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Flufenacet water-dispersible granule and preparation method thereof

A technology of flufenacet and dispersible granules, which is applied in the field of pesticide preparations and its preparation, can solve problems such as difficulty in making, difficult to granulate, and low melting point of flufenacet, and achieve rapid disintegration, qualified stability, and improved Effect of disintegration and suspension properties

Inactive Publication Date: 2016-12-14
江苏省农用激素工程技术研究中心有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The purpose of the present invention is to overcome the problems of low melting point of flufenacet, difficulty in granulation, and difficulty in making water-dispersible granules, and provide a kind of flufenacet water-dispersible granules with good disintegration performance and suspension performance and its Preparation

Method used

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  • Flufenacet water-dispersible granule and preparation method thereof
  • Flufenacet water-dispersible granule and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1)

[0022] The flufenacet water-dispersible granules of the present embodiment are made of the following components in percentage by weight:

[0023] 60% flufenacet technical product, 4% sodium sulfate of alkylphenol polyoxyethylene ether formaldehyde condensate as wetting agent, 6% sodium salt of alkylnaphthalene sulfonic acid formaldehyde condensate as dispersant, 2 % of ammonium sulfate as a disintegrant, 8% of kaolin as a solid carrier and 20% of cornstarch as a solid carrier.

[0024] The above-mentioned flufenacet technical source comes from Jiangsu Provincial Agricultural Hormone Engineering Technology Research Center Co., Ltd., and its purity meets the relevant quality requirements; the above-mentioned sodium sulfate of alkylphenol polyoxyethylene ether formaldehyde condensate used as a wetting agent comes from Solvay The above-mentioned sodium salt of alkylnaphthalenesulfonic acid formaldehyde condensate as a dispersant comes from Akzo Nobel Auxiliary Company; the above-m...

Embodiment 2~ Embodiment 5)

[0033] The preparation method of each embodiment is the same as that of the examples, except that each component and its weight percentage are the same, see Table 1 for details:

[0034] Table 1

[0035]

[0036] In Table 1, sodium alkylnaphthalene sulfonate as a wetting agent and sodium polycarboxylate as a dispersant all come from Huntsman Auxiliary Company, and the source of other components is the same as that in Example 1.

experiment example )

[0038] Detect the relevant performance index of the water-dispersible granule that each embodiment makes, and the results are shown in Table 2:

[0039] Table 2

[0040]

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Abstract

The invention discloses a flufenacet water-dispersible granule and a preparation method thereof. The flufenacet water-dispersible granule is prepared from the following components by weight: 10 to 80% of crude flufenacet, 2 to 6% of a wetting agent, 4 to 15% of a dispersing agent and 0 to 10% of a disintegrating agent, with the balance being a solid carrier, wherein the wetting agent is alkylphenol polyoxyethylene formaldehyde condensate sulfate and / or alkyl naphthalene sulfonat, and the dispersing agent is alkyl naphthalene sulfonic acid-formaldehyde condensate sodium salt and / or polycarboxylate. The water-dispersible granule is rapid in disintegration, has a suspension rate of no less than 85%, a pH value (1% aqueous solution) of 6.0 to 8.0, a wet sieve passing rate of no less than 8% and a lasting foamability index of no more than 40 mL of foam in 1 min, and has qualified stability after hot storage at 45 DEG C for 45 days.

Description

technical field [0001] The invention relates to a pesticide preparation and a preparation method thereof, in particular to a flufenacet water-dispersible granule and a preparation method thereof. Background technique [0002] Water-dispersible granules, also known as dry suspension concentrates or granular wettable powders, can disintegrate quickly in water to form a high-suspension dispersion system. It has the following advantages: ① No dust, safe for operators; ② Stable physical and chemical properties, especially for pesticides that are unstable in water; ③ Good fluidity, easy to pack, and easy to measure; ④ High active ingredients, dispersed in water Good performance. [0003] The chemical name of flufenacet is 4'-fluoro-N-isopropyl-2-[5-(trifluoroglycoside)-1,3,4-thiadiazo-2-imine]acetamide, which belongs to aromatic Acetamide compounds have a similar weed control spectrum to chloroacetamide herbicides, and can extensively control annual grass weeds, sedges and small...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N43/824A01N25/14A01P13/00
CPCA01N43/82A01N25/14A01N2300/00
Inventor 孔繁蕾李娟
Owner 江苏省农用激素工程技术研究中心有限公司