Preparing method for urea solution used for vehicles

A technology of urea and solution for vehicles, applied in separation methods, chemical instruments and methods, gas treatment, etc., can solve problems such as catalyst deactivation, environmental pollution, and blocked pipelines, and achieve simple preparation process, wide source of raw materials, and high production efficiency high effect

Inactive Publication Date: 2016-09-07
NANNING XIAYANG CHEM TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The raw materials for the production of urea for vehicles are ordinary urea and ultrapure water, and impurities such as metal ions, aldehydes, insolubles, and biurets will inevitably be introduced into ordinary urea during the production and packaging process, and these impurities will not only cause the catalyst of the SCR system inactivation, and clogging of pipes
Therefore, the commonly used method is to crystallize and purify common urea by chemical reagents. This process has the disadvantages of low yield, high cost, and easy environmental pollution.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] A preparation method for vehicle urea solution, comprising the following steps:

[0029] (1) Ingredients: Weigh 20kg of agricultural urea, 60kg of high-purity water, 8kg of ethanol, 4kg of N-methylsuccinamide and 1kg of PEG-2 distearate;

[0030] (2) Dissolving: Mix the above-mentioned urea and high-purity water in parts by weight, and stir for 10 minutes at a temperature of 50°C and a rotation speed of 500r / min to obtain a urea solution;

[0031] (3) Adsorption and impurity removal: add 3 kg of cellulose xanthate adsorbent to the above urea solution, continue stirring for 20 minutes, and then filter to remove solid impurities to obtain a clarified urea solution;

[0032] (4) Ion exchange: Perform ion exchange on the clarified urea solution at a flow rate of 5m3 / h to obtain a pure urea solution;

[0033] (5) Mixing: Mix the pure urea solution with the above-mentioned ethanol, N-methylsuccinamide and PEG-2 distearate at a speed of 500r / min for 10 minutes to obtain the v...

Embodiment 2

[0038] A preparation method for vehicle urea solution, comprising the following steps:

[0039] (1) Ingredients: Weigh 25kg of agricultural urea, 70kg of high-purity water, 5kg of ethanol, 6kg of N-methylsuccinamide and 1.5kg of PEG-3 stearate;

[0040] (2) Dissolution: Mix the above-mentioned urea and high-purity water in parts by weight, and stir for 15 minutes at a temperature of 55°C and a rotation speed of 300r / min to obtain a urea solution;

[0041] (3) Adsorption and impurity removal: Add 3.5 kg of cellulose xanthate adsorbent to the above urea solution, continue to stir for 30 minutes, and then filter to remove solid impurities to obtain a clarified urea solution;

[0042] (4) Ion exchange: Perform ion exchange on the clarified urea solution at a flow rate of 8m3 / h to obtain a pure urea solution;

[0043] (5) Mixing: Mix the pure urea solution with the above-mentioned ethanol, N-methylsuccinamide and PEG-3 stearate at a speed of 300r / min for 15 minutes to obtain the v...

Embodiment 3

[0048] A preparation method for vehicle urea solution, comprising the following steps:

[0049] (1) Ingredients: Weigh 30kg of agricultural urea, 80kg of high-purity water, 8kg of ethanol, 7kg of N-methylsuccinamide and 2kg of PEG-5 stearate;

[0050] (2) Dissolving: Mix the above-mentioned urea and high-purity water in parts by weight, and stir for 20 minutes at a temperature of 60°C and a rotation speed of 500r / min to obtain a urea solution;

[0051] (3) Adsorption and impurity removal: Add 5 kg of cellulose xanthate adsorbent to the above urea solution, continue to stir for 20 minutes, and then filter to remove solid impurities to obtain a clarified urea solution;

[0052] (4) Ion exchange: Perform ion exchange on the clarified urea solution at a flow rate of 10m3 / h to obtain a pure urea solution;

[0053](5) Mixing: Mix the pure urea solution with the above-mentioned ethanol, N-methylsuccinamide and PEG-5 stearate at a speed of 500r / min for 10 minutes to obtain the vehicl...

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PUM

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Abstract

The invention discloses a preparing method for a urea solution used for vehicles. The preparing method comprises the following steps that by weight, 20-35 parts of urea, 60-80 parts of high-purity water, 5-10 parts of ethanol, 4-7 parts of N-methylsuccinimide and 1-3 parts of polyoxyethylene stearate are weighed; urea and high-purity water are mixed and stirred, and a urea solution is obtained; a cellulose xanthate adsorbent is added into the urea solution, stirring and filtering are carried out, and a clarified urea solution is obtained; then ion exchange is carried out, and a purified urea solution is obtained; finally, the purified urea solution, ethanol, N-methylsuccinimide and polyoxyethylene stearate are stirred evenly, and the urea solution used for vehicles is obtained. The method has the advantages of being simple in preparing process, high in production efficiency, environmentally friendly, low in cost, remarkable in impurity removing effect and the like, and industrial production is easy to achieve.

Description

technical field [0001] The invention relates to the technical field of automobile tail gas treatment, in particular to a method for preparing a urea solution for automobiles. Background technique [0002] In recent years, air quality has continued to decline, and smog has become increasingly serious. Motor vehicle exhaust emissions account for about 20% to 25% of the causes of smog on average. At present, there are more than 57 million tons of pollutants emitted by motor vehicles every year in the country, including nitrogen oxides, hydrocarbons, carbon monoxide, and particulate matter. Among them, nitrogen oxides and particulate matter emitted by automobiles exceed 85%, and hydrocarbons and carbon monoxide exceed 70%. In addition, heavy-duty diesel vehicles, which account for less than 20 percent of the car population, emit about 60 percent of nitrogen oxides. Therefore, the control of motor vehicle emissions has become an increasingly urgent task. [0003] In the field o...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D53/94B01D53/56
CPCB01D53/9418B01D2258/012
Inventor 韦明
Owner NANNING XIAYANG CHEM TECH CO LTD
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