Synthesis method of lithium iron phosphate positive material for lithium ion battery
A lithium-ion battery, lithium iron phosphate technology, applied in the direction of battery electrodes, phosphorus compounds, chemical instruments and methods, etc., can solve the problem of high raw material cost, achieve uniform particle size, low production cost, maintain consistency and stability Effect
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[0031] Battery preparation and electrochemical performance test method
[0032] ①. Preparation of battery positive sheet:
[0033] The obtained lithium-ion battery cathode material lithium iron phosphate, conductive carbon powder, and organic binder polyvinylidene fluoride (PVDF) were mixed according to a mass ratio of 92:3:5 to obtain a mixed body, and 10 grams of the mixed powder. Add 12 grams of N-methylpyrrolidone (NMP), an organic solvent, and stir thoroughly to form a slurry, which is coated on the surface of the aluminum foil, dried, and rolled several times to obtain a battery positive electrode sheet;
[0034] ②. Battery assembly and performance test
[0035] The electrochemical performance of lithium iron phosphate was evaluated using a 2016 type half-cell. The rolled battery pole pieces are stamped into 12 mm diameter discs. After accurately weighing their mass, the mass of lithium iron phosphate in the pole pieces is calculated according to the formula composition. A diap...
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[0037] Example 1
[0038] A method for synthesizing lithium iron phosphate as a positive electrode material for lithium ion batteries, which specifically includes the following steps:
[0039] (1) Add 115 parts of phosphoric acid to 400 parts of deionized water, stir to form a phosphoric acid solution, add 56 parts of reduced iron powder to the above phosphoric acid solution under stirring, and react for 2 hours, then add the resulting product to the ball mill After 2h of ball milling, the material is discharged to obtain a precursor A;
[0040] (2) Dissolve 42 parts of lithium hydroxide and 15 parts of sucrose in 250 parts of deionized water, and add the resulting lithium hydroxide solution to the precursor A obtained in step (1) under stirring, and then obtain the result after stirring. Precursor B;
[0041] (3) The precursor B obtained in step (2) is spray-dried with a small two-fluid spray dryer in the laboratory under agitation. The feed rate is controlled at 5ml / min, and the...
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[0046] Example 2
[0047] A method for synthesizing lithium iron phosphate as a positive electrode material for lithium ion batteries, which specifically includes the following steps:
[0048] (1). Add 105 parts of phosphoric acid to 400 parts of deionized water and stir to form a phosphoric acid solution. Under stirring, add 50 parts of reduced iron powder to the above phosphoric acid solution and react for 2 hours, then add the resulting product to the ball mill After ball milling for 2h, the material is discharged to obtain a precursor A;
[0049] (2). Dissolve 38 parts of lithium hydroxide and 15 parts of sucrose in 250 parts of deionized water to obtain a lithium hydroxide solution, add it to the precursor A obtained in step (1) under stirring, and obtain the precursor after stirring. 物B;
[0050] (3) The precursor B obtained in step (2) is spray-dried with a small two-fluid spray dryer in the laboratory under agitation. The feed rate is controlled at 5ml / min and the temperatu...
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