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Environment-friendly low-temperature sintered high-heat-conduction dielectric paste and preparation method therefor

A technology of dielectric slurry and low-temperature sintering, which is applied in the direction of quartz/glass/glass enamel, electrical components, circuits, etc., can solve the problems of low temperature-resistant flexible heating film and high thermal conductivity dielectric slurry, and achieve good environmental protection characteristics , the effect of good heat conduction effect

Inactive Publication Date: 2017-05-17
DONGGUAN COREHELM ELECTRONICS MATERIAL TECH CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] There are a wide variety of dielectric paste products in the prior art; however, there are few reports on low-temperature dielectric pastes, especially high thermal conductivity properties of high-temperature resistant flexible heating films

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030] Embodiment 1, an environment-friendly low-temperature sintering high thermal conductivity medium slurry, including the following materials by weight, specifically:

[0031] Low melting point glass powder 10%

[0032] High thermal conductivity filler (AlN, particle size is 100nm) 45%

[0033] Organic binder phase 45%.

[0034] Among them, the particle size of the low-melting point glass powder is less than 5 μm, and the low-melting point glass powder is prepared according to the following parts by weight, specifically:

[0035] Bi 2 o 3 30%

[0036] V 2 o 5 10%

[0037] TeO 2 15%

[0038] B 2 o 3 10%

[0039] ZnO 7%

[0040] SnO 2 3%

[0041] CuO 10%

[0042] BaO 15%.

[0043] In addition, the organic bonding phase includes resin, solvent, and auxiliary agent; among them, the resin is ethyl cellulose, the solvent is terpineol, the dispersant used in the auxiliary agent is BYK-AT204, and the disinfectant used in the auxiliary agent is BYK-AT204. The...

Embodiment 2

[0062] Embodiment 2, an environment-friendly low-temperature sintering high thermal conductivity medium slurry, including the following materials by weight, specifically:

[0063] Low melting point glass powder 15%

[0064] High thermal conductivity filler (AlN, particle size 1μm) 40%

[0065] Organic binder phase 45%.

[0066] Among them, the particle size of the low-melting point glass powder is less than 5 μm, and the low-melting point glass powder is prepared according to the following parts by weight, specifically:

[0067] Bi 2 o 3 25%

[0068] V 2 o 5 10%

[0069] TeO 2 20%

[0070] B 2 o 3 15%

[0071] ZnO 7%

[0072] SnO 2 3%

[0073] CuO 10%

[0074] BaO 10%.

[0075] In addition, the organic binder phase includes resin, solvent, and additives; among them, the resin is polyvinyl butyral, the solvent is terpineol, the dispersant used in the additive is BYK-AT204, and the additive used in the The antifoaming agent used in the product is BYK-066N,...

Embodiment 3

[0094] Embodiment 3, an environment-friendly low-temperature sintering high thermal conductivity medium slurry, including the following materials by weight, specifically:

[0095] Low melting point glass powder 20%

[0096] High thermal conductivity filler (AlN, particle size is 500nm) 40%

[0097] Organic binder phase 40%.

[0098] Among them, the particle size of the low-melting point glass powder is less than 5 μm, and the low-melting point glass powder is prepared according to the following parts by weight, specifically:

[0099] Bi 2 o 3 30%

[0100] V 2 o 5 10%

[0101] TeO 2 25%

[0102] B 2 o 3 10%

[0103] ZnO 8%

[0104] SnO 2 2%

[0105] CuO 8%

[0106] BaO 12%.

[0107] In addition, the organic binder phase includes resin, solvent, and additives; among them, the resin is polyvinyl butyral, the solvent is terpineol, the dispersant used in the additive is BYK-AT204, and the additive used in the The antifoaming agent used in the product is BYK-0...

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Abstract

The invention discloses environment-friendly low-temperature sintered high-heat-conduction dielectric paste and a preparation method therefor. The dielectric paste is prepared from the following materials based on weight percentages: 5-30% of low-melting-point glass powder, 10-60% of high-heat-conduction filler and 15-60% of organic binding phase; and the organic binding phase is prepared from the following materials based on weight percentages: 5-50% of resin, 10-90% of solvent and 0.8-21% of auxiliaries. The dielectric paste has the following advantages as follows: 1, no environmental pollution content and achieving a good environmental protection effect; 2, comprising low-melting-point glass powder and having low-temperature sintering characteristic; and 3, by virtue of the added high-heat-conduction filler, achieving a high heat conduction effect; the preparation method comprises the following technological steps of 1, preparing the low-melting-point glass powder; 2, preparing the organic binding phase; and 3, preparing the dielectric paste; and by adoption of the preparation method, the environment-friendly low-temperature sintered high-heat-conduction dielectric paste can be effectively produced and prepared.

Description

technical field [0001] The invention relates to the technical field of electronic materials, in particular to an environment-friendly low-temperature sintered high thermal conductivity medium slurry and a preparation method thereof. Background technique [0002] Dielectric paste is the basic material for the manufacture of thick film heating elements. It is a paste made of low-melting glass powder, organic binders and additives that are uniformly mixed by three-roll rolling (reminiscent of toothpaste, paint, etc.). For the dielectric slurry, on the one hand, it can be used as a transition layer between the substrate of the heating element and the electrothermal function layer to relieve interlayer stress and improve the bonding strength between the electric heating unit and the substrate; The packaging material ensures the insulation of the surface of the heating element and improves its heating uniformity and heat transfer speed. [0003] There are a variety of dielectric ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01B3/08C03C12/00
CPCH01B3/084C03C12/00H01B3/087
Inventor 蒋国辉苏冠贤
Owner DONGGUAN COREHELM ELECTRONICS MATERIAL TECH CO LTD