Nano material visible light degradation device as well as preparation method and degradation method thereof
A nanomaterial and visible light technology, applied in chemical instruments and methods, light water/sewage treatment, special compound water treatment, etc., can solve problems such as separation and secondary pollution, and achieve simple production process, reduced equipment cost, and convenient implementation. Effect
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[0031] The complete steps of the preparation method of the nanomaterial visible light degradation device of the present invention are as follows:
[0032] 1) Synthesis of nanomaterials
[0033] 1.1) Add 0.1 g of graphite oxide (10-500 nanometers) and sodium sulfite and cadmium chloride to 30-100 ml of distilled water in a molar ratio of 1: (1-3): (1-3), and stir for 10 After -30 minutes, heat to 100-110° C. until the reaction is complete, filter, and dry to obtain nanomaterials.
[0034] 1.2) Grinding the synthesized nanomaterials into fine powder.
[0035] 3) Gluing the nanomaterials to the glass tube of the visible light source.
[0036] 4) Visible light photocatalytic reaction device. Place a 5-15W long small lamp in a glass tube coated with nanomaterials, and then place the glass tube in a water sample glass container, and the reaction device is completed.
[0037] 5) When using the device, more visible light sources can be set outside the glass container to improve the...
Embodiment 1
[0041] The complete steps of the preparation method of the nanomaterial visible light degradation device of the present invention are as follows:
[0042] 1) Synthesis of nanomaterials
[0043] 1.1) Add 0.1 g of graphite oxide (10 nanometers) with sodium sulfite and cadmium chloride to 30 ml of distilled water in a molar ratio of 1:1:1, stir for 10-30 minutes and then heat to 100-110°C until the reaction After completion, filter and dry to obtain nanomaterials.
[0044] 1.2) Grinding the synthesized nanomaterials into fine powder.
[0045] 3) Gluing the nanomaterials to the glass tube of the visible light source.
[0046] 4) Visible light photocatalytic reaction device. Place a 5W long small lamp in a glass tube coated with nanomaterials, and then place the glass tube in a water-like glass container, and the reaction device is completed.
[0047] 5) When using the device, two 5W visible light sources can be installed outside the glass container to improve the photolysis eff...
Embodiment 2
[0049] The complete steps of the preparation method of the nanomaterial visible light degradation device of the present invention are as follows:
[0050] 1) Synthesis of nanomaterials
[0051] 1.1) Add 0.1g of graphite oxide (200nm) with sodium sulfite and cadmium chloride to 80ml of distilled water in a molar ratio of 1:2:2, stir for 10-30 minutes and heat to 100-110°C until the reaction After completion, filter and dry to obtain nanomaterials.
[0052] 1.2) Grinding the synthesized nanomaterials into fine powder.
[0053] 3) Gluing the nanomaterials to the glass tube of the visible light source.
[0054] 4) Visible light photocatalytic reaction device. Place a 10W long small lamp in a glass tube coated with nanomaterials, and then place the glass tube in a water-like glass container, and the reaction device is completed.
[0055] 5) When using the device, three 5W visible light sources can be installed outside the glass container to improve the photolysis efficiency.
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