A fingerprint detection method for the freshness of abalone viscera
A technology of abalone viscera and fingerprints, which is applied to measurement devices, instruments, scientific instruments, etc., can solve the problems of comparative research and less adaptive research on weight distribution algorithms, and achieves fast detection speed, simple operation and repeatability. Good results
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Embodiment 1
[0050] A fingerprint detection method for the freshness of abalone viscera, comprising the following steps (carrying out 10 groups in the same batch for processing and detection):
[0051] (1) Perform HS-SPME-based pretreatment on the abalone viscera samples: remove the viscera from the freshly bought abalone, homogenate and weigh the viscera, put each 0.3g portion into a ziplock bag, blow in nitrogen, A total of 15 samples were weighed, and the 0h test was carried out first on the 1st, and the remaining 7 samples were divided into two groups for storage in different groups. . 0h detection first: Weigh 0.3217g visceral homogenate into a 4mL headspace bottle, add 1.4mL saturated saline, preheat at 30°C for 10min, push the SPME handle to insert the fiber head of the extraction head into the headspace bottle, Then place it on a magnetic stirring heater with an equilibrium temperature of 80°C and a rotation speed of 90 rad / min, keep it for 40 minutes, retract the extraction fiber...
Embodiment 2
[0058] A fingerprint detection method for the freshness of abalone viscera, comprising the following steps (carrying out 10 groups in the same batch for processing and detection):
[0059] (1) Perform HS-SPME-based pretreatment on the abalone viscera samples: remove the viscera from the freshly bought abalone, homogenate and weigh the viscera, put each 0.3g portion into a ziplock bag, blow in nitrogen, A total of 15 samples were weighed, and the 0h test was carried out first on the 1st, and the remaining 7 samples were divided into two groups for storage in different groups. . 0h detection first: Weigh 0.4112g visceral homogenate into a 4mL headspace bottle, add 1.5mL saturated saline, preheat at 35°C for 15min, push the SPME handle to insert the fiber head of the extraction head into the headspace bottle, Then place it on a magnetic stirring heater with an equilibrium temperature of 70°C and a rotation speed of 85rad / min, keep it for 60 minutes, retract the extraction fiber ...
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