Spraying type aqueous chitosan wound dressing
A wound dressing and chitosan technology, applied in medical science, bandages, etc., can solve the problems of chemical residues, long film-forming time, health hazards, etc., and achieve good water resistance, accelerated healing, and easy to carry effects
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Embodiment 1
[0034] Take by weighing the chitosan gel of 1g amount, the viscosity-average molecular weight (Mn) of the chitosan that prepares chitosan gel is 100000, and deacetylation degree is 95%, is dispersed in the distilled water of 100mL with homogenizer , to obtain uniformly dispersed chitosan turbid solution; keep the chitosan turbid solution at 5°C, and then pass carbon dioxide gas under a certain pressure state, and observe the color change of the solution, it can be found that the chitosan gel is turbid With the introduction of carbon dioxide, the solution changes from turbidity to clear and transparent state. Therefore, it can be seen that under the condition of low temperature and high pressure, chitosan gel can be dissolved in carbon dioxide.
[0035] Use a polarizing microscope (DYP-990 polarizing microscope, Shanghai Dianying Optical Instrument Co., Ltd.) to observe the dissolution of chitosan before and after the amount of carbon dioxide, and the magnification is 400 times...
Embodiment 2
[0037] Chitosan is made into a hydrogel, and then uniformly dispersed in distilled water, and carbon dioxide gas is continuously introduced under high pressure and low temperature conditions to obtain a chitosan solution, which is then sterilized by irradiation, canned, and sprayed chitosan is obtained. The syrup wound dressing and the chitosan aqueous wound dressing are stored in a high-pressure container bottle, and the spray-on chitosan aqueous wound dressing is composed of chitosan, glycerin, carbon dioxide and distilled water system, and the mass percentages of each component are respectively: Chitosan 4%, glycerin 2%, carbon dioxide 20%, distilled water 74%, wherein, the degree of deacetylation=90% of chitosan is selected, and the viscosity average molecular weight (Mη) is respectively: 10000, 50000, 100000, 170000.
[0038] Take pictures of the appearance of spray-on chitosan aqueous wound dressing prepared by chitosan with different viscosity-average molecular weight, s...
Embodiment 3
[0040] Chitosan is made into a hydrogel, and then uniformly dispersed in distilled water, and carbon dioxide gas is continuously introduced under high pressure and low temperature conditions to obtain a chitosan solution, which is then sterilized by irradiation, canned, and sprayed chitosan is obtained. The syrup wound dressing and the chitosan aqueous wound dressing are stored in a high-pressure container bottle, and the spray-on chitosan aqueous wound dressing is composed of chitosan, glycerin, carbon dioxide and distilled water system, and the mass percentages of each component are respectively: Chitosan 4%, glycerin 2%, carbon dioxide 20%, distilled water 74%, wherein, the viscosity average molecular weight (Mη) is: 50000, the degree of deacetylation (DD) of choosing chitosan is 75%, 90%, 95%, respectively. %.
[0041] Take pictures of the appearance of spray-on chitosan aqueous wound dressing prepared by choosing chitosan with different deacetylation degrees, see image ...
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