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Method for identifying chuanxiong rhizomes in far-reaching tonic wine

A technology of Shiquan Dabu wine and Chuanxiong, which is applied in the field of traditional Chinese medicine detection, to achieve the effect of good reproducibility, strong specificity and strong controllability

Inactive Publication Date: 2017-01-04
GUIZHOU XINBANG PHARMACEUTICAL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the existing quality standard of Shiquan Dabu wine, the identification of Chuanxiong is not involved. Therefore, to study a method that is easy to operate and can accurately identify Chuanxiong in Shiquan Dabu wine will help improve the quality of Shiquan Dabu wine It is especially necessary to test the standard

Method used

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  • Method for identifying chuanxiong rhizomes in far-reaching tonic wine
  • Method for identifying chuanxiong rhizomes in far-reaching tonic wine
  • Method for identifying chuanxiong rhizomes in far-reaching tonic wine

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Experimental program
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Effect test

Embodiment 1

[0045] The identification method of Rhizoma Chuanxiong in Shiquan Dabu wine comprises the following steps:

[0046] (1) Preparation of the test solution: Take 25 mL of this product, add 40 mL of diethyl ether and shake to extract, obtain the diethyl ether solution, evaporate to dryness, add 2 mL of methanol to the residue to dissolve it, and use it as the test solution;

[0047] (2) Preparation of the reference drug solution: take 1 g of the Rhizoma Chuanxiong reference drug, add 25 mL of ether, heat and reflux for 1.5 h, filter, evaporate the filtrate to dryness, add 2 mL of methanol to the residue to dissolve it, and use it as the reference drug solution;

[0048] (3) Preparation of reference substance solution: take the reference substance of angelica lactone A and place it in a brown bottle, add methanol to make a solution containing 0.1 mg of angelica lactone A reference substance per 1 mL, as the reference substance solution;

[0049] (4) Identification: According to the...

Embodiment 2

[0051] The identification method of Rhizoma Chuanxiong in Shiquan Dabu wine comprises the following steps:

[0052] (1) Preparation of the test solution: Take 30 mL of this product, add 50 mL of diethyl ether and shake and extract to obtain a diethyl ether solution, evaporate to dryness, add 3 mL of methanol to the residue to dissolve it, and use it as the test solution;

[0053] (2) Preparation of the reference drug solution: take 1 g of the reference drug of Rhizoma Chuanxiong, add 30 mL of ether, heat and reflux for extraction for 2 hours, filter, evaporate the filtrate to dryness, add 2 mL of methanol to the residue to dissolve it, and use it as the reference drug solution;

[0054] (3) Preparation of reference substance solution: take the reference substance of angelica lactone A and place it in a brown bottle, add methanol to make a solution containing 0.1 mg of angelica lactone A reference substance per 1 mL, as the reference substance solution;

[0055] (4) Identificat...

Embodiment 3

[0057] The identification method of Rhizoma Chuanxiong in Shiquan Dabu wine comprises the following steps:

[0058] (1) Preparation of the test solution: take 20mL of this product, add 30mL of diethyl ether and shake and extract to obtain diethyl ether, evaporate to dryness, add 1mL of methanol to the residue to dissolve it, and use it as the test solution;

[0059] (2) Preparation of the reference medicinal material solution: take 1 g of the Rhizoma Chuanxiong reference medicinal material, add 20 mL of ether, heat and reflux for extraction for 1 hour, filter, evaporate the filtrate to dryness, add 2 mL of methanol to the residue to dissolve it, and use it as the reference medicinal material solution;

[0060] (3) Preparation of reference substance solution: take the reference substance of angelica lactone A and place it in a brown bottle, add methanol to make a solution containing 0.1 mg of angelica lactone A reference substance per 1 mL, as the reference substance solution; ...

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Abstract

The invention discloses a method for identifying chuanxiong rhizomes in far-reaching tonic wine. The method is a thin layer chromatography method that chuanxiong rhizome reference medicine materials and European angelica lactone A reference products are adopted as reference, and the ratio of normal hexane to ethyl acetate is (3-6):(1-2). The method for identifying the chuanxiong rhizomes in the far-reaching tonic wine is easy to operate and high in controllability, and the chuanxiong rhizome ingredient in the far-reaching tonic wine can be efficiently identified. The method is high in separation degree, good in reproducibility, high in specificity, high in sensitivity and good in stability, feminine reference is free of interference, and thin layer plates of different factories and the temperature and humidity conditions all have no influence. According to the method for identifying chuanxiong rhizomes in the far-reaching tonic wine, the chuanxiong rhizome ingredient in the far-reaching tonic wine can be identified accurately, comprehensively, scientifically and effectively, the quality detection standard is improved, and the stability, safety and effectiveness of product quality are further ensured.

Description

technical field [0001] The invention relates to a method for identifying Rhizoma Chuanxiong in Shiquan Dabu wine, and specifically belongs to the technical field of traditional Chinese medicine detection. Background technique [0002] Shiquan Dabu wine is made from Codonopsis pilosula, Atractylodes macrocephala (stir-fried), Poria cocos, licorice (honey-roasted), angelica, Chuanxiong, white peony (stir-fried), rehmannia glutinosa, astragalus (honey-roasted) and cinnamon. The auxiliary materials are liquor and sucrose. The function of this product is to warm and invigorate qi and blood. Rehmannia glutinosa nourishes blood and nourishes yin, replenishes essence and produces marrow; Codonopsis pilosula nourishes spleen and invigorates the middle, nourishes qi and produces blood, yang produces yin and grows, and it is a king medicine. Atractylodes invigorates the spleen and qi; Poria cocos invigorates the spleen and dampness; Astragalus invigorates the spleen and invigorates q...

Claims

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Application Information

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IPC IPC(8): G01N30/90
CPCG01N30/90
Inventor 包雪爱
Owner GUIZHOU XINBANG PHARMACEUTICAL CO LTD
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