] The invention relates to a preparation method of an anti-efflorescence tile adhesive, which belongs to the technical field of adhesive preparation. Background technique [0002] Tile adhesive is a very common bonding material used in building decoration and decoration projects. It is often used to paste ceramic tiles, mosaics, stones, etc. However, due to the high alkali content of ordinary Portland cement, traditional cement-based tile adhesives are prone to efflorescence, which affects the overall appearance of the building. On the other hand, wall materials such as hollow bricks, fly ash bricks, and aerated concrete are more and more widely used, and the water absorption and volume deformation of these wall materials are generally higher. Large, affecting the glue and stability of tiles, resulting in hollowing and cracking are extremely common and severe. Contents of the invention [0003] The technical problem to be solved by the present invent...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09J1/00C09J11/04C09J11/06C09J11/08
CPCC09J1/00C09J11/04C09J11/06C09J11/08
Inventor 张静薛培龙宋奇
Owner 张静