Tourmaline ceramic loaded TiO2-NCP solid supported photocatalyst preparation process
A ceramic loading and photocatalyst technology, which is applied in physical/chemical process catalysts, metal/metal oxide/metal hydroxide catalysts, water/sewage treatment, etc., to achieve the effect of easy recycling and reuse
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Embodiment 1
[0039] The tourmaline ceramic supported TiO2 -The preparation technology of NCP immobilized photocatalyst comprises the following specific steps:
[0040] 1) Preparation of tourmaline ceramics
[0041] a. Cleaning, drying, pulverizing magnesium tourmaline, black tourmaline, lithium tourmaline and sodium manganese tourmaline, and processing it into 2000 mesh through Raymond machine or jet mill;
[0042] b. 6kg of polycrystalline tourmaline powder and 4kg of pottery clay were mixed and stirred for 60 minutes to form a uniform shape;
[0043] c. Slowly inject the water-soluble titanium hydroxide inorganic sol with a concentration of 0.85wt% into the beater according to the weight of 1:3, so that the tourmaline powder and clay form a solid state containing 30% water, and the titanium hydroxide inorganic sol is made of Titanium tetrachloride + 35% ammonia water + 50% hydrogen peroxide, after high-speed stirring, constant temperature and pressure, centrifugal separation, natural pr...
Embodiment 2
[0054] The tourmaline ceramic supported TiO 2 -The preparation technology of NCP immobilized photocatalyst comprises the following concrete steps:
[0055] 1) Preparation of tourmaline ceramics
[0056] a. cleaning, drying, pulverizing magnesium tourmaline, black tourmaline, lithium tourmaline and sodium manganese tourmaline, and processing it into 2200 mesh through Raymond machine or jet mill;
[0057] b. 6.5kg of polycrystalline tourmaline powder and 3.5kg of pottery clay were mixed and stirred for 60 minutes to form a uniform shape;
[0058] c. Slowly inject the water-soluble titanium hydroxide inorganic sol with a concentration of 0.87wt% into the beater according to the weight of 1:4, so that the tourmaline powder and clay form a solid state containing 30% of water, and the titanium hydroxide inorganic sol is made of Titanium tetrachloride + 35% ammonia water + 50% hydrogen peroxide, after high-speed stirring, constant temperature and pressure, centrifugal separation, n...
Embodiment 3
[0069] The tourmaline ceramic supported TiO 2 -The preparation technology of NCP immobilized photocatalyst comprises the following specific steps:
[0070] 1) Preparation of tourmaline ceramics
[0071] a. Cleaning, drying, pulverizing magnesium tourmaline, black tourmaline, lithium tourmaline and sodium manganese tourmaline, and processing it into 2500 mesh through Raymond machine or jet mill;
[0072] b. 7kg of polycrystalline tourmaline powder and 3kg of pottery clay were mixed and stirred for 60 minutes to form a uniform shape;
[0073] c. Slowly inject the water-soluble titanium hydroxide inorganic sol with a concentration of 0.90wt% into the beater according to the weight of 1:5, so that the tourmaline powder and clay form a solid state containing 30% of water, and the titanium hydroxide inorganic sol is made of Titanium tetrachloride + 35% ammonia water + 50% hydrogen peroxide, after high-speed stirring, constant temperature and pressure, centrifugal separation, natur...
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