A method of preparing a highly-sensitive type meat freshness degree detecting and indicating card through an electrostatic spinning process
A sensitive, acid-base indicator technology, applied in the field of nanoscience, can solve the problems of large amount of acid-base indicator, unstable indicator, volatile solvent, etc., to improve the indicator sensitivity, simple method, and large specific surface area. Effect
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Embodiment 1
[0041] The embodiment of the present invention provides a high-sensitivity meat freshness detection indicator card prepared by electrospinning. The preparation process is attached figure 1 Shown:
[0042] Step 101: Dissolve bromocresol violet in N,N-dimethylformamide (DMF) and stir until complete to obtain an acid-base indicator compound solution. Dissolve polylactic acid and polyvinylpyrrolidone with a mass ratio of 1:1 in an organic solvent (dichloromethane: N,N-dimethylformamide (DMF) = 6:1) to form a polymer with a mass fraction of 10%. spinning dope.
[0043] Step 102: Take an appropriate amount of acid-base indicator solution and add it to the polymer spinning stock solution, so that the ratio of the acid-base indicator to the total mass of the polymer is 1:19, stir until evenly mixed, and obtain a spinning solution doped with an acid-base indicator. silk liquid.
[0044] Step 103: Electrospinning to obtain a nanofiber film doped with an acid-base indicator, and asse...
Embodiment 2
[0049] Step 101: Dissolve methyl red and bromothymol blue with a mass ratio of 6:5 in N,N-dimethylformamide (DMF), and stir until complete to obtain an acid-base indicator compound solution. Polyacrylonitrile was dissolved in N,N-dimethylformamide (DMF) to prepare a polymer spinning dope with a mass fraction of 8%.
[0050] Step 102: Take an appropriate amount of acid-base indicator solution and add it to the polymer spinning stock solution, so that the ratio of the acid-base indicator to the total mass of the polymer is 1:19, and stir until it is evenly mixed to obtain a spinning solution doped with an acid-base indicator. silk liquid.
[0051] Step 103: Electrospinning to obtain a nanofiber membrane doped with an acid-base indicator.
[0052] The specific process of electrospinning is as attached figure 2 As shown, the spinning voltage is 10-15kV, the advancing speed is 1mL / h, and the receiving distance is 10-15cm. The electronic photo of the nanofiber membrane is attach...
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