Three-dimensional "photo frame and photo" structure nano gold material, its synthesis method and application
A synthesis method, nano-gold technology, applied in the direction of nanotechnology, nanotechnology, nanotechnology for materials and surface science, etc., can solve problems such as difficult to obtain discontinuous shell structure with controllable morphology, and achieve good application Effects of foreground, ease of handling, unique optical properties
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[0032] (1) Preparation of gold nanoparticles with different morphologies
[0033] Gold nanoparticles with different morphologies, such as spherical, rod-shaped, and cubic-shaped, can be used as modified crystal nuclei to prepare photo-frame structured nanoparticles with different morphologies.
[0034] Wherein, gold nanoparticles can be synthesized by any method known in the industry.
[0035] Taking a synthesis process of gold nanorod nuclei as an example, the preparation process of nano gold seeds includes: 10mL of 5×10 -4 M of HAuCl4 solution was added to 10 mL of 0.2 M CTAB solution, and then 1.2 mL of ice-cold NaBH 4 The solution (0.01M) was quickly added to the above mixed solution, and stirred vigorously for 2 min. Stand at room temperature for at least 10 minutes before use. Preparation of gold ion growth solution: 4mL of HAuCl 4 (0.01M) and 0.8mL AgNO 3 Add the solution (0.01M) into 80mL of CTAB solution (0.1M) and mix well, add 0.64mL of ascorbic acid solution (...
Embodiment 1
[0045] (1) Preparation of rod-shaped gold nanoseeds (gold nanorods)
[0046]Preparation of nano-gold seeds: 10 mL of 5 × 10 -4 M of HAuCl4 solution was added to 10 mL of 0.2 M CTAB solution, and then 1.2 mL of ice-cold NaBH 4 The solution (0.01M) was quickly added to the above mixed solution, and stirred vigorously for 2 min. Stand at room temperature for at least 10 minutes before use. Preparation of gold ion growth solution: 4mL of HAuCl 4 (0.01M) and 0.8mLAgNO 3 Add the solution (0.01M) into 80mL of CTAB solution (0.1M) and mix well, add 0.64mL of ascorbic acid solution (0.1M) into the growth solution, stir and mix evenly, add 1.6mL of 1.0M dilute hydrochloric acid solution to adjust the growth The pH of the liquid. Then, 0.02 mL of nano-gold seed solution was quickly added to the growth solution, stirred for 10 s, and left at room temperature for 6 h to prepare gold nanorod particles. Centrifuge at 8000 rpm for 10 min, and redisperse the precipitated gold nanorods in...
Embodiment 2
[0054] (1) Preparation of cubic gold nanoseeds (gold nanocubes)
[0055] Preparation of cubic gold nanoparticles: 0.25mL of 0.01M HAuCl4 solution was added to 7.5mL of 0.1MCTAB solution, and then 0.6mL of ice-cold NaBH4 solution (0.01M) was quickly added to the above mixed solution and stirred vigorously for 2min. Let stand at room temperature for at least 1 hour before use. Preparation of gold ion growth solution: Add 0.8mL of HAuCl4 (0.01M) and 6.4mL of CTAB solution (0.1M) into 32mL of deionized water and mix thoroughly, and add 3.8mL of ascorbic acid solution (0.1M) into the growth solution , stir to mix well. Then 0.02 mL of nano-gold seed solution was quickly added to the growth solution, stirred for 10 s, and left at room temperature for 6 h to obtain cubic gold nanoparticles. Centrifuge at 8000 rpm for 10 min, and redisperse the precipitated gold nanoparticles in deionized water for later use.
[0056] (2) Preparation of gold-silver nanoparticles with core-shell str...
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