Water solubility resisting PVA nanofiber composite fabric and preparation method thereof

A composite fabric and nanofiber technology, which is applied in spinning solution preparation, fiber treatment, ultrasonic/sonic fiber treatment, etc., can solve the problems of easy separation, difficult complete bonding, and less research, so as to achieve stable structure and performance, Improves service life and prevents separation

Active Publication Date: 2016-08-31
SUZHOU UNIV
View PDF3 Cites 7 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the poor mechanical properties of the nanofiber membrane, it must be combined with the base fabric to have practical application value in the field of clothing. However, when the nanofiber and the base fabric are combined, it is not easy to completely bond between the two, and it is easy to separate d...

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Water solubility resisting PVA nanofiber composite fabric and preparation method thereof
  • Water solubility resisting PVA nanofiber composite fabric and preparation method thereof
  • Water solubility resisting PVA nanofiber composite fabric and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] A preparation method of water-soluble PVA nanofiber composite fabric, comprising the steps of:

[0032] (1) Pretreatment of base fabric: spinning nylon (54g / m 2 ) cut into a 30cm×100cm sample, and pretreat it with plasma, the processing power is 200w, and the processing time is 3min;

[0033] see figure 1 and figure 2 After the pretreatment of the base fabric, the surface roughness of the fiber in the nylon fiber is significantly improved, forming a large number of nano-scale unevenness, which is conducive to the bonding with the nanofiber;

[0034] (2) Preparation of PVA spinning solution: take 25 g of PVA with a molecular weight of 95,000, add 225 g of deionized water, and use a constant temperature magnetic stirrer for 3 hours at 90° C. to obtain a high molecular weight PVA solution I with a mass fraction of 10%; Weigh 100g of PVA with a molecular weight of 20,000-30,000, add 300g of deionized water, and use a constant temperature magnetic stirrer for 3.5h at 9...

Embodiment 2

[0040] A preparation method of water-soluble PVA nanofiber composite fabric, comprising the steps of:

[0041] (1) Base fabric pretreatment: electric spinning (65g / m 2 ) for plasma pretreatment with a processing power of 300w and a processing time of 3min.

[0042] (2) Prepare PVA spinning solution: make PVA spinning solution as described in step (2) in Example 1.

[0043](3) Preparation of composite fabric: Fix the electrospinning through plasma pretreatment on the receiving drum of the spiral flake electrospinning machine, pour the prepared PVA solution into the semi-cylindrical solution tank, turn on the power, and pass The control panel sets the spinning voltage to 70kV, the generator speed to 15r / min, the spinning distance to 170mm, and the receiver speed to 1.5m / min. The helix rotates at the set speed in the solution tank containing the spinning solution, so that the spinning solution adheres to the tip of the helix and brings the liquid to the spinning area, for...

Embodiment 3

[0048] A preparation method of water-soluble PVA nanofiber composite fabric, comprising the steps of:

[0049] (1) Base fabric pretreatment: polyester taffeta (60g / m 2 ) for plasma pretreatment, processing power 250w, processing time 5min;

[0050] (2) prepare PVA spinning solution: make PVA spinning solution as described in step (2) in embodiment one;

[0051] (3) Preparation of composite fabric: fix the polyester taffeta that has undergone plasma pretreatment on the receiving drum of the spiral sheet electrospinning machine, pour the prepared PVA solution into the semi-cylindrical solution tank, and turn on the power , set the spinning voltage to 80kV, the generator speed to 20r / min, the spinning distance to 160mm, and the receiver speed to 2m / min through the control panel. The helix rotates at a set speed in the solution tank filled with spinning solution, so that the spinning solution is attached to the tip of the helix and the liquid is brought to the spinning are...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
Peel strengthaaaaaaaaaa
Peel strengthaaaaaaaaaa
Peel strengthaaaaaaaaaa
Login to view more

Abstract

A preparation method of a water solubility resisting PVA nanofiber composite fabric comprises the following steps that firstly, plasma pretreatment is carried out on base cloth; secondly, a PVA solution I with the PVA molecular weight being 95,000 and the mass percent being 10% is prepared, a PVA solution II with the PVA molecular weight being 20,000-30,000 and the mass percent being 25% is prepared, the PVA solution I and the PVA solution II are mixed according to the mass ratio of (2:8)-(5:5), and a PVA spinning solution is obtained; thirdly, PVA nanofiber prepared through the PVA spinning solution deposits on the base cloth processed in the first step, and a composite fabric is formed; fourthly, after the composite fabric is soaked in a glutaraldehyde solution, washing and air dying are carried out, and the composite fabric is processed through a vacuum oven. By means of the technical scheme, the production process is free of environment pollution, the production efficiency and the yield of the composite fabric are high, and the composite fabric is stable in structure and performance and high in water solubility resistance.

Description

technical field [0001] The invention relates to a nanofiber composite fabric and a preparation method thereof, in particular to a water-soluble PVA nanofiber composite fabric and a preparation method thereof. Background technique [0002] Due to the high specific surface area of ​​nanofibers, good adsorption performance, and excellent properties such as the small pore size of nanofiber membranes, electrospun nanofibers have attracted attention in the field of protective fabrics. Their protective properties mainly include: filtration, antibacterial, water-proof and breathable, and thermal protection. , Chemical protection, UV protection, etc. [0003] At present, there are relatively many studies on the self-protective properties of nanofiber membranes, and they mainly focus on filtration and antibacterial aspects. Due to the poor mechanical properties of the nanofiber film, it must be combined with the base fabric to have practical application value in the field of clothing...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): D04H13/00D06M10/02D01D1/02D01D5/00D06M13/123
CPCD01D1/02D01D5/003D01D5/0084D04H13/00D06M10/025D06M13/123D10B2501/00D10B2501/04
Inventor 赵楚楚张昕江爱云潘志娟
Owner SUZHOU UNIV
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap