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Method for preparing high-strength high-plasticity aluminum-based composite material

An aluminum-based composite material and composite material technology, which is applied in the field of preparing high-strength and high-plastic aluminum-based composite materials, can solve the problems of low cost, strength and plasticity at the same time, and achieve strength and plasticity improvement and fine grain structure Effect

Active Publication Date: 2017-02-01
SHANGHAI JIAO TONG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] Aiming at the problem that the strength and plasticity of the particle-reinforced aluminum-matrix composite cannot be obtained at the same time, the present invention proposes a method for in-situ production of micro-nano particle-reinforced aluminum-matrix composite material, combined with large plastic deformation modification, to prepare a At the same time, it has high strength and high plasticity aluminum matrix composite material, and the process is simple and easy to operate, low cost and high efficiency, and can generate large size samples

Method used

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  • Method for preparing high-strength high-plasticity aluminum-based composite material

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] In the experiment, high-purity Al, industrial pure Mg, industrial pure Zn, Al-50Cu, Al-12Zr master alloy, KBF 4 and K 2 TiF 6 In situ autogenous 5 wt.% TiB was formulated for the raw material 2 Reinforced Al-6.7Zn-2.2Mg-2.3Cu-0.1Zr alloy composites. First, put high-purity Al into the crucible to melt and heat up to 780 ℃, cover with JZF-03 high-temperature covering agent; 4 , K 2 TiF 6 After uniform mixing at a mass ratio of 1:2, drying is added to the melt obtained in step (1); after the reaction is completed, the reaction by-product is taken out, and Al-50Cu, Al-12Zr master alloy alloy and industrial pure Mg are added in sequence And industrial pure Zn, add JZJ type harmless aluminum alloy refining agent to the melt for degassing and refining, let it stand at 750 ℃ ​​for 15min, and then pour it into a casting mold at 730 ℃ to form a casting billet. 5wt.% TiB obtained by casting 2 The reinforced Al-6.7Zn-2.2Mg-2.3Cu-0.1Zr alloy composites were subjected to homog...

Embodiment 2

[0035] In the experiment, high-purity Al, industrial pure Mg, industrial pure Zn, Al-50Cu, Al-12Zr master alloy, KBF 4 and K 2 TiF 6 In situ autogenous 5 wt.% TiB was formulated for the raw material 2 Reinforced Al-6.6Zn-2.2Mg-2.2Cu-0.09Zr alloy composites. First, put high-purity Al into the crucible to melt and heat up to 780 ℃, cover with JZF-03 high-temperature covering agent; 4 , K 2 TiF 6 After uniform mixing at a mass ratio of 1:2, drying is added to the melt obtained in step (1); after the reaction is completed, the reaction by-product is taken out, and Al-50Cu, Al-12Zr master alloy alloy and industrial pure Mg are added in sequence And industrial pure Zn, add JZJ type harmless aluminum alloy refining agent to the melt for degassing and refining, let it stand at 750 ℃ ​​for 15min, and then pour it into a casting mold at 730 ℃ to form a casting billet. 5wt.% TiB obtained by casting 2 The reinforced Al-6.7Zn-2.2Mg-2.3Cu-0.1Zr alloy composites were subjected to homo...

Embodiment 3

[0037] A method for preparing high-strength and high-plastic aluminum-based composite materials, through the method of in-situ autogenous melt control, to prepare as-cast TiB 2 Particle-reinforced Al-8Zn-2.5Mg-2Cu-0.2Zr alloy composite material, and then using self-designed orthogonal lamination extrusion equipment to achieve in-situ self-generated TiB 2 Large plastic deformation of multi-pass orthogonal lamination extrusion of particle-reinforced Al-8Zn-2.5Mg-2Cu-0.2Zr alloy composites to obtain uniformly dispersed micro-nano TiB 2 Grain and fine equiaxed matrix grain structure, combined with T6 heat treatment of Al-8Zn-2.5Mg-2Cu-0.2Zr alloy, prepared TiB with high strength and high plasticity at the same time 2 Particle-reinforced Al-8Zn-2.5Mg-2Cu-0.2Zr alloy composites.

[0038] The structure of the cross-laminate extrusion equipment used is as follows: figure 1 As shown, it includes an upper indenter 1, a die barrel 2 and a die head 3. The middle of the die barrel 2 is p...

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Abstract

The invention relates to a method for preparing a high-strength high-plasticity aluminum-based composite material. High-purity Al, industrial pure Mg, industrial pure Zn, Al-50Cu, Al-12Zr intermediate alloy, KBF<4> and K<2>TiF<6> serve as raw materials, and by the adoption of an in-situ melt synthesis control method, the in-situ TiB<2> micro-nano particle reinforced Al-Zn-Mg-Cu alloy composite material is prepared. The extrusion deformation direction of each pass is perpendicular to the extrusion direction of the last pass. Extrusion deformation is conducted in multi-pass orthorhombic laminated extrusion mold equipment, a large amount of accumulated shearing strain can be applied to the particle reinforced aluminum-based composite material, and then the mechanical stirring function is achieved. In-situ synthesis TiB<2> particle aggregates in the composite material are scattered, micro-nano TiB<2> particles are evenly dispersed and distributed in an aluminum matrix, Al-Zn-Mg-Cu matrix grain structures of the composite material can be refined, and even and fine isometric crystals are obtained. The aluminum-based composite material prepared through the method can achieve high strength and high plasticity simultaneously.

Description

technical field [0001] The invention belongs to the technical field of materials, and in particular relates to a method for preparing a high-strength and high-plasticity aluminum-based composite material. Background technique [0002] With the development of modern science and technology, the requirements for material properties in practical applications have become more stringent. Especially in high-end fields such as aerospace and weapon manufacturing, structural materials should have high specific stiffness and specific modulus while requiring high strength and high plasticity. It is difficult for traditional metal materials to meet such complex performance requirements. For example, although traditional steel materials have good strength and plasticity, their density is too high, which is not suitable for a large number of applications in aerospace and other fields that require high specific strength of components; and titanium alloys, although high in strength, Howeve...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C22C1/10C22C21/10C22C32/00C22F1/053
CPCC22C1/1036C22C21/10C22C32/0073C22F1/053C22C1/1052
Inventor 刘钧陈哲汪明亮吴一陈东钟圣怡王浩伟
Owner SHANGHAI JIAO TONG UNIV
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