Preparing technology of copper-based powder metallurgy material
A technology of powder metallurgy and preparation process, which is applied in the field of preparation process of copper-nickel powder metallurgy materials, which can solve the problems affecting the performance of materials, insufficient hardness and strength, etc., achieve high hardness and strength, reduce segregation, and refine the structure.
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[0021] The preparation technology of copper-based powder metallurgy material, it comprises the following steps:
[0022] Aluminum, copper and nickel particles are used as raw materials, and the content of nickel is 10wt%, the content of aluminum is 1-2 wt%, and the balance is copper; then the aluminum particles are placed in the induction heating furnace, and the aluminum particles are dissolved Finally, copper and nickel particles are added for smelting, and the scum is removed after the dissolution to obtain the alloy liquid; the alloy liquid is dropped onto the surface of the high-speed rotating copper wheel and thrown out, and the alloy strip is obtained by cooling; the alloy strip is soaked in 10% Hydrochloric acid for a few minutes to remove the oxide layer on the surface of the alloy strip, and rinsed with distilled water and anhydrous ethanol for several times, and then dried in a vacuum drying oven; cut the dried alloy strip, and then ball milled to obtain alloy powder...
Embodiment 1
[0027] Put 1wt% aluminum grains in an induction heating furnace, add 89wt% copper grains and 10wt% nickel grains for melting after the aluminum grains are dissolved, remove the scum after the dissolution, and obtain the alloy liquid; drop the alloy liquid into a high-speed rotating The surface of the red copper wheel is thrown out, cooled to obtain alloy strips; the alloy strips are soaked in 10% hydrochloric acid for several minutes, rinsed with distilled water and anhydrous ethanol for several times, and then dried in a vacuum drying oven; then cut and dried The final alloy strip was ball-milled for 18 hours with a ball-to-material ratio of 4.5:1 to obtain alloy powder; the alloy powder was placed in a graphite mold, first sintered at 280°C for 30s, then at 500°C for 60s, and then at 650°C Sintering at ℃ for 30s; followed by solution treatment at 650℃ for 12min; followed by cold deformation treatment with a cold deformation of 30%; and finally aging treatment at 300℃ for 3h t...
Embodiment 2
[0029] Put 1.5 wt% aluminum particles in an induction heating furnace, add 88.5 wt% copper particles and 10wt% nickel particles for melting after the aluminum particles are dissolved, remove the scum after the dissolution, and obtain the alloy liquid; drop the alloy liquid to The surface of the high-speed rotating red copper wheel is thrown out and cooled to obtain the alloy strip; the alloy strip is soaked in 10% hydrochloric acid for several minutes, rinsed with distilled water and anhydrous ethanol for several times, and then dried in a vacuum oven; then Cut the dried alloy strips, and then use ball-to-material ratio of 4.5:1 to ball mill for 20 hours to obtain alloy powder; place the alloy powder in a graphite mold, sinter at 300°C for 25s, then sinter at 560°C for 50s, Sintering at 680°C for 25s; followed by solution treatment at 680°C for 11 minutes; followed by cold deformation treatment with a cold deformation of 32%; and finally aging treatment at 330°C for 2.5 hours t...
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