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Multistage extraction unit for animal and plant raw materials, and method and application thereof

An extraction device, animal and plant technology, applied in separation methods, chemical instruments and methods, solvent extraction, etc., can solve the problems of difficult extraction, low extraction efficiency, large volume, etc., and achieve high crushing efficiency and filtration efficiency. and the effect of improving leaching efficiency and improving leaching efficiency

Inactive Publication Date: 2017-02-01
王芹
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The applicant found in the research that the existing extraction device has the following problems: First, the yield of the active ingredient in the existing extraction device is low, the extraction efficiency is low, and it is difficult to extract the active ingredient in the plant by tableting or centimeter-level coarse crushing. Leaching into the solvent, and the method of spraying the solvent is difficult to fully extract, and the extraction efficiency of the obtained active ingredients is low
Secondly, although the existing technology involves the design of extracting plant raw materials using membrane separation devices, the permeate obtained by primary filtration is often separated and refined with a filter membrane with a smaller pore size to obtain specific chemical components (such as protein separation), but there is no help on how to increase the yield of active ingredients
Again, the applicant found that using the existing membrane extraction device, the obtained permeate has a low concentration and a large volume, which not only increases the cost of the solvent, but also increases the subsequent energy consumption for refining and concentrating the permeate.

Method used

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  • Multistage extraction unit for animal and plant raw materials, and method and application thereof
  • Multistage extraction unit for animal and plant raw materials, and method and application thereof
  • Multistage extraction unit for animal and plant raw materials, and method and application thereof

Examples

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Embodiment 1

[0039] refer to figure 1 , the multi-stage extraction device for animal and plant raw materials includes an extraction tank 1, a membrane filter 2, a pulverizer 3 and a concentrated liquid membrane separation device, and the extraction tank 1 is connected to the pulverizer 3 through a raw material delivery pipe 101 1. The first pump 4 is connected to the inlet pipeline of the membrane filter 2, and the permeate outlet of the membrane filter 2 is connected to the permeate output pipe 201; The liquid return pipe 202 is connected with the extraction tank 1 and connected with the concentrated liquid membrane separation device through the concentrated liquid delivery pipe 203 . The concentrated liquid separation device comprises a leaching tank 5 and a filter membrane separator 6, the leaching tank 5 is connected with the inlet pipeline of the filter membrane separator 6 by a second pump 7, and the concentrated solution outlet of the filter membrane separator 6 is connected to the ...

Embodiment 2

[0043] refer to figure 2 , this embodiment includes the above structure, the difference between this embodiment and embodiment 1 is: there are multiple concentrated liquid membrane separation devices, and the multiple concentrated liquid membrane separation devices are along the concentrated liquid conveying direction, from the upper level to the lower level It is arranged in multiple stages, and the adjacent concentrated liquid membrane separation devices are connected through the concentrated liquid feeding pipe 601 and the permeate liquid feeding pipe 602 respectively; in the adjacent concentrated liquid membrane separation devices: the lower concentrated liquid The permeate outlet of the membrane separation device is connected to the leaching tank 5 of the upper concentrated liquid membrane separation device through a countercurrent pipeline 603 .

[0044] There are various designs for the solvent replenishment tube 501: refer to figure 2 , it can be designed that only ...

Embodiment 3

[0047] refer to image 3 , the present embodiment except including all structures of embodiment 2, difference is: comprise solvent storage tank 8, extraction tank 1 is connected with solvent storage tank 8 through solvent delivery pipe 102, is provided with temperature regulator 103 on the solvent delivery pipe 102 and valves. It includes a solvent supplement tank 9, the liquid inlet end of the solvent supplement pipe 501 is connected to the solvent supplement tank 9, and the solvent supplement pipe 501 is provided with a temperature regulator 502 and a valve. Including the permeate return pipe 204, the permeate outlet of the membrane filter 2 is connected to the extraction tank 1 through the permeate return pipe 204, and the permeate return pipe 204 can return the low-concentration permeate to the extraction tank 1, until the permeate concentration reaches a higher value, the permeate return pipe 204 is closed, and the high-concentration permeate is discharged from the perme...

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Abstract

The invention relates to a multistage extraction unit for animal and plant raw materials, and a method and application thereof, belonging to the technical field of animal and plant extraction. The extraction unit comprises an extraction tank (1), a filtration membrane filter (2), a pulverizer (3) and a concentrated solution membrane separation device, wherein the extraction tank (1) is connected with the pulverizer (3) through a raw material delivery pipe (101), and connected with a feed port of the filtration membrane filter (2) through a first pump (4) via a pipeline; a filtrate outlet of the microfiltration membrane filter (2) is connected with a filtrate output pipe (201); and a concentrated solution outlet of the filtration membrane filter (2) is respectively connected with the extraction tank (1) through a concentrated solution return pipe (202) and connected with the concentrated solution membrane separation device through a concentrated solution delivery pipe (203). The extraction unit can pulverize the raw materials into fine powder and perform membrane separation extraction, has the advantages of high extraction efficiency and high yield, and is capable of obviously enhancing the concentration of the obtained filtrate, reducing the solvent consumption and lowering the production cost.

Description

technical field [0001] A multi-stage extraction device for animal and plant raw materials and its method and application belong to the technical field of animal and plant extraction. Background technique [0002] Extraction of animal and plant raw materials refers to the use of appropriate solvents or methods to extract and process active ingredients (the active ingredients can be dissolved in solvents) from animal and plant raw materials (all or a certain part). In the existing large-scale industrial production, the method of extracting active ingredients from animal and plant raw materials is to dry and compress the animal and plant raw materials to obtain flake raw materials, and spray the flake raw materials with solvent to obtain the extract. Alternatively, the animal and plant raw materials are crushed into centimeter-sized particles and added to a solvent (such as ethanol solution) for hot reflux extraction. When separating the solid-liquid of the extract, a centimete...

Claims

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Application Information

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IPC IPC(8): B01D11/02
CPCB01D11/0284B01D11/0292B01D11/0257
Inventor 不公告发明人
Owner 王芹
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