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Method utilizing biochar for preparing nanocarbon sol

A nano-carbon sol, bio-carbon technology, applied in nano-carbon and other directions, can solve the problems of complex post-processing, low production efficiency, low nano-carbon efficiency, etc., and achieve the effects of abundant resources, low cost and simple method.

Inactive Publication Date: 2017-03-22
BEIJING NAIAISI NEW MATERIAL TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] The nano-carbon prepared by the prior art generally has low efficiency and requires complicated post-processing
For example, the existing electrolyte does not use a neutral electrolyte, and the electrode uses a graphite electrode with a purity of more than 99%, which leads to low production efficiency
The prepared product is very easy to settle or agglomerate, which is difficult to apply to modern agriculture

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] The two electrodes are put into the neutral electrolyte aqueous solution, and the neutral electrolyte aqueous solution adopts carbon nanometer solution; the conductivity of the neutral electrolyte aqueous solution is adjusted to 2000 millisieverts, and the conductive material is placed between the two electrodes, and the two The conductive carbon material between the electrodes is granular or powdered conductive biochar, and the specific surface area of ​​the conductive carbon material is 500m 2 / g; the conductive carbon material is placed in a porous insulating container; the effective current density is 48A / m 2 , the distance between the two electrodes is 10cm, the voltage is equal to 110 volts, and the electrolysis time is 6 hours. Biochar uses charcoal to form conductive material after heating treatment, and adopts 400Hz DC pulse voltage.

Embodiment 2

[0018] Put the two electrodes into the neutral electrolyte aqueous solution, and the neutral electrolyte aqueous solution adopts carbon nanometer solution; the conductivity of the neutral electrolyte aqueous solution is adjusted to 1800 millisieverts, and the conductive material is placed between the two electrodes, and the two The conductive carbon material between the electrodes is granular or powdered conductive biochar, and the specific surface area of ​​the conductive carbon material is 500m 2 / g; the conductive carbon material is placed in a porous insulating container; the effective current density is 48A / m 2 , the distance between the two electrodes is 10cm, the voltage is equal to 110 volts, and an ultrasonic device is added at the same time, the frequency of the ultrasonic device is 10kHz, the power is 50w; the electrolysis time is 4 hours. Biochar uses charcoal to form conductive material after heating treatment, and adopts 400Hz DC pulse voltage.

Embodiment 3

[0020] The two electrodes are put into the neutral electrolyte aqueous solution, and the neutral electrolyte aqueous solution adopts carbon nanometer solution; the conductivity of the neutral electrolyte aqueous solution is adjusted to 2000 millisieverts, and the conductive material is placed between the two electrodes, and the two The conductive carbon material between the electrodes is granular or powdered conductive biochar, and the specific surface area of ​​the conductive carbon material is 200m 2 / g; the conductive carbon material is placed in a porous insulating container; the effective current density is 35A / m 2 , the distance between the two electrodes is 80cm, the voltage is equal to 110 volts, and the electrolysis time is 12 hours. Biochar uses straw charcoal to form conductive material after heat treatment, and adopts 400Hz DC pulse voltage.

[0021] The scope of the present invention is not limited to the scope of the examples that can be obtained is that the mas...

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Abstract

The invention discloses a method utilizing biochar for preparing nanocarbon sol. The method is characterized in that two electrodes are placed in a neutral electrolyte water solution, and a carbon nano solution is adopted in the neutral electrolyte water solution; the conductivity of the neutral electrolyte water solution is adjusted to range from 1,800 mSv to 2,000 mSv, a conductive material is arranged between the two electrodes, and the conductive carbon material between the two electrodes is particle or powder conductive biochar, and the specific surface area of the conductive carbon material is larger than 100 m<2> / g; the conductive carbon material is placed in a porous insulation container; the distance between the two electrodes is 1-80 cm, the voltage is smaller than or equal to 110 V, and the direct current pulse voltage of 1-400Hz is adopted; and the effective current density ranges from 35 A / m<2> to 48 A<2>, and the electrolysis time is 4-24 h. According to the method, the preparing time is greatly shortened, the electrode materials are not limited, and the cost can be obviously reduced.

Description

technical field [0001] The invention relates to the field of using nanometer carbon as a fertilizer additive. Background technique [0002] The nano-carbon prepared by the prior art generally has low efficiency and requires complex post-processing. For example, the existing electrolyte does not use a neutral electrolyte, and the electrode uses a graphite electrode with a purity of more than 99%, so the production efficiency is low. The prepared product is very easy to settle or agglomerate, and it is difficult to apply to modern agriculture. Contents of the invention [0003] A method for preparing nano-carbon sol by using biochar, characterized in that: two electrodes are placed in a neutral electrolyte aqueous solution, and the neutral electrolyte aqueous solution adopts a carbon nano solution; the conductivity of the neutral electrolyte aqueous solution is adjusted to 1800-2000 Millisieverts, the conductive material is placed between two electrodes, and the conductive...

Claims

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Application Information

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IPC IPC(8): C01B32/15C05D9/00
CPCC05D9/00C01P2004/64
Inventor 李开生邢文英左力刚
Owner BEIJING NAIAISI NEW MATERIAL TECH
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