Multiplex load type silicon-based phosphorus removal agent, and preparation method and application thereof
A base phosphorus removal agent and load-type technology, which is applied in chemical instruments and methods, adsorbed water/sewage treatment, water pollutants, etc. Increase the porosity and specific surface area, and avoid the effect of water turbidity and yellowing
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Embodiment 1
[0047] The multi-loaded silicon-based phosphorus removal agent provided in this example is prepared through the following steps:
[0048] (1) Activate the attapulgite clay dissolved in water under alkaline conditions; specifically, after dissolving the attapulgite clay in water, adjust the pH to 8 with 10% NaOH solution, and activate it for 1 hour under continuous stirring;
[0049] When dissolving the attapulgite clay, in parts by mass, the consumption of attapulgite clay is 10 parts, and the consumption of water is 44 parts;
[0050] (2) Adjust the activated attapulgite clay aqueous solution in step (1) to be acidic, so that iron sulfate is loaded on the attapulgite clay; specifically, adjust the pH of the activated attapulgite clay aqueous solution in step (1) to 2 After that, add ferric sulfate powder and continue to stir for 1h;
[0051] (3) Under heating conditions, polyvinylpyrrolidone is added to the solution system in step (2) to form a stable dispersion system; spec...
Embodiment 2
[0057] The preparation method of the multi-loaded silicon-based phosphorus removal agent provided in this example is the same as in Example 1, except that the activation time in step (1) is adjusted to 2 hours.
[0058] When it is used for precipitating phosphorus in sewage, it is added according to the mass ratio of one ten-thousandth of the water sample in the same way as in the comparative example. The test results show that the supernatant at 2 cm below the liquid surface is clear and colorless, and the total phosphorus content in the water sample after phosphorus removal is 0.91mg / L, so the phosphorus removal efficiency is 90.9%.
Embodiment 3
[0060] The preparation method of the multi-loaded silicon-based phosphorus removal agent provided in this example is the same as in Example 1, except that the activation time in step (1) is adjusted to 3 hours.
[0061] When it is used for precipitating phosphorus in sewage, it is added according to the mass ratio of one ten-thousandth of the water sample in the same way as in the comparative example. The test results show that the supernatant at 2 cm below the liquid surface is clear and colorless, and the total phosphorus content in the water sample after phosphorus removal is 0.98mg / L, so the phosphorus removal efficiency is 90.2%.
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