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Electrolytic corrosive agent of industrial pure titanium TA2 and electrolytic polishing corrosion method

An industrial pure titanium and electropolishing technology, applied in the field of metallographic structure detection, can solve the problems of poor operation by new experimental operators and unsatisfactory corrosion effect of industrial pure titanium TA2, and achieve good erosion effect, good corrosion effect, and preparation. simple effect

Inactive Publication Date: 2017-02-15
AECC AVIATION POWER CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Generally speaking, for duplex titanium alloys, the effect of this corrosive agent is very good, but the corrosion effect for industrial pure titanium TA2 is not ideal, and its structure can only be seen when the sample is well ground and polished.
Artificial manual grinding and polishing requires operators to have good work experience to prepare, but it is not easy for new experimental operators to operate

Method used

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  • Electrolytic corrosive agent of industrial pure titanium TA2 and electrolytic polishing corrosion method
  • Electrolytic corrosive agent of industrial pure titanium TA2 and electrolytic polishing corrosion method
  • Electrolytic corrosive agent of industrial pure titanium TA2 and electrolytic polishing corrosion method

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Embodiment 1

[0035] The industrially pure titanium TA2 in the annealed state is inlaid with dental tray powder, and after curing, it is ground with 120#, 320#, 600# (1000#) sandpaper in sequence according to the preparation method of the metallographic sample. After replacing the sand paper, the grinding direction is perpendicular to the wear marks of the previous sand paper, and the wear marks of the previous process are removed. After grinding each type of sandpaper, the sample should be cleaned to avoid leaving the residual abrasive from the previous process in the next process, so as to protect the surface of the sample.

[0036] After grinding the sample, use No. 1 electrolytic corrosion agent (HF: 90ml, (NH 4 ) 2 S 2 o 8 : 10g, CH 3 CH 2 OH: 200ml, distilled water: 360ml) for electrolytic corrosion, electrolytic corrosion parameters are: polishing voltage: 50V, electrolyte flow rate: 20, electropolishing corrosion time 50s; corrosion voltage: 25V, electrolyte flow rate 20, corro...

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Abstract

The invention discloses an electrolytic corrosive agent of industrial pure titanium TA2 and an electrolytic polishing corrosion method, and belongs to the field of metallographic structure detection in an industrial pure titanium physical and chemical detection technology. The method comprises the following steps: 1) grinding and cleaning pretreated industrial pure titanium TA2 to prepare a to-be-corroded test sample; and 2) performing electrolytic polishing corrosion method on the surface of the to-be-corroded test sample by the electrolytic corrosive agent. The electrolytic corrosive agent is simple in preparation, good in corrosion effect and pollution-free; and the industrial pure titanium TA2 is subjected to metallographic examination, so that the microscopic structure of the industrial pure titanium TA2 can be displayed well, and the microstructure of the TA2, the form of alpha phase, the grain boundary and the like can be reflected objectively. The electrolytic polishing corrosion method is good in effect, stable in corrosion process, good in display effect of the microstructure of the test sample after corrosion, and high in operability.

Description

technical field [0001] The invention belongs to the field of metallographic structure detection in the physical and chemical detection technology of industrial pure titanium, and specifically relates to an electrolytic etchant and an electrolytic polishing corrosion method of industrial pure titanium TA2. Background technique [0002] Titanium and its alloys have been more and more used in the aerospace field, because their density is lighter than steel, but their mechanical strength is similar to that of steel, and they have good heat resistance, so they have attracted more and more attention. Titanium and its alloys are divided into α-titanium alloys, α-β two-phase titanium alloys and β-titanium alloys according to their stable phases at room temperature. In addition, there are two categories: near-α-titanium alloys and near-β-titanium alloys. For α-titanium alloys, there are difficulties in metallographic preparation, and industrial pure titanium is even more difficult to...

Claims

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Application Information

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IPC IPC(8): G01N1/32
CPCG01N1/32
Inventor 侯春梅李卫军胡锴董晓峰刘伟吴楠魏磊杨杰
Owner AECC AVIATION POWER CO LTD
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