Method for preparing high-strength high-plasticity aluminum-based composite material
An aluminum-based composite material and composite material technology, which is applied in the field of preparing high-strength and high-plastic aluminum-based composite materials, can solve the problems of low cost, strength and plasticity at the same time, and achieve strength and plasticity improvement and fine grain structure Effect
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Embodiment 1
[0033] In the experiment, high-purity Al, industrial pure Mg, industrial pure Zn, Al-50Cu, Al-12Zr master alloy, KBF 4 and K 2 TiF 6 In situ autogenous 5 wt.% TiB was formulated for the raw material 2 Reinforced Al-6.7Zn-2.2Mg-2.3Cu-0.1Zr alloy composites. First, put high-purity Al into the crucible to melt and heat up to 780 ℃, cover with JZF-03 high-temperature covering agent; 4 , K 2 TiF 6 After uniform mixing at a mass ratio of 1:2, drying is added to the melt obtained in step (1); after the reaction is completed, the reaction by-product is taken out, and Al-50Cu, Al-12Zr master alloy alloy and industrial pure Mg are added in sequence And industrial pure Zn, add JZJ type harmless aluminum alloy refining agent to the melt for degassing and refining, let it stand at 750 ℃ for 15min, and then pour it into a casting mold at 730 ℃ to form a casting billet. 5wt.% TiB obtained by casting 2 The reinforced Al-6.7Zn-2.2Mg-2.3Cu-0.1Zr alloy composites were subjected to homog...
Embodiment 2
[0035] In the experiment, high-purity Al, industrial pure Mg, industrial pure Zn, Al-50Cu, Al-12Zr master alloy, KBF 4 and K 2 TiF 6 In situ autogenous 5 wt.% TiB was formulated for the raw material 2 Reinforced Al-6.6Zn-2.2Mg-2.2Cu-0.09Zr alloy composites. First, put high-purity Al into the crucible to melt and heat up to 780 ℃, cover with JZF-03 high-temperature covering agent; 4 , K 2 TiF 6 After uniform mixing at a mass ratio of 1:2, drying is added to the melt obtained in step (1); after the reaction is completed, the reaction by-product is taken out, and Al-50Cu, Al-12Zr master alloy alloy and industrial pure Mg are added in sequence And industrial pure Zn, add JZJ type harmless aluminum alloy refining agent to the melt for degassing and refining, let it stand at 750 ℃ for 15min, and then pour it into a casting mold at 730 ℃ to form a casting billet. 5wt.% TiB obtained by casting 2 The reinforced Al-6.7Zn-2.2Mg-2.3Cu-0.1Zr alloy composites were subjected to homo...
Embodiment 3
[0037] A method for preparing high-strength and high-plastic aluminum-based composite materials, through the method of in-situ autogenous melt control, to prepare as-cast TiB 2 Particle-reinforced Al-8Zn-2.5Mg-2Cu-0.2Zr alloy composite material, and then using self-designed orthogonal lamination extrusion equipment to achieve in-situ self-generated TiB 2 Large plastic deformation of multi-pass orthogonal lamination extrusion of particle-reinforced Al-8Zn-2.5Mg-2Cu-0.2Zr alloy composites to obtain uniformly dispersed micro-nano TiB 2 Grain and fine equiaxed matrix grain structure, combined with T6 heat treatment of Al-8Zn-2.5Mg-2Cu-0.2Zr alloy, prepared TiB with high strength and high plasticity at the same time 2 Particle-reinforced Al-8Zn-2.5Mg-2Cu-0.2Zr alloy composites.
[0038] The structure of the cross-laminate extrusion equipment used is as follows: figure 1 As shown, it includes an upper indenter 1, a die barrel 2 and a die head 3. The middle of the die barrel 2 is p...
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