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Reclaimed rubber prepared from oil field oil sludge and production method thereof

A technology of reclaimed rubber and oil sludge, which is applied in the field of reclaimed rubber, can solve the problems of small amount of oilfield sludge used, high production cost of reclaimed rubber, and large amount of miscellaneous rubber powder, so as to reduce solid waste discharge, improve the quality of reclaimed rubber, and reduce consumption. The effect of dosage increase

Inactive Publication Date: 2016-12-07
青岛三聚猫环保能源科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

First, the consumption of oil sludge is low. The mass fraction of oilfield sludge used in the production of reclaimed rubber is 40-50%. The amount of oilfield sludge used is small, resulting in low sludge consumption, which is not conducive to the application of this technology in the oilfield sludge treatment industry. promotion; second, the amount of miscellaneous rubber powder is large, and the production cost of reclaimed rubber is high

Method used

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  • Reclaimed rubber prepared from oil field oil sludge and production method thereof

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0044] For the reclaimed rubber prepared from oilfield oil sludge provided in this example, the mass percent composition of the raw material formula is:

[0045] Oily sludge: 63.1%;

[0046] Waste tire rubber powder: 15.1%;

[0047] Clay: 21.1%;

[0048] Activator 420: 0.2%;

[0049] Ethylene tar: 0.3%;

[0050] Alkylphenol disulfides: 0.2%.

[0051] The production method of the reclaimed rubber prepared from the oilfield oil sludge comprises the steps of:

[0052] S1: Oilfield sludge pretreatment

[0053] Remove the gravel impurities in oilfield oil sludge to obtain oily sludge;

[0054] S2: Preparation of reclaimed rubber by reaction

[0055] The reaction kettle is preheated in advance to 220°C, and the raw material oily sludge, waste tire rubber powder, and clay are first added to the reaction kettle, and mixed evenly, and then the activator 420, ethylene tar, and alkylphenol disulfide are put into the reaction kettle After mixing evenly, close the reactor, and react ...

Embodiment 2

[0059] For the reclaimed rubber prepared from oilfield oil sludge provided in this example, the mass percent composition of the raw material formula is:

[0060] Oily sludge: 57.6%;

[0061] Waste tire rubber powder: 8.5%;

[0062] Clay: 33.5%;

[0063] Activator 420: 0.12%;

[0064] Ethylene tar: 0.17%;

[0065] Alkylphenol disulfides: 0.11%.

[0066] The production method of the reclaimed rubber prepared from the oilfield oil sludge comprises the steps of:

[0067] S1: Oilfield sludge pretreatment

[0068] Remove the gravel impurities in oilfield oil sludge to obtain oily sludge;

[0069] S2: Preparation of reclaimed rubber by reaction

[0070] The reaction kettle is preheated in advance to 220°C, and the raw material oily sludge, waste tire rubber powder, and clay are first added to the reaction kettle, and mixed evenly, and then the activator 420, ethylene tar, and alkylphenol disulfide are put into the reaction kettle After mixing evenly, close the reactor, and re...

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Abstract

The invention belongs to the field of oil field oil sludge resourceful treatment, especially discloses reclaimed rubber prepared from oil field oil sludge as a main raw material, and also discloses a production method. The reclaimed rubber prepared from the oil field oil sludge is composed of the raw materials by the mass percentage: 50%-65% of oily sludge, 5%-20% of a waste tire rubber powder, 20%-40% of clay, 0.1%-0.4% of an activator 420, 0.1%-0.3% of ethylene tar, and 0.1%-0.3% of alkyl phenol disulfide. According to the reclaimed rubber prepared with oil field oil sludge, through formula optimization design, the content of the oily sludge is increased significantly, the consumption of the oil field sludge is increased, and the oil field oil sludge resourceful treatment effect is increased by 20% or more; with use of the waste tire rubber powder, the use amount is only 5%-20% and is significantly reduced, and the production cost is saved; the reclaimed rubber has relatively short reclaiming reaction time and has high degree of desulfurization, and the reclaimed rubber properties all reach national corresponding reclaimed rubber standards.

Description

technical field [0001] The invention relates to the technical field of oilfield oil sludge resource treatment, in particular to a reclaimed rubber prepared from oilfield oil sludge as a main raw material, and also relates to a production method thereof. Background technique [0002] Oilfield oil sludge or oil sludge mainly refers to a large amount of oily solid waste produced in the process of petroleum exploration, development and smelting. At present, my country has listed oil sludge as oily waste in the National Catalog of Hazardous Wastes. [0003] The treatment and disposal of oilfield oil sludge is a major scientific problem in the world. At the same time, the "National Cleaner Production Promotion Law" and "Solid Waste Environmental Pollution Prevention Law" require that oil sludge must be treated in a harmless manner. According to the State Council of the People's Republic of China No. 369 "Regulations on the Collection and Use of Sewage Discharge Fees" (implemented...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08J11/28C08J11/18C08J11/16C08L17/00
CPCC08J11/16C08J11/18C08J11/28C08J2317/00C08L17/00Y02W30/62
Inventor 毛亚宁
Owner 青岛三聚猫环保能源科技有限公司
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